The interfacial microstructure of joined single crystal and polycrystalline alumina

The interfacial microstructures of 96 and 98% polycrystalline alumina joined with single crystal sapphire have been investigated in relation to the joining parameters. Joining has been evaluated based on either using a thin spin-on silica interlayer or by placing the alumina and sapphire in direct contact. The materials were joined by placing the coated or uncoated surfaces in contact and heating in the range of 1340–1475 °C with minimum external load. With the aid of a silica interlayer, sapphire and 98% polycrystalline alumina were successfully joined in 180 min at 1400 °C and above, while samples without a silica interlayer failed to join under these conditions. However, sapphire and 96% polycrystalline alumina were joined both with and without the use of silica interlayer. A variety of interfacial morphologies have been observed, including amorphous regions, fine crystalline alumina, and intimate contact between the sapphire and polycrystalline alumina.     

A novel automated image analysis method for maceral analysis

A new image analysis technique has been developed which allows maceral analysis of coal to be carried out. The technique is able to separate the liptinite component from the background resin by using two separate images of the surface captured with different camera exposure times. At normal exposure, the liptinite has a similar grey scale value to the surrounding resin, but at a higher exposure time, the resin remains black whilst the liptinite grey scale increases significantly enough to distinguish it from the resin. The method has been tested for repeatability and reproducibility and found to be within the ISO Standard requirements.     

生物超微弱发光的光子计数成象方法

介绍了我们研制和设计的用于测量生物超微弱发光的光子计数成象系统，包括光子成象头，高帧频ＣＣＤ摄象机，图象采集系统和计算机，可以定量地探测出生物的发光强度分布 ，还能够显示出其发光的图象，确定发光的形状和位置，本系统的信噪比为１０：１，最小探测功率达１０＾－１６Ｗ，灵敏度高，动态范围大。     

In－BiCaVIG的晶体生长与性能

本文报导了用助熔剂法成功地生长大尺寸掺铟ＢｉＣａＶＩＧ晶体的方法以及实验结果，介绍了该单晶在近红外区的磁光器件中的重要应用。     

LED显示技术的现状和发展

综合介绍了ＬＥＤ显示技术的现状，详细叙述了全色ＬＥＤ显示的关键技术和主要性能，对ＬＥＤ在室内，室外的应用前景作出评述。     

强度型光纤传感器的信号检测系统

本文阐述了一种可提高强度型光纤传感器测量精度的检测系统。该系统利用同一检测电路交替检测信号、参考通道的输出信号，并将信号、参考两通道的检测结果相除，从而消除了因发光二极管光源波动及检测电路系统不稳定所带来的误差。采用同步相关技术抑制了噪声，提高了输出信噪比。实验证明，当时间常数ＲＣ为０．０５Ｓ时，采用该检测系统可获得优于千分之一的零点稳定性和优于２×１０３的输出信噪比。     

ERD facility for analysis of hydrogen and deuterium in solids

Hydrogen is the lightest element in nature, and so, its detection and quantitative analysis is difficult by the conventional methods utilized for other elements. In the recent years the technique of elastic recoil detection analysis (ERD) using 1–2 MeV He⁺ beam has been developed to quantitatively and simultaneously analyze hydrogen and its isotopes in solids. Such a facility has been set up using the 2 MeV Van-de-Graaff accelerator at IIT Kanpur. It facilitates H and D analysis in a material up to a depth of ∼ 1μm with a detection sensitivity of 0·1 at.% and depth resolution of about 300 ?. The application potential of this setup is illustrated by presenting the results of measurements performed on Al:H:D systems prepared by plasma source ion implantation and highT _c YBCO pellets exposed to humid atmosphere.     

湿化学法制备纳米ATO导电粉

采用非均相成核法 ,在Sn(OH) 4 晶种上均匀生长Sb掺杂Sn(OH) 4 ,制备纳米ATO粉末。以电阻测定系统研究了合成条件如掺杂浓度、反应温度、pH值、SnCl4浓度等对最终粉末电阻性能的影响。以TG DSC热分析、XRD、TEM等手段研究了晶粒生长过程 ,XRD显示为四方金红石型结构 ,平均粒径为15nm。当Sb/Sn(mol比 ) =0 .0 5 ,pH =2 ,T =60℃ ,SnCl4=1.2～ 1.8mol·L-1时 ,粉体电阻小于 0 .5Ω。     

非晶硅基薄膜的等离子体刻蚀光发射谱检测

本文研究了采用锁定放大相干检测技术的等离子体光发射谱检测系统。用该系统检测了仅用CF4作为刻蚀气体刻蚀非晶硅基薄膜的等离子体光发射谱。分析了检测结果和刻蚀机理。