一种制氢预转化催化剂还原的新方法

对上海高桥分公司2×10~4m~3/h(标准状态)制氢装置原设计的预转化催化剂还原流程进行了改进。先跳开预转化反应器,利用转化炉制取氢气,再用自产的高纯氢气代替重整氢,对预转化催化剂进行单独升温还原,避免了催化剂在还原初期因发生甲烷化反应而超温失活的问题,使催化剂具有更好的活性和稳定性。     

A Relational Model of Workplace Victimization: Social Roles and Patterns of Victimization in Dyadic Relationships.

This article proposes a model of the ways in which dyadic interactions between employees who occupy 1 of 4 archetypal social roles in organizations can lead to either episodic or institutionalized patterns of victimization. The model shows how the occurrence of victimization involving these 4 role types is influenced by organizational variables such as power differences, culture, and access to social capital. The model integrates behavioral and social structural antecedents of victimization to develop a relational perspective on the dynamics of harmful behavior in the workplace. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Reduction mechanism of tioglycolic acid on keratin fibers using microspectrophotometry and FT-Raman spectroscopy

In order to investigate the reduction mechanism of thioglycolic acid (TG) on the keratin fibers, cross-sectional samples of white human hair treated with TG were prepared. The heterogeneous reaction between TG and keratin fibers involving the diffusion of TG into human hair was analyzed at the molecular level using microspectrophotometry and FT-Raman spectroscopy. The diffusion of TG into human hair clearly increased by increasing the treatment time and by raising pH. The TG relative concentration and the disconnected relative concentration of disulfide (–SS–) groups at various depths of the hair samples with pH 9.0 were in good agreement, indicating that the reaction rate (the disconnection of –SS– groups) was faster than the diffusion rate of TG into human hair. From these experiments, we demonstrated that TG diffuses gradually beyond the cuticle region, and toward the inside of the cortex region along with the disconnection of –SS– groups.     

Estimation and Optimization of the Principal H-Maser Parameters

The scale along the coordinate axes in the equations of motion hitherto used for an H-maser (in relative units) is shown to depend on Q as the quality factor for an H-maser. This hinders both analysis of the operation of the H-maser and optimization of its parameters. The modified equations of motion proposed here do not have that shortcoming. We determine the atomic flux into the bulb that gives the H-maser the best metrological characteristics.     

Failure analysis of a broken tooth

Several days after heart surgery, a patient discovered his upper right canine tooth had broken at the root. Such tooth damage, recognized post-operatively, is usually assumed to be caused by blunt mechanical force from an instrument used by the anesthesiologist during placement of a breathing tube at the start of surgery. In this case, the patient had saved the crown portion of the broken tooth, and it was possible to examine the root fracture characteristics. The curvature and direction of the crack path and natural tooth situation suggested that failure could be described through a cantilever beam model. This was confirmed when a whole extracted sample tooth was embedded and broken by a measured force in a manner consistent with the model. The resulting fracture surface matched that of the patient’s broken canine tooth. However, the high load and force direction necessary to fracture the root was inconsistent with forces applied during the anesthesia procedure. The failure analysis and further investigation indicated tooth clenching on the breathing tube during recovery was the likely cause of fracture. This paper presents an alternate explanation for intubation-related dental injury, demonstrates the practicality of fractographic analysis of biological materials, and introduces a methodology for simulating in vitro tooth settings for mechanical testing.     

基于WVD的防空雷达直升机信号特征分析

基于直升机目标旋转部件的调制模型，本文针对防空雷达提出了分析直升机信号特征的一种新方法——WVD法，并对直升机目标旋转部件调制回波信号在不同噪声情况下加以仿真分析，结果表明：用WVD分析雷达回波中直升机信号特征是一种非常有效的方法。     

600 A IGBT开关电路及其散热系统设计

采用IGBT开关电路，对大功率电阻带进行直流脉宽调制控制，实现了内燃机车大功率直流发电机负载实验中的负载大小的连续调节。为了避免在实验过程中IGBT器件的温度过高，采用独特的双管IGBT结构和双向强迫风冷的散热系统。实验表明该电路运行稳定、可靠。     

饼干炉湿度控制的改进方法

在大空间的温度控制系统中 ,采用简单的PID控制规律 ,对空间的温度、湿度进行解藕计算 ,将空间的相对湿度控制转化为送风含湿量的控制。该控制方式稳定、可靠 ,并且节约能源。本方法适用于所有的烘烤炉中     

天然气井井筒及井口安全技术研究

天然气勘探开发具有高温、高压、高风险,安全技术及管理难度大等特点,通过实例分析天然气井存在的主要问题,提出应采取的关键安全技术及需要解决的问题。     

丙烯腈－苯乙烯共聚物水解磺化产物对泥浆的稳定作用

在实验室条件下对用丙烯腈－苯乙烯共聚物在硫酸存在下的水解磺化产物（ＨＳＡＳ）处理的泥浆性能进行了评定。ＨＳＡＳ处理的泥浆有较小的滤失性，较好的耐盐和抗高温性。