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991.
放电等离子烧结工艺对Ca3Co4O9陶瓷织构及电性能的影响 总被引:1,自引:0,他引:1
采用溶胶-凝胶与放电等离子烧结(SPS)相结合的方法制备了Ca3Co4O9陶瓷.通过X射线衍射、扫描电镜等表征手段,研究了放电等离子烧结工艺对Ca3Co4O9物相、显微结构和性能的影响.实验结果表明片状颗粒和放电等离子烧结工艺,特别是烧结温度的提高有利于Ca3Co4O9织构的形成.初步认为是片状颗粒在脉冲电流所产生的脉冲磁场作用下发生重排,使颗粒定向排列.本实验范围内,当烧结温度从700℃提高到900℃时,Ca3Co4O9晶粒取向度从0.75增大到0.87,700℃下的电阻率从6.24×10-5 Ωm降低到5.59×10-5 Ωm.此外,Ca3Co4O9块体表现出典型的半导体电学特征,电导率随着SPS烧结温度和测量温度的升高而增大,当SPS烧结温度为850℃时,P型Ca3Co4O9化合物在700℃有最大电导率. 相似文献
992.
993.
994.
机械合金化过程中Fe75 Al25二元系统的结构演变 总被引:7,自引:3,他引:7
采用X射线衍射仪、差式扫描量热仪等研究机械合金化过程中Fe75Al25元素混合粉的结构演变及热处理对粉体结构的影响。研究表明:球磨过程中,Al向Fe中扩散,直至Al完全溶入Fe中形成非平衡过饱和固溶体Fe(Al)。球磨过程中,Fe75Al25元素混合粉晶粒细化呈现先快后慢的趋势,球磨25h后的晶粒尺寸为6.9nm。Fe75Al25元素混合粉在球磨后的热处理过程中,由无序的Fe(A1)固溶体向有序的DO3-Fe3Al金属间化合物转变。 相似文献
995.
Naphthenic acid corrosion (NAC) and erosion-corrosion (NAEC) behavior of Mo-bearing (0-7.0 wt.%) stainless steels have been investigated in laboratory to evaluate the essential role of Mo on their NAC and NAEC resistance. The NAC and NAEC resistance of a high-velocity-oxygen-fuel (HVOF) thermal sprayed Mo-bearing stainless-steel coating was also investigated in both laboratory and an oil refinery. It was found that increasing the Mo content remarkably enhanced the NAC and NAEC resistance of stainless steels. The Mo-rich areas or phases in the steels played an importance role in resisting the NAEC. The HVOF coating showed excellent NAC and NAEC resistance in laboratory tests. The 700-day field test in an oil refinery revealed that the coating can effectively prevent the carbon-steel substrate from erosion-corrosion during long-term exposure in oil-refining environment. The corresponding NAC and NAEC mechanisms of the stainless steels and the beneficial role of Mo were discussed by taking account of inherent susceptibility of metal elements to corrosion, possible effects of Mo on surface films, and Mo-induced change in microstructure and microhardness. 相似文献
996.
综述了内氧化法制备Al2O3/Cu复合材料的研究现状,总结了内氧化法制备Al2O3/Cu复合材料的必备条件,对内氧化动力学和热力学进行了详细的阐述,并以Cu2O为氧源,采用内氧化法制备了Al2O3/Cu复合材料,验证了其优越的室温和高温性能;对以复合材料棒材为原料制备的点焊电极进行装机试验,结果表明其寿命为传统Cu-Cr—Zr电极的3~5倍;最后着重分析了内氧化法制备Al2O3/Cu复合材料发展过程中亟待解决的问题。 相似文献
997.
微量稀土Er对Al-5Mg合金组织与性能的影响 总被引:12,自引:0,他引:12
采用铸锭冶金法,制备含不同量稀土元素Er的Al-5Mg合金。利用拉伸力学性能测试、OM、XRD、SEM、TEM及EDS分析等分析测试手段,研究微量Er对Al-5Mg合金微观组织与力学性能的影响。结果表明:Er可以明显提高Al-5Mg合金的强度,添加0.4%Er(质量分数)的Al-5Mg合金的冷轧态屈服强度(σ0.2)提高了81MPa,而延伸率变化不大;Er的加入还能减少Al-5Mg合金的枝晶偏析,并可显著细化合金的晶粒组织;Er对晶粒的细化机理与其添加量有关,当Er含量较低时,符合传统的稀土细化机理;当Er含量较高时,由于在熔体中形成了初生Al3Er质点,在结晶形核时可以作为非均质形核核心,从而可显著细化晶粒组织;Er对合金的强化效应主要来自于晶粒细化及在晶内形成的细小二次Al3Er质点。根据实验结果可知,添加0.4%Er可使合金具有较为优异的综合性能。 相似文献
998.
999.
Akhtar Farid GUO Shi-ju 《中国有色金属学会会刊》2006,16(3):629-632
Pressureless infiltration process to synthesize Si3N4/Al composite was investigated. Al-2%Mg alloy was infiltrated into Si3N4 and Si3N4 containing 10% Al2O3 preforms in the atmosphere of nitrogen. It is possible to infiltrate Al-2%Mg alloy in Si3N4 and Si3N4 containing 10% Al2O3 preforms. The growth of the dense composite of useful thickness was facilitated by the presence of magnesium powder at the interface and by flowing nitrogen. During infiltration Si3N4 reacted with aluminium to form Si and AIN, the growth of composite was found to proceed in two ways, depending on the Al2O3 content in the initial preform. Firstly, preform without Al2O3 content gives rise to AIN, Al3.27Si0.47 and Al type phases after infiltration. Secondly, perform with 10% Al2O3 content gives rise to AIN-Al2O3 solid solution phase (AION), MgAl2O4, Al and Si type phases. AlON phase was only present in composite, containing 10% Al2O3 in the Si3N4 preforms before infiltration. 相似文献
1000.
A novel grating matching method for 3D reconstruction 总被引:2,自引:0,他引:2
Automatic 3D surface reconstruction has been an important research topic in digital photogrammetry for many years. Shaping from stereoscopic information is one of the widely studied topics in computer vision. Its central part is to solve the stereo matching problem automatically. Most algorithms used to solve the matching problem can be categorized as either area-base techniques or feature-based techniques. Feature-based techniques have gained more and more popularity for and it is the method that supports activities in object recognition and image understanding. But none of the former research can ensure the 100% matching exactness, thus, cannot complete high precision 3D surface measurement. In order to improve the precision of 3D measurement, we design a novel grating matching method, which can ensure 100% matching accuracy. It does not need any other assistant symbol or flag, only select one of the gratings which have to be projected to the objects. On the beginning of the measurement, the background of the object is captured by a CCD camera. Later gratings include single grating and group gratings will be projected to the object in sequence. All the images include gratings will make a subtraction with the background. The difference of the two images will be treated as 3D cues to acquire the 3D shape. Because no recognizing work is needed, the location of the single grating and each one in the group can be positioned exactly. From a lot of experiments, the proposed grating matching method is proved and it is a technique with high precision, low costs, easy operation, and an automatically matching method. Furthermore, it can be widely used in most of 3D vision recovery systems. 相似文献