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181.
氮化铝(AIN)因其具有高热导率,作为基片材料在电子元器件中得到日益重视。本文主要论述了氮化铝陶瓷制备过程中各种烧结参数,包括烧结助剂、烧结气氛、保温时间、常压烧结、热压烧结、微波烧结和等离子烧结等对氮化铝陶瓷性能的影响。并指出可通过合适的AIN粉体制备技术,结合快速烧结方法可得到具有晶粒细小、结构均匀、高致密度和高导热率的AIN陶瓷。 相似文献
182.
This paper reports the development of a method for simultaneously measuring zeolite, silicate, and phosphate in laundry detergent
products by inductively coupled plasma atomic emission spectrometry. A sample is decomposed under alkaline oxidative conditions
to decompose zeolite, silicate, phosphate, and organic substances. Then hydrochloric acid is added to the decomposed solution
to dissolve aluminum hydroxide precipitate before analysis. This sample preparation procedure was investigated by using a
total organic carbon analyzer and was confirmed to be applicable to simultaneous measurements of zeolite, silicate, and phosphate.
Relative standard deviation for the analysis is less than 2.1%, recovery is more than 99.0%, and the calibration curve gives
a correlation coefficient ofR=1.000. The detection limit of this method for aluminum and silicon is 0.1%, and for phosphorus, 0.2% by weight in the product.
This method is applicable to various laundry detergent products that contain zeolite, silicate, or phosphate and is five times
faster than the three wet chemical methods. 相似文献
183.
184.
采用金属铝粉氧化大量放热的自分散法与MgO合成镁铝尖晶石和在低温下直接制成高纯镁铝尖晶石制品进行了研究。结果表明:在1400℃温度下可制成镁铝尖晶石制品。 相似文献
185.
186.
The preparation of near stoichiometric spinel and alumina-rich spinel composites from Al2 O3 and MgO powders with the addition of Na3 AlF6 up to 4 wt% in the temperature range 700°–1600°C was studied; 98 wt% spinel containing 72 wt% Al2 O3 can be produced from the mixture of 72 wt% (50 at.%) Al2 O3 + 28 wt% (50 at.%) MgO powders with the addition of 1 wt% Na3 AlF6 fired at 1300°C for 1 h. Spinels containing 81–85 wt% Al2 O3 can be produced from either the mixture of 90 wt% (78 at.%) Al2 O3 + 10 wt% (22 at.%) MgO or the mixture of 95 wt% (88 at.%) Al2 O3 + 5 wt% (12 at.%) MgO powders with the addition of 4 wt% Na3 AlF6 in the temperature range 1300°–1600°C by using a torch-flame firing for 3 min, followed by quenching in water, while the same system under slow cooling in a furnace results in spinel containing 74–76 wt% Al2 O3 . Microscopic studies indicate that the alumina-rich spinel composites consist of a continuous majority spinel phase and an isolated minority corundum phase, regardless of slow cooling in a furnace or quenching in water. 相似文献
187.
188.
Maud Cansell Noredine Moussaoui Alain Pierre Petit Alain Denizot Nicole Combe 《European Journal of Lipid Science and Technology》2006,108(6):459-467
Two n‐3 polyunsaturated fatty acid (PUFA)‐rich diets differing in their chemical and physical forms were given to rats during 2 wk. Liposomes [phospholipids (PL) organized in bilayer structures] made from a natural marine lipid extract or a mixture of fats containing fish oil [similar fatty acids esterified in triacylglycerols (TAG)] were used. The influence of n‐3 PUFA dietary sources on plasma parameters, i.e. TAG, cholesterol and PL concentrations, was investigated. A similar hypotriglyceridemic effect of n‐3 PUFA from liposomes or fish oil was observed. In contrast, feeding rats with liposomes led to different PL and cholesterol patterns. In the plasma of rats fed liposomes, total cholesterol amounts were positively correlated with PL levels. Liposome and fish oil feedings caused a marked increase in the amounts of n‐3 PUFA, which occurred mainly at the expense of n‐6 PUFA. However, the enrichment in n‐3 PUFA in the different plasma lipid classes differed substantially when ingested in the form of fish oil or liposomes. These results were interpreted in terms of different lipid bioavailability and metabolic fate during the digestive steps and in the liver, with the dietary source. 相似文献
189.
Z. F. Zhang Z. M. Sun H. Hashimoto T. Abe 《Journal of the European Ceramic Society》2002,22(16):2957-2961
To synthesize Ti3SiC2 samples, pulse discharge sintering (PDS) technique was utilized to sinter elemental powders of Ti/Si/C with stoichiometric and off-stoichiometric ratios in a temperature range of 1200–1500 °C. The results showed that high purity Ti3SiC2 could not be obtained from the Ti/Si/C powder with molar ratio of 3:1:2, and Ti3SiC2 preferred to form at relatively low sintering temperature for a short time. When 5Ti/2Si/3C and 3Ti/1.5Si/2C powders were sintered for 15 min, the TiC content was respectively decreased to 6.4 and 10 wt.% at 1250–1300 °C. The corresponding relative density of the samples sintered from 5Ti/2Si/3C powder was calculated to be as high as 99% at the temperature above 1300 °C. It is suggested that low-temperature rapid synthesis of Ti3SiC2 would be possible through the PDS technique, provided that the composition of the starting powders should be adjusted to be off-stoichiometric ratio from 3:1:2. 相似文献
190.
Two surface modification methods—plasma surface treatment and chemical agent treatment—were used to investigate their effects on the surface properties of ultrahigh‐molecular‐weight polyethylene (UHMWPE) fibers. In the analyses, performed using electron spectroscopy for chemical analysis, changes in weight, and scanning electron microscope observations, demonstrated that the two fiber‐surface‐modified composites formed between UHMWPE fiber and epoxy matrix exhibited improved interfacial adhesion and slight improvements in tensile strengths, but notable decreases in elongation, relative to those properties of the composites reinforced with the untreated UHMWPE fibers. In addition, three kinds of epoxy resins—neat DGEBA, polyurethane‐crosslinked DGEBA, and BHHBP‐DGEBA—were used as resin matrices to examine the tensile and elongation properties of their UHMWPE fiber‐reinforced composites. From stress/strain measurements and scanning electron microscope observations, the resin matrix improved the tensile strength apparently, but did not affect the elongation. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 655–665, 2007 相似文献