从废钼合金催化剂中提取钼等有价元素方法的研究

ＭｏＣｏＮｉ合金料首先氧化焙烧碱浸出，滤饼再加纯碱焙烧水浸出使钼与钴镍分离，最后用萃取法分离钴镍的工艺流程，对废钼合金催化剂进行了综合回收。采用该工艺流程和生产线分别生产出合格的工业级钼酸钠、氧化钴和氧化镍。     

化学镀Ni－Cu－P合金的工艺及镀层性能研究

探讨了化学镀Ｎｉ－Ｃｕ一Ｐ合金的镀液组成及工艺条件，并采用Ｘ射线衍射和弯曲法，研究了Ｎｉ－Ｃｕ－Ｐ镀层的组织结构和镀层结合力，结果表明，所研究的镀液组成，在适当工艺条件下，能够实现Ｎｉ、Ｃｕ离子的共沉积，并得到良好质量的合金镀层。经４００℃热处理，镀层中有和相析出，同时硬度达到最大值。镀态下，该镀层具有良好的结合力，且随镀层中铜含量的增加和热处理温度的提高，镀层结合力能得到进一步改善。     

焊前处理方式对LF6铝合金扩散焊的影响

利用Ｇｌｅｅｂｌｅ－１５００热／力模拟试验机，研究了ＬＦ６铝合金的扩散焊工艺，通过对焊接温度、压力、时间的调整和选用不同的料前处理方法，确定了最佳的扩散规范，研究结果表明：在一定的温度和时间范围内，ＬＦ６５铝合金扩散焊接头的剪切哟度随焊接温度和时间的增加而提高；化学浸蚀法比机械打磨法能更有效的去除铝合金表面的氧化膜；在现有试验条件下，得到ＬＦ６铝合金扩散焊的最佳规范参数，搭接试扩散焊接头的剪切强度     

PC／ABS合金的研制及其在汽车上的应用

对ＰＣ／ＡＢＳ合金开发和研制及其在汽车上的应用作了评述。介绍了上海杰事公司在该领域的进展。     

AN EXPERIMENTAL INVESTIGATION OF THE GROWTH OF SMALL CORNER FATIGUE CRACKS IN ALUMINIUM 6061-T651

Results of an experimental investigation of the fatigue growth of small corner cracks emanating from small flaws are presented. Growth-arrest behaviour was observed, and increases in crack length during growth periods were of the order of the transverse grain size. For the test material, the corner crack front intersects, on average, only three–six grains in the small crack regime monitored, so only a small number of constrained, interior grains is encountered. It is suggested that the presence of partially constrained surface grains may contribute to the 'anomalous' growth behaviour which has been observed by a number of investigators.
The crack growth histories of the test data presented exhibit considerable scatter. It is shown that a Student's t -test can be used to estimate confidence intervals in order to provide a measure of the observed scatter. The variation in confidence intervals in the transition from small to long fatigue crack growth is discussed.     

Pre-bainitic Transformation in Fe-Ni Alloy

Ｔｈｅｐｒｅ－ｂａｉｎｉｔｉｃｐｈｅｎｏｍｅｎｏｎｉｓｏｎｅｏｆｔｈｅｉｍ－ｐｏｒｔａｎｔｓｕｂｊｅｃｔｓｏｆｂａｉｎｉｔｉｃｔｒａｎｓｆｏｒｍａｔｉｏｎｗｈｉｃｈｉｓｓｔｉｌｃｏｎｔｒｏｖｅｒｓｉａｌ．Ｏｎｅｖｉｅｗｉｓｔｈａｔｔｈｅｓｏｌｕｔｅａ...     

高强度低密度大模量菲晶态Ai—Li合金

利用单辊快速凝固装置制备出高强度、低密度、大楼量的非晶态Ａｌ６１Ｌｉ２．５Ｙ２５Ｎｉ１１．５（ｗｔ－％）合金，其最大拉伸断裂强度、显微硬度和弹性模量分别为１０３９ＭＰａ、４８８ＤＰＮ和９８．７ＧＰａ．与同成分的晶态合金相比，具有较高的电极电位、较宽的电压钝化区，其腐蚀抗力为晶态合金的７倍．在恒加热速率的晶化过程中出现４个晶化峰，晶化激活能的计算表明，Ａｌ６１Ｌｉ２．５Ｙ２５Ｎｉ１１．５非晶合金的晶化过程为一级反应．     

烧结直接淬火对WC－TiC－Co合金WC相微观结构及力学性能的影响

本文以ＴＥＭ和ＸＲＤ为主要手段，研究ＷＣ－ＴｉＣ－Ｃｏ硬质合金（ＹＴ１４）在直接淬火后ＷＣ相的微观结构和微观应力，比较了常规烧结态与淬火态试样ＷＣ相之间的差异，探讨了直接淬火对合金力学性能的影响。结果表明，在保持合金其他性能不降低的同时，直接淬火的抗弯强度比常规烧结提高２８％左右。并首次发现，经直接淬火热处理的ＹＴＩ４合会中与Ｃｏ相相邻的ＷＣ晶粒边界出现滑移台阶，这是淬火过程中热应力使ＷＣ晶粒内位错在｛０００１｝密排面聚集，并可能沿｛０００１｝＜１１２０＞易滑移系统强滑移的结果。直接淬火试样的微观应力比重新加热淬火的低。     

Thermal expansion of Pyros from 20 to 1273 K

Pyros, which is a Ni-base alloy (82% Ni, 8% Cr, 4% W, 3% Mn, and 3% Fe), has been used extensively in France since 1926 as a temperature sensor and as a reference material for thermal expansion measurements. In this paper we present recent data on the expansion and expansivity of Pyros from 20 to 1273 K. Expansivity results, obtained by taking the derivative of a cubic-spline polynomial fitting performed to the L/L experimental data, show that Pyros is a stable material in the 20 to 1273 K temperature range. Furthermore, since the expansivity values are similar to those of steels, Pyros should be of special interest to laboratories which are concerned with expansion measurements on steels. Therefore, we suggest that Pyros be considered as a suitable reference material for thermal expansion measurements on steels, and until more accurate results are obtained, we propose our results as reference data between 20 and 1273 K.Paper presented at the Ninth Symposium on Thermophysical Properties, June 24–27, 1985, Boulder, Colorado, U.S.A.     

铝阳极氧化膜颜色的检验和观察法

介绍铝及铝合金阳极氧化膜颜色的概念和描写,对颜色的儿种测量方法进行了比较,重点分析观察法及其在各国标准中的异同。在此基础上,提出了GB8013中的对颜色进行观察的条件和理论根据。