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151.
In the absence of a bulk diffusion effect, it is shown for the first time that the impedance spectra for the chlorine evolution reaction on a rotating thin ring electrode comprise three consecutive semicircles in the capacitive half of the complex plane. The first (highest frequency) semicircle is due to the charge-transfer resistance for chloride discharge and the simultaneous chlorine adsorption coupled to the double-layer capacitance. The second semicircle (around 5 Hz) is due to the adsorption and desorption of a chlorine intermediate. The third (lowest frequency, around 0.5 Hz) semicircle is due to the relaxation of surface oxygen species. The impedance data allow the steps of the overall reaction to be examined individually. On a Pt surface the rate of chloride discharge and simultaneous chlorine adsorption (the admittance of the first semicircle) is first order with respect to chloride concentration and has a potential-dependence close to 58 mV/decade. The rate of the adsorption and desorption process (the admittance of the second semicircle) is second order with respect to chloride concentration, and has a potential dependence close to 30 mV/decade. The time constant for the adsorption/desorption processes is ca 20 ms, independent of electrode potential in the range studied. These features are consistent with a mechanism in which a faster discharge reaction (Cl− Clad + e) is followed by a slower surface combination reaction (2Clad → Cl2), but inconsistent with mechanisms in which ion + atom desorption is predominant, the initial chloride discharge is slow, or a unipositively charged chlorine species is involved. 相似文献
152.
本文通过对某液压挖掘机工作装置实验样本长度的研究,详细讨论了样本长度的确定方法,重点分析了趋势曲线拟合法,提出了样本长度精度区间分析的方法,并在处理大量实验数据的基础上,从载荷分布及寿命估算的角度做了实际的验证.编制了应用程序,使样本长度确定至寿命估算整个过程程序化. 相似文献
153.
154.
Learning a sequence of target locations when the sequence is uncorrelated with a sequence of responses and target location is not the response dimension (pure perceptual-based sequence learning) was examined. Using probabilistic sequences of target locations, the author shows that such learning can be implicit, is unaffected by distance between target locations, and is mostly limited to first-order transition probabilities. Moreover, the mechanism underlying learning affords processing of information at anticipated target locations and appears to be attention based. Implications for hypotheses of implicit sequence learning are discussed. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
155.
156.
采用隔壁精馏塔分离苯-甲苯-对二甲苯物系,用Aspen Plus软件模拟了隔壁精馏塔内温度分布及液相组成分布,考察了汽相和液相分配比对产品纯度的影响。对隔壁精馏塔模拟得到的优化操作条件为:隔壁精馏塔的理论板数为30块,侧线采出在第14块理论板,进料段为15块理论板,在进料段的第7块理论板进料,进料组成n(苯)∶n(甲苯)∶n(对二甲苯)为1∶3∶1,回流比为8.8,液相分配比为2.96,汽相分配比为0.83。在此条件下,各组分的摩尔分数大于98.5%,与实验结果基本吻合。当进料组成n(苯)∶n(甲苯)∶n(对二甲苯)为1∶3∶1时,采用隔壁精馏塔可比常规两塔流程节能27.18%。 相似文献
157.
针对炼铁厂炼焦车间贮煤塔和开闲器驱动装置存在故障频繁,堵煤、开闭器易损坏和吹风管堵塞等问题,通过分析并结合实际情况,将煤塔漏嘴由27只减为9只双曲线形状漏嘴,开闭器驱动装置由车载驱动改为固定驱动。改造后,解决了使用中堵煤及开闭器驱动装置损坏等问题,降低了设备故障率,减少了生产成本,增加了装煤量,满足了生产需要。 相似文献
158.
159.
南水北调中线水源工程丹江口水力发电厂机电设备改造项目已进入实施阶段。对电厂机电设备改造的范围、内容、进度安排进行了介绍,对直接指定汉江集团作为安装单位的原因进行了阐述,对设备改造过程中存在的工作难点和技术难题进行了分析。 相似文献
160.
Polyurethanes were prepared from pure 4,4′-diphenylmethane diisocyanate (MDI), 1,4-butane diol (BDO) or 1,2-ethane diol (EDO) and α,ω-hydroxyl poly(propylene oxide) (PPO) by reaction injection moulding (RIM). Hard segment (MDI + BDO or EDO) level was 45–50 wt%. The PPO had about 20% ethylene oxide copolymerized in at the chain ends to provide 80% primary OH end groups. Mn was varied from 2000 to 4000. Dibutyl tin dilaurate catalyst and mould temperature were varied. Dynamic mechanical, wide-angle X-ray, differential scanning calorimeter, molecular weight and tensile elongation measurements were made on the RIM polyurethanes. At low reaction rates (low catalyst or temperature) highly crystalline, well phase separated but low molecular weight polymers were produced. At high catalyst or temperature levels more poorly phase separated but high molecular weight, tough polymers resulted. Higher Mn PPO gave better phase separation and EDO gave higher melting temperatures. Preventing hard segment crystallinity by substituting asymmetric MDI or glycols resulted in phase compatibility. 相似文献