热处理时间对LiFeP04的晶体影响

将氧化铁、磷酸二氢铵、碳酸锂混合,在高温条件下热处理形成熔融液,淬冷、干燥、研磨制得锂铁磷酸盐玻璃粉末,将锂铁磷酸玻璃粉末与柠檬按一定质量比混合,在氮气气氛条件下热处理制取磷酸铁锂,考察热处理时间对晶体的影响。利用X－射线衍射仪、扫描电子皿微镜分析样品物相成分、晶体微观结构、晶体粒径分布。根据分析结果显示LiFePO4的结晶度、粒径与热处理时间成正比。     

钛白副产硫酸亚铁制备超细透明氧化铁黄研究

以钛白粉厂副产物硫酸亚铁为原料,以氨水为沉淀剂,采用空气氧化法制备超细透明氧化铁黄.分别研究了影响晶种形成和晶体生长的主要影响因素.通过优化实验,得出了最佳工艺条件.晶种制备阶段：温度为30℃,空气流量为2L/min,溶液的pH为4～6,搅拌速度为400r/min,Fe2＋浓度为1mol/L.晶体生长阶段：温度为85℃,空气流量为2L/min,溶液pH为4～6.     

贫磁铁矿反浮选降硅试验

湖北省某地具有较为丰富铁矿资源,矿石中铁含量较低,原矿中全铁（TFe）含量约15%,属于贫磁铁矿,铁矿物的嵌布粒度较细,通过单一弱磁选很难得到全铁品位超过60%的铁精矿,针对该矿弱磁选精矿进行反浮选提铁脱硅研究,一粗一精开路反浮选流程精矿品位可达60%以上,铁回收率60%,产率50%左右.通过小型闭路试验,反浮选最终获得较好指标：精矿产率为68.57%,品位为58.62%,回收率为82.83%.     

Ore-blending optimization model for sintering process based on characteristics of iron ores

An ore-blending optimization model for the sintering process is an intelligent system that includes iron ore characteristics,expert knowledge and material balance.In the present work,14 indices are proposed to represent chemical composition,granulating properties and high temperature properties of iron ores.After the relationships between iron ore characteristics and sintering performance are established,the "two-step" method and the simplex method are introduced to build the model by distinguishing the calculation of optimized blending proportion of iron ores from that of other sintering materials in order to improve calculation efficiency.The ore-blending optimization model,programmed by Access and Visual Basic,is applied to practical production in steel mills and the results prove that the present model can take advantage of the available iron ore resource with stable sinter yield and quality performance but at a lower cost.     

不锈钢粉尘内配煤团块高温自还原过程中金属铁的聚集

用不锈钢生产中的高碱度二次粉尘制备内配煤团块,在高温下自还原获得含铬、镍的金属铁粒.研究影响铁粒聚集长大的因素.研究表明：（1）内配煤团块的渣相碱度（w（CaO）/w（SiO2））小于2.8时,还原产物冷却过程中渣相与金属铁粒才能自然分离.碱度越低,渣量越大,越不利于金属铁聚集长大;（2）提高内配碳比,渣相残碳量明显升高,渣中过量的碳阻碍金属相聚集长大;（3）提高还原温度,直接还原铁的海绵状结构解体,逐渐聚集成颗粒状金属铁.还原温度越高,越有利于金属铁的聚集长大     

Fe-Si droplets associated with graphite on blast furnace coke

Fe-Si droplets on the surface of blast furnace (BF) coke from 25 to 50 cm at the tuyere level are mostly composed of Fe3Si, which has various shapes (round, elongated, and irregular) and penetration degrees into the BF coke matrix. The shapes and penetration degrees may depend on the saturation of molten iron by silicon during interaction with the coke matrix. The droplets are covered by a tiny shell of carbon. Graphite observed inside the droplets can be divided into two categories: well-formed tabular crystals with relatively large size and flakes with structures similar as those in cast iron. The textures of the droplets reflect composition, interaction with the coke matrix, and cooling conditions.     

优选混凝剂及助凝剂处理低温低浊水的方法

文章研究了低温低浊水混凝剂及助凝剂的优化选择,考察了浊度、COD M n、氨氮等水质特征,分析了低温低浊水的处理效果。结果表明,混凝剂和助凝剂投加量增大,上清液中浊度、COD去除率不断提高。在PAFC用量为12 mg/L,活化硅酸用量为0.12 mg/L条件下,浊度、COD去除率分别达到最大值98.3%和87%,剩余浊度和剩余COD M n分别为0.21 NTU、0.64 mg/L。而PAC＋PAM表现出更好的除氨氮效果,剩余氨氮为0.07 mg/L。     

铜官山铜（铁）矿地质特征及找矿方向预测

矿区位于中生代溧阳火山盆地南西部,郎溪中生代红层盆地北侧,在东西向坳陷带和北北东向断裂带的交汇部位处,现已发现小型铜、铁矿床和多个铜铁矿化点。经过先期勘查,区内已圈定铜矿体3个,矿体平面形态为S形,矿体主要赋存于北北东断裂中,产状与断裂一致。矿石有益组分主要为铜、铁、铅、锌、金等。在铜官山矿床外围及深部具有较好的找矿潜力,铜铁矿找矿潜力较大。