真空热还原制锂工艺的技术经济分析

系统介绍了以碳酸锂为原料 ,加入石灰或铝氧土后 ,经焙烧、硅铁或铝粉真空热还原制取金属锂的工艺。本法与氯化锂熔体电解制取锂的工艺相比 ,具有产品成本低、纯度高、环境状况好的优点。     

纳米Fe粉的制备研究

总结了纳米Fe粉的制备方法,重点介绍了一种新的制备方法——封闭循环氢还原法。该方法以FeSO·47H2O和NaOH为原料,采用沉淀方法制备粒径为30～70nm的Fe2O3粉末,其反应条件为:反应温度50℃,反应终点pH值大于12,陈化时间1h。用封闭循环氢还原法,在400℃下还原Fe2O3得到了Fe粉。其粒径在20～50nm之间,含量为99.16%。     

Repair of Cracked Aluminum Overhead Sign Structures with Glass Fiber Reinforced Polymer Composites

Transportation departments have been using aluminum overhead sign structures since the 1950s. It is well documented that cracks develop in the welds between diagonal and chord members due to fatigue stresses from wind-induced vibration of the slender members. The cracks propagate to complete failure of the members, which can cause collapse of the truss and inflict injuries. The original design of overhead sign structures did not consider fatigue as a limit state. In addition, field welding of aluminum structures for any possible repairs is prohibited. A repair method for the cracked aluminum welded connections between diagonals and chord members using glass fiber reinforced polymer composites (GFRPs) is proposed. The static load carrying capacity of the welded connection, and the cracked connection repaired with GFRP composites are established. The paper describes the surface preparation of the aluminum tubular members, and the architecture and application sequence of the GFRP composite to retrofit the connection. Experimental results are presented from static tests of welded aluminum connections, welded aluminum connections retrofitted with GFRP composites, and new aluminum connections that depend only on GFRP composite elements for their strength. The results from monotonic static tests carried out on cracked welded specimens from actual sign structures show that the retrofitted connection with GFRP reinforcement achieved 1.17 to 1.25 times the capacity of the welded aluminum connection without any visible cracks. This result, and the minimal traffic disruption anticipated in the actual field application, makes this retrofit method a good candidate for implementation.     

铝对W9Mo3Cr4V高速钢组织和硬度的影响

用Ｘ－射线仪，扫描电镜和透射电镜系统研究了铝对钨钼系高速钢铸态，退火以及淬回火组织的影响，铝含量超过２．０％，淬火组织中出现含析出合金的铁素体组织和晶界屈氏体，导致钢硬的降低。     

天津钢管公司DRC直接还原厂生产工艺与自动控制

天津钢管公司DRC直接还原厂将采用英国戴维国际工程公司的DRC煤基直接还原技术,以铁矿石、煤、石灰石为原燃料,用回转窑来生产直接还原铁(DRI)。该厂将由两条回转窑生产线组成,每条生产线的生产能力为15万tDRI/年,回转窑规格为φ5.0m×80m。工厂生产主线将采用计算机集散控制系统(DCS)以实现对生产过程的自动控制。     

Reduction of Stibnite at Moderate Temperature

Reduction of stibnite with hydrogen in the presence of calcium oxide has been experimentally inves-tigated at moderate temperature. The results reveal that the effluent generated in the reduction pro-cess contains much less air-polluting substance H_2S, and that the reaction activation energy is63. 3 kJ/mol. The form of antimony changes considerably when the reaction temperature varies.     

熔融还原炉内二次燃烧和传热

总结了熔融还原炉内二次燃烧和传热的研究成果，对于转炉采用二次燃烧提高废钢比也有借鉴作用。