快速烧结法制备连续碳化硅纤维

通过熔融纺丝，不熔化处理制得连续聚碳硅烷（ＰＣＳ）不熔化纤维，采用快速烧结方法制备出性能较好的连续ＳｉＣ纤维。探讨了气封条件的选择，以及烧结速度对ＳｉＣ纤维的组成，结构及性能的影响。结果表明，快速烧结条件下，可以实现向纤维上施加张力以及纤维的无机化转变，烧结速度加快会降低纤维的Ｃ／Ｓｉ（原子比），同时有利于提高纤维的抗拉强度和热稳定性。     

炉外钢包采用合成渣粉脱硫试验

针对抚顺钢铁公司１５吨转炉脱硫效率低的状况，进行了炉外钢包合成渣粉脱硫试验，提高了脱硫效率，增加了经济效益。     

Preparation and Properties of Sintering Additives Coated Si3N4 from Heterogeneous Nucleation Processing

The sintering additives such as Al2O3 and /or Y2O3 were coated on the surfaces of Si3N4 particles via heterogeneous nucleation processing using a buffered pH solution as the precipitation reagent .They nucleated and grew only on the surfaces of Si3N4 and did not form sol particles in solution by TEM observation .The isoelectric point(IEP) of coated Si3N4 was different from that of as-received Si3N4.The IEP of Al(OH)3-coated Si3N4 occurred at pH8.4, which is close to that of alumina .When Al(OH)3-coated Si3N4 particles were coated with Y(OH)3,the IEP of coated Si3N4 powder shifted from pH8.4 to pH9.2 ,similar to that of yttria.In addition ,the rheological data showed that Al2O3 and /or Y2O3 coated Si3N4 suspension is nearly Newtonian and that added Si3N4 suspension shows a shear rate thinning behavior.     

BaTiO_3系PTCR热敏电阻器用烧结助剂的研究

研究了烧结助剂的作用，实验结果表明：如只引入半导化元素，不引入烧结助剂，则室温电阻率ρ２５很大，甚至是绝缘体。由于烧结助剂的加入，既改善了ＰＴＣＲ热敏电阻陶瓷的烧结性，又改善了其ρ２５、耐电压Ｖｂ、ＰＴＣ效应等特性，从而使产品的各种特性易于重复。烧结助剂昔日多用ＡＳＴ，现在常用ＳｉＯ２，其加入量ｘ宜小于２％。ＳｉＯ２的纯度、杂质等化学特性，与粒子形状、粒度分布、晶系等物理特性，对ＰＴＣＲ热敏电阻器的电性能有很大的影响。据此提出了ＢａＴｉＯ３系ＰＴＣＲ热敏电阻器用ＳｉＯ２的技术标准。     

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本文介绍了采用复合吸收剂净化天然气的试验结果,在现有三甘醇等脱水剂中添加单乙醇胺,在脱水的同时脱除H_2S,在保证净化气露点低于-21℃的条件下,使净化气中H_2S含量亦低于5mg/m～3。     

全钒钛矿冶炼时添加剂对钛渣脱硫能力的影响

1 前言 生铁中的含硫量对生铁质量影响很大。全钒钛矿冶炼时,由于渣中TiO_2。在高温和还原条件下生成Ti(C、N )等物质,使钛渣性能变坏,恶化钛渣脱硫的动力学条件,导致钛渣脱硫能力下降。本研究旨在探讨全钒钛矿冶炼时加入添加剂对钛渣脱硫能力的影响。