具有除草活性的双膦酸衍生物的研究动态

许多含双膦酸结构单元的化合物都显示了良好的除草活性,本文对这类化合物的结构特点、生物活性以及相关的研究动态进行了归纳和概述。     

溴化锂致冷液中铁的催化动力学法测定

在硫酸介质中，痕量铁（Ⅲ）对过氧化氢与甲基橙的氧化还原作用有一定的催化活性，当加入1，10－菲Luo啉作活化剂，其反应速度加快。本文探讨了该催化褪色体系测铁的最佳条件。本法检出限为3．2ng/ml，测定范围0－0．30μg/25ml。将其用于溴化锂致冷液中铁的测定，其变动系数为2．23－4．26％，回收率为97－105％，本法与原子吸收法分析结果基本一致。     

生长温度对等离子体增强化学气相沉积生长ZnO薄膜质量的影响

以Zn(C2 H5) 2 和CO2 为反应源 ,在低温下用等离子体增强化学气相沉积方法 ,在Si衬底上外延生长了高质量的ZnO薄膜。用X射线衍射谱和光致发光谱研究了衬底温度对ZnO薄膜质量的影响。X射线衍射结果表明 ,在生长温度为2 3 0℃时制备出了高质量 ( 0 0 0 2 )择优取向的ZnO薄膜 ,其半高宽为 0 2 6°。光致发光谱显示出强的紫外自由激子发射与微弱的与氧空位相关的深缺陷发光 ,表明获得了接近化学配比的ZnO薄膜     

Preparation of Laminin-apatite-polymer Composites Using Metastable Calcium Phosphate Solutions

A synthetic polymer with a laminin-apatite composite layer on its surface would be useful as a percutaneous device. The preparation of such a composite was attempted in the present study using poly（ ethylene terephthalate ） （PET） and polyethylene （PE） as the synthetic polymer. PET and PE plates and those pretreated with an oxygen plasma were alternately dipped in calcium and phosphate ion solutions, and then immersed in a metastable calcium phosphate solution supplemented with laminin （ LCP solution ）. The PET and PE plates pretreated with an oxygen plasma formed a uniform and continuous layer of a laminin-apatite composite on their surfaces. In contrast, the PET and PE plates that had not been pretreated with an oxygen plasma did not form a continuous layer of a laminin-apatite composite on their surfaces. The hydrophilic functional groups on the PET and PE surfaces introduced by the plasma treatment were responsible for the successful laminin-apatite coruposite coating.     

烧结钕-铁-硼永磁材料的研究进展

钕-铁-硼磁体被称为第三代稀土永磁材料，烧结钕-铁-硼磁体是目前综合磁性能最高的永磁材料。介绍了烧结钕-铁-硼磁体的研究现状、应用领域，阐述了烧结钕-铁-硼磁体的有关理论及先进生产工艺的特点，重点分析了低氧湿压、片铸、放电等离子烧结等工艺的特点，指出了目前国内烧结钕-铁-硼磁体存在的主要问题及今后的研究方向。