Early detection of ageing in solder joints through laser probe thermal analysis of the peltier effect

We have recently developed an optical contactless method for testing the quality of solder joints during accelerated thermal cycling ageing processes.¹ The method was based upon the measurement of the dynamic thermal behaviour of the joint to short bursts of Joule heating. It has proved to be efficient in revealing the formation of cracks at the lead-solder interface. We present a method to evaluate ageing at a much earlier stage in the cycling process. We have observed in earlier work,¹ that before cracks appear, structural changes occur in the solder at the lead-solder interface. The thermal response of the solder joint is recorded over time to a Peltier heat perturbation produced by flowing a current pulse through the interface where structural changes occur. The key point in this method is to discriminate the Peltier effect from the Joule thermal response because both effects generate heat. The variation of the early Peltier response in the thermal cycling ageing tests is seen as a quantitative signature of the structural changes in the lead-solder interface.     

核电厂管系振动鉴定

本文介绍了核电厂管道振动鉴定概况,讨论了目前使用的管系振动的鉴定方法,给出了鉴定准则。     

简易高性能纳秒脉冲发生器

为了实现电子散射飞行时间谱仪电子束的脉冲化及产生时一幅变换器的启动或停止信号。我们利用开关晶体管的雪崩特性研制了一个性能好，成本低的纳秒脉冲发生器。该发生器输出上升时间好于Ｉｎｓ，幅度达１０Ｖ的负尖脉冲，用作时一幅变换器的启动或停止信号；也输出上升时间约３ｎｓ，幅度５－３０Ｖ连续可调和宽度５－２３０ｎｓ可调的正脉冲，用作电子束脉冲化的调制信号，脉冲重复率为１５０×１０＾３ｓ＾－１。它可广泛用于类似     

高纯锗探测器的快定时性能及其应用

为了将高纯锗（ＨＰＧｅ）探测器用于快定时的物理实验中，本实验研究厂影响高纯锗探测器定时谱仪时间性能的各种因素，找出了获得谱仪最小时间分辨的各种最佳参数。并建立了分辨时间为４．１９ｎｓ，能量分辨率为２０ｋｅＶ，微分非线性好于±２．０％，计效率可承受１２０×１０￣３ｓ￣（－１）的时间微分扰动角关联谱仪。利用此谱仪，以￣（２０４）Ｂｉ为探针核，研究了Ｂｉ系高温超导的微观机理，取得了较好的结果。     

高放废液中^147Pm的测定

建立了高放废液中~(147)Pm的测定方法。用HDEHP萃取稀土,再用HDEHP萃淋树脂柱分离AM和稀土。然后用高效液相色谱法将~(147)Pm从Eu、Ce等其它稀土中分离出来,用液体闪烁法测量~(147)Pm的放射性活度。     

中国油田堵水技术综述

本文论述了我国油田堵水技术的发展及其在油田开发中的作用,总结和阐述了油井化学堵水技术和注水井吸水剖面调整技术的原理和效益,指明了实践证实的有成效的工艺方法和堵水技术发展方向。     

Dante Cicchetti: Award for Distinguished Senior Career Contributions to Psychology in the Public Interest.

Provides the biography of Dante Cicchetti and announces that he has received the APA Award for Distinguished Senior Career Contributions to Psychology in the Public Interest (2004) for his seminal role in bridging theory, research, and practice by fostering the emergence and coalescence of the field of developmental psychopathology. A selected bibliography is also provided. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Material removal and surface damage in EDM of Ti3SiC2 ceramic

Material removal and surface damage of Ti₃SiC₂ ceramic during electrical discharge machining (EDM) were investigated. Melting and decomposition were found to be the main material removal mechanisms during the machining process. Material removal rate was enhanced acceleratively with increasing discharge current, i_e, working voltage, u_i, but increased deceleratively with pulse duration, t_e. Microcracks in the surface and loose grains in the subsurface resulted from thermal shock were confirmed, and the surface damage in Ti₃SiC₂ ceramic led to a degradation of both strength and reliability.     

Flame retardant and the degradation mechanism of high impact polystyrene/Fe-montmorillonite nanocomposites

High impact polystyrene/Fe-montmorillonite (HIPS/Fe-MMT) nanocomposites were successfully prepared by melting intercalation. The nanostructures of HIPS/Fe-MMT were testified by X-ray diffraction (XRD) and transmission electron microscope (TEM). Corresponding to pure HIPS, the thermal stability of HIPS/Fe-MMT nanocomposites was notably improved. The peaks of heat release rate (PHRR) and the mass loss rate (MLR) were significantly reduced after the formation of the HIPS/Fe-MMT nanocomposites from cone calorimetry. And nanocomposites PHRR was further lower with the increase of Fe-MMT content in the range of 1 to 5 wt%. The degradation mechanism of HIPS and HIPS/Fe-MMT nanocomposites was conducted by pyrolysis gas chromatography mass spectrometry (Py-GC-MS). And the reason of the enhancement of thermal stability maybe is that structural iron is the operative site for radical trapping in the Fe-MMT and the nanostructure enhances the interaction of the chains of the HIPS.