无溶剂重防腐环氧涂料的制备与研究

采用中低相对分子质量树脂体系以及改性脂环胺固化剂,以化学、物理防锈颜料,体质填料为粉料体系制备无溶剂重防腐环氧涂料。通过 EIS、划线盐雾剥离、耐 3. 5% NaCl溶液和 10% NaOH溶液、混合溶液浸泡后的附着力,研究了涂层屏蔽性、耐碱性、湿态附着力。结果表明：铁钛粉、 绢云母粉、长石粉粉料体系涂层屏蔽性、耐碱性最佳;改性脂环胺固化剂屏蔽性好,湿态附着力性能优异;采用 EIS、划线盐雾剥离,耐 3. 5% NaCl溶液、 10% NaOH溶液浸泡以及混合溶液浸泡后附着力下降程度来评价涂层屏蔽性、耐碱性、湿态附着力性能具有一定的可参考性,研究结果与涂层耐阴极剥离实验性能正相关,可用于涂层耐阴极剥离性能的早期评价与判断。     

露天铝土矿山粉尘治理措施

介绍了露天矿山铝土生产流程、产尘源及产尘设备。针对各产尘源的治理进行了分步分析。提出了治理措施。从而有效降低了铝土露天矿山生产过程中外排及岗位粉尘浓度。     

水平管内流型转换区湿气流经多孔板的压降特性

较之于传统的单孔板,多孔板有压损系数小、整流、低噪声等多方面优点,在湿气流量测量中具有重要应用价值。以空气和水为两相工质,在水平管内湿气流型转换区对小孔分别呈圆形和矩形的2个多孔板的压降特性进行了实验。结果表明:圆孔、槽孔多孔板的湿气压降特性无明显差别;多孔板的气相压降倍率与气相、液相弗劳德数均密切相关;与实验结果相比,现有均相流模型的预报结果均偏高,现有分相流模型的预报结果均偏低;通过气相、液相弗鲁德数双参数对孔板湿气压降模型进行修正,可明显提高压降关联式的预报准确度;基于均相流模型双参数修正所得的多孔板压降关联式的预报精度最优,对圆孔多孔板、槽孔多孔板的预报偏差分别在±7%、±10%以内。     

新型水下焊接电源及送丝机构的研究

研究了一种新型的水下焊接系统。系统中孤焊电源输出阶梯型的外特性，送丝系统采用脉动送丝方式。在单片机控制下，脉动送丝波形与外特性同步调控。在停止送丝阶段，单片机夸电源输出电压为峰值，焊丝在此电压下返烧并形成熔滴。送丝脉冲到来的瞬间，电源输出电压切换为基值。熔滴依靠送丝动量向熔地方向前进，最终向熔池过渡，随着焊炬的移动而彤成一道焊缝。实验结果表明，使用这个系统进行气体保护药芯焊丝水下湿法焊接时，电压、电流波形均匀工整，短路过渡频率受控，焊接过程稳定，水下焊缝成形较为美观。     

Machining characteristics and fracture morphologies in a copper-beryllium (Cu-2Be) alloy

The technology of materials removal is improved greatly by the introduction of advanced cutting tools like cubic boron nitride, ceramics, polycrystalline diamond and the more recent whisker-reinforced materials. In this paper, the influence of cutting temperature on machinability, mechanical properties, microstructure, and fracture morphology of Cu-2Be alloy using a polycrystalline diamond cutter is investigated. The information on machining, microstructure, and fracture morphology of Cu-2Be alloy are very useful to understand their fabrication characteristics and the basic mechanisms of its deformation and fracture. The machinability (in terms of surface finish) of Cu-2Be alloy is evaluated as a function of cutting temperature, resulting from wet and dry cutting. Machining is carried out on a Hardinge Cobra 42 CNC machine (Hardinge Inc., Elmira, NY), and the machining parameters used—cutting speed, depth of cut, and feed rate—are kept constant during both wet and dry cutting. The machined surface finish on Cu-2Be alloy is measured using a surface finish analyzer (Surftest 401, series 178) technique. The machined specimens are examined for their strength and hardness properties using a standard Universal Testing Machine and Rockwell hardness tester, respectively. Wet cutting (using coolants) produced a smooth surface finish when compared with dry cutting of the Cu-2Be alloy. The machined specimens are examined for their microstructural features using a Nikon optical microscope. The specimens are etched using a suitable etchant solution for revealing such microstructure constituents as grain size, phase proportions, and the possible overheated areas (especially in dry cutting). The fractured surfaces from the tensile and impact toughness tests are investigated for their fracture morphologies (dry and wet cutting) using a microprocessor-controlled scanning electron microscope (Jeol Model JSM 5910 LV). A detailed analysis is also made to understand and interpret the basic fracture mechanisms responsible for crack initiation and crack propagation. The Cu-2Be alloy showed relatively higher mechanical properties in wet cutting in comparison to dry cutting operations. Fracture studies demonstrated intergranular and ductile fractures as dominant modes of fracture mechanisms in Cu-2Be alloy.     

2010年长江流域暴雨洪水初步分析

分析2010年长江流域暴雨洪水,有利于更全面认识长江流域暴雨洪水特性,可为今后更好开展长江流域防汛水情保障工程。从主汛期长江流域暴雨及气候特征、干支流主要洪水过程及洪水特性等方面,进行了初步的总结和分析。2010年长江主汛期洪水发生范围广、持续时间长且局部地区洪水量级大,通过与三峡水库蓄水前后几次大的历史洪水分析对比,初步认为,2010年长江流域主汛期出现的洪水为长江上中游区域性较大洪水。     

一种新型MEMS双稳态微电磁驱动器的研究

介绍了一种新型MEMS双稳态微电磁驱动器,通过理论分析和有限元分析工具Ansys对器件的结构参数进行了优化设计,并证明了设计的可行性。利用金属基表面微加工技术与体硅微加工技术成功制作出这种驱动器,并对其弹性平台的弹性系数进行了标定,对驱动器的双稳态进行了调试。结果表明：此驱动器具有良好的双稳特性,响应时间短（约10ms）的特点。     

Reinforced Wool Keratin Fibers via Dithiol Chain Re-bonding

Regenerated wool keratin fibers (RWKFs) have heretofore attracted tremendous interest according to environmental friendliness, ample resource, and intrinsic biocompatibility for broad applications. In this realm, both uncontrollable keratin fibril assembly procedure and resultant insufficient mechanical strength, have greatly hindered their large-scale manufacture and commercial viability. Herein, a continuous wet-spinning strategy is put forward to rebuild wool keratin into compact regenerated bio-fibers with improved strength via disulfide re-bonding. Dithiothreitol (DTT) has been introduced to renovate disulfide linkage inside keratin polypeptide chains, and bridge keratin fibrils via covalent thiol bonding to form a continuous backbone as mechanical support. A thus-derived RWKF manifests a tensile strength of 186.1 ± 7.0 MPa and Young's modulus of 7.4 ± 0.2 GPa, which exceeds those of natural wool, feathers, and regenerated wool or feather keratin fibers. The detailed wet-spinning technical parameters, such as coagulation, oxidation, and post-treatment, have been systematically optimized to guarantee the continuous preparation of high-strength regenerated keratin fibers. This work offers insight into solving the concurrent challenges for continuous manufacture of regenerated protein fibers and sustainability concerns about biomass waste.     

微波杀菌及包装材料的微波穿透性对湿豆皮保鲜品质的影响

目的 探究不同包装材料结合微波杀菌对湿豆皮保鲜效果的影响,为湿豆皮提供新的保鲜方案。方法 将湿豆皮分别装入OPP/PE和PET/PE/CPP材料的包装袋中,经密封后进行微波杀菌处理,测定其贮藏期间的指标。结果 经微波处理后,湿豆皮在OPP/PE中的表面温度比在PET/PE/CPP中高8 ℃,菌落总数少0.66 lg(CFU/g),说明微波更易穿透OPP/PE材料,更能有效延缓长期贮藏中因微生物活动造成的氧气含量下降和二氧化碳上升,延缓湿豆皮的pH值、水分含量和拉伸性的下降,抑制其TVB-N含量的上升,从而抑制组织结构的破坏,减缓脂质酸败的速率,还可减小色差的变化幅度,维持更高的感官评价得分。结论 采用微波处理能够有效延长湿豆皮的保鲜期,OPP/PE和PET/PE/CPP材料组湿豆皮的保鲜期分别延长了15、12 d左右,且对不同材料包装的湿豆皮品质的影响差异显著。采用微波穿透性更好的包装材料,其微波作用强度更大,杀菌效果更明显,保鲜效果更好。     

Wet Chemical Treatment and Mg Doping of p-InP Surfaces for Ohmic Low-Resistive Metal Contacts

Manufacturing a low-resistive Ohmic metal contact on p-type InP crystals for various applications is a challenge because of the Fermi-level pinning via surface defects and the diffusion of p-type doping atoms in InP. Development of wet-chemistry treatments and nanoscale control of p-doping for InP surfaces is crucial for decreasing the device resistivity losses and durability problems. Herein, a proper combination of HCl-based solution immersion, which directly provides an unusual wet chemical-induced InP(100)c(2 × 2) atomic structure, and low-temperature Mg-surface doping of the cleaned InP before Ni-film deposition is demonstrated to decrease the contact resistivity of Ni/p-InP by the factor of 10 approximately as compared to the lowest reference value without Mg. Deposition of the Mg intermediate layer on p-InP and postheating of Mg/p-InP at 350 °C, both performed in ultrahigh-vacuum (UHV) chamber, lead to intermixing of Mg and InP elements according to X-ray photoelectron spectroscopy. Introducing a small oxygen gas background (O₂ ≈ 10⁻⁶ mbar) in UHV chamber during the postheating of Mg/p-InP enhances the indium outdiffusion and provides the lowest contact resistivity. Quantum mechanical simulations indicate that the presence of InP native oxide or/and metal indium alloy at the interface increases In diffusion.