XRD测定炭素材料的石墨化度

介绍了用X射线衍射(XRD)测定炭素材料石墨化度的原理和方法,指出:用高纯硅粉作内标校准测量误差是必要的;当炭石墨的衍射线呈现不对称时,必须进行多重峰分离,这说明试样含有不同石墨化度的组分,同时可计算出它们相应的含量。     

细粒砂金选收研究

为选收细长、密实、不规则的细粒砂金，保证其在分选中的有效重力大干介质阻力，应制定以跳汰为基础的船选工艺和先分级、后分选的岸上选厂工艺，优选适宜矿砂各自特性的选矿设备和操作参数．恰当地应用旋流器、人造草皮和毛毯等．也可有效地捕收细粒砂金．     

梅山高炉瓦斯泥综合利用的研究

分析研究国内外高炉粉尘使用情况，结合梅山高炉瓦斯泥的性质、特征和现状，提出用弱磁-强磁选的选矿方法，从梅山高炉瓦斯泥中回收铁精矿的设想。通过试验室试验，取得了较好的技术经济指标，达到了预期效果，并可降低锌含量。     

基于复杂性寻踪的非独立图像盲分离

复杂性寻踪是近期发展起来的一种结合非高斯性和时间相关的投影寻踪方法,目的是在多元数据中找到一个投影方向,使得数据在该方向上的投影具有最令人感兴趣的结构。它是投影寻踪方法在时间序列应用上的扩展,相似于依赖时间的信号源盲分离和独立分离分析。由相互独立的图像混合而成的混合图像的盲分离技术已经相当成熟,但对非独立混合的图像的盲分离仍然是个难题。从时间序列的复杂性寻踪出发,推导出一个复杂性寻踪的定点算法。该算法是经典的快速独立分量分析算法（FastICA）的扩展,继承了FastICA的优点,简单易行,不需要用户选择学习率,并且算法具有快速稳定收敛的性质。该算法应用到非独立图像的混合图像的盲分离时,取得了较好的分离结果。     

Rapid growth of angle-confined large-domain graphene bicrystals

In the chemical vapor deposition growth of large-area graphene polycrystalline thin films,the coalescence of randomly oriented graphene domains results in a high density of uncertain grain boundaries (GBs).The structures and properties of various GBs are highly dependent on the misorientation angles between the graphene domains,which can significantly affect the performance of the graphene films and impede their industrial applications.Graphene bicrystals with a specific type of GB can be synthesized via the controllable growth of graphene domains with a predefined lattice orientation.Although the bicrystal has been widely investigated for traditional bulk materials,no successful synthesis strategy has been presented for growing two-dimensional graphene bicrystals.In this study, we demonstrate a simple approach for growing well-aligned large-domain graphene bicrystals with a confined tilt angle of 30° on a facilely recrystallized single-crystal Cu (100) substrate.Control of the density of the GBs with a misorientation angle of 30° was realized via the controllable rapid growth of subcentimeter graphene domains with the assistance of a cooperative catalytic surface-passivation treatment.The large-area production of graphene bicrystals consisting of the sole specific GBs with a tunable density provides a new material platform for fundamental studies and practical applications.     

Operational experience and relation to deposition process for NEG-coated chambers installed on the ESRF electron storage ring

A majority of the ESRF insertion device sections have been equipped with NEG-coated low gap vacuum chambers made of extruded aluminium and PVD coated with a low-temperature non-evaporable getter coating at ESRF. The low initial outgassing and quick conditioning allowed some modifications for chamber installation and accelerator restart procedures. The operational behaviour of those chambers has been studied not only by means of vacuum gauges but also with ionisation chambers measuring the bremsstrahlung sent to the connected synchrotron beamlines. The NEG-coating film thickness was optimised taking into account vacuum performance and also coating process parameters and duration. The 2nd more flexible and powerful NEG-coating device is under commissioning in the NEG-coating facility at ESRF.     

一种新型的激光—等离子体辅助化学气相沉积装置的研究

为探索用激光离子体共同辅助化学气相沉积过程以实现室温沉积的可能性，设计并制造了一种新型的ＣＶＤ装置，实际了ＳｉＨ４－ＮＨ３－Ｎ２体系制取Ｓｉ３Ｎ４膜的试验。结果表明，激光和等离子体是可以相互促进，共同辅助ＣＶＤ过程的，且两者均处于较代的能量水平。     

中煤龙化KDON-30000/24000型空分设备工程建设总结

简介中煤龙化KDON-30000/24000型空分设备的工艺流程和主要技术参数,阐述在空分工程建设及试压过程中出现的问题和处理办法,从仪控组态和管道设计两方面对空分设备工程设计提出了建议,最后总结空分设备工程建设经验。     

焦化汽柴油加氢捕硅剂的制备及性能评价

目的 脱除焦化汽柴油馏分中的有机硅化合物,避免催化剂硅中毒。方法 以拟薄水铝石粉为载体制备原料,镍钼为活性金属组分,采用等体积浸渍法制备了加氢捕硅剂,利用N₂吸附脱附、X射线衍射、吡啶红外光谱、扫描电镜等方法对其进行分析表征,并在200 mL加氢中试装置上考查了捕硅剂的脱硅活性和2 000 h活性稳定性。结果 自主开发的捕硅剂比表面积和孔容较高,酸性适宜,活性金属分布均匀,强度满足工业装置装填要求。捕硅剂的脱硅活性较高,在典型的工业条件下,脱硅率>90%,在2 000 h活性稳定性试验过程中,脱硅率稳定>90%,活性稳定性良好,且具有较高的容硅能力。结论 自主开发的捕硅剂具有广阔的工业应用前景,对清洁燃料的生产及保护装置的长周期稳定运行具有十分重要的意义。     

采煤机位置监测装置的原理与应用

介绍了采煤机位置监测装置的主要功能、组成、工作原理以及应用。