Kinetics study of Ti[O(CH2)4OCHCH2]4 initiated ring‐opening polymerization of ε‐caprolactone by differential scanning calorimetry

Chemical shrinkage was used for the in situ measurement of the progressing chemical stabilization reactions and the influence of ozone during the stabilization of polyacrylonitrile. A method for evaluating the activation energy through the sensitivity temperature is presented. The calculated results show that the activation energies were 161.57 kJ/mol in air and 181.23 kJ/mol in ozone-enriched air. Therefore, the chemical reactions were postponed during stabilization in ozone-enriched air. Ozone seemed to act in three ways: first, ozone promoted the formation of the serious skin–core structure. Second, ozone accelerated the chemical reactions and shortened the stabilization time at lower heating rates. Third, ozone postponed the chemical reactions. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci 2008     

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Numerical Simulation of Deforming Manufacture Process for Automobile Bevel Gear Blank

1 Introduction Rear axle bevel gearis a vital kind of annular accessory with high precision and hugeload availablefeatures ,andit is widely used as the differential drive in automobiles and tractor .In China ,the traditional manufactureapproach of producing the rear axle bevel gear blankis die forging,which not only requires a highinvestment ofproduct equipments , but also involves a low material utilization and great noise .In order to overcome thesedrawbacks , manyresearchers have done a gre…     

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