稳定态二氧化氯杀菌剂的制备及应用

稳定态二氧化氯(C1O2)是一新型杀菌消毒剂，具有高效、广谱、安全的特性，适用范围广，不产生对人体有害物质。介绍了稳定态ClO2的性质、检测、制备条件及其在有关领域的应用。     

Effect of Nitrogen Atmosphere on the Densification of a 3-mol%-Yttria-Doped Zirconia

The densification behavior of a 3-mol%-Y₂O₃-doped ZrO₂ (3Y-ZrO₂) has been investigated under N₂ and O₂ atmospheres. Powder compacts have been sintered at 1550° and 1400°C for various times. The density of the specimen sintered at 1550°C is higher in N₂ than in O₂, while the contrary result is obtained in the case of the specimen sintered at 1400°C. Such results can be explained in terms of nitrogen solubility and oxygen vacancy in a ZrO₂ matrix. Because nitrogen solubility into the ZrO₂ increases with an increase in heat-treatment temperature, leading to the formation of oxygen vacancy, the densification rate becomes higher. The present study thus shows evidence of nitrogen solubility into the ZrO₂ and its role on the densification behavior of 3Y-ZrO₂.     

XH—14（15）直流不停电电源控制系统的改造

对ＸＨ－１４（１５）直流不停电电源控制系统存在的问题作了较全面剖析，所提出的和集控单元改造原控制系统是可行的。试验和运行结果表明，改造的新一代控制系统能较理想地满足负载要求。     

陀螺稳定装置载体角振动仿真模型构建方法

建立了坦克装甲车辆行驶角振动和陀螺稳定装置载体角振动关系的数学模型,实现了在坦克装甲车辆行驶振动条件下火炮稳定性能的计算机仿真测试,为评价火炮控制系统的设计提供了一种依据。     

Direct Measurement of Transformation Zone Strains in Toughened Zirconia

Residual strains responsible for crack tip shielding have been measured within transformation zones surrounding cracks in Mg-PSZ. Two techniques were used for strain measurement: moiré interferometry and high-resolution image matching. Both methods provide maps of differential in-plane displacements within the specimen surface intersected by the crack, the latter method with the higher resolution. The results are compared with finite-element analysis to assess surface relaxation effects, and the measured strains are used to evaluate the crack tip shielding stress intensity factor. Calculations based on the assumption that the unconstrained transformation strain is hydrostatic dilatation yielded results that were significantly smaller than the measured toughness increases.     

'Polymorph Method' Determination of Monoclinic Zirconia in Partially Stabilized Zirconia Ceramics

The polymorph method, which provides phase analysis from a small number of integrated intensities in a powder diffraction scan, is adapted for the determination of monoclinic zirconia in a mixture with cubic, tetragonal. and orthorhombic zirconias and the γ-phase (Mg₂Zr₅O₁₂). Such a mixture is representative of Mg-PSZ after subeutectoid aging. The quantitative determination of the monoclinic depends in principle on a knowledge of the relative amounts of the other phases present in the mixture. It is demonstrated, however, that without this knowledge, even in complex mixtures, the traditional polymorph method analysis gives an acceptable estimate of the monoclinic fraction in the sample.     

基于ANSYS的某型雷达稳定平台的有限元分析与优化

针对某方提出的在能实现功能的基础上,质量更轻、刚度更大的要求,设计了某型雷达稳定平台。运用Creo软件进行了雷达稳定平台的建模,简化后导入ANSYS软件中建立有限元模型。在建立有限元模型时,分别采用了不同划分网格的方法。改变了网格划分的方法,改变网格的关联中心,改变网格的关联度,改变网格细化度,进行网格质量比较,最终得到网格质量最好的有限元模型。网格畸变度从0.6达到了0.27。进一步改变平台的材料,并进行了模态分析,得到了平台前六阶固有频率。分析结果表明,改进设计使刚度基本不变,但是质量减轻了34.5kg,减轻了17.7%。稳定平台的结构设计方法、提高网格质量的方法和材料的改变方法,为同类设计与分析提供了参考。     

Solar furnace surface treatment of plasma-sprayed thermal barrier coatings

An original process of superficial thermal treatment is described. This process has been successfully applied to partially stabilized yttria-zirconia coatings (ZrO₂-Y₂O₃) to increase the lifetime of the thermal barriers. A thin superficial layer was melted, and morphological transformations were observed. A microstructural comparison between as-sprayed layers and thermally treated layers is presented.     

稳恒磁场下Ni-W合金镀膜的制备与耐蚀性

研究了施加稳恒磁场(0~1 T)对电镀Ni-W合金的影响。测定不同方向、不同强度稳恒磁场下的电流效率、合金组成及镀层的耐蚀性,并用扫描电镜和X射线衍射对镀层的微观形貌及结构进行了观察和分析。对实验结果进行了分析讨论,找出稳恒磁场对这些性能指标的影响规律。结果表明:与不施加磁场相比,施加磁场后镀层的表面更均匀、细致、平整;镀层的含钨量上升:当B⊥J,B=1.0 T时,含钨量上升了约7%;当B∥J,B=1.0 T时,含钨量上升了约9%;镀膜的非晶化程度增强;镀膜的耐蚀性提高;但Ni-W合金电镀的电流效率降低。     

Isothermal oxidation of physical vapor deposited partially stabilized zirconia thermal barrier coatings

Thermal barrier coatings (TBCs), consisting of physical vapor deposited (PVD) partially stabilized zirconia (PSZ, 8 wt.%Y₂O₃) and a diffusion aluminide bond coat, were characterized as a function of time after oxidative isothermal heat treatment at 1373 K in air. The experimental characterizations was conducted by X-ray diffraction analysis and scanning electron microscopy (SEM) with energy-dispersive spectroscopy. During cooling to room temperature, spallation of the PSZ ceramic coatings occurred after 200 and 350 h of isothermal heat treatment. This failure was always sudden and violent, with the TBC popping from the substrate. The monoclinic phase of zirconia was first observed on the bottom surface of the PVD PSZ after 200 h of isothermal heat treatment. The failure of TBCs occurred either in the bond coat oxidation products of αAl₂O₃ and rutile TiO₂ or at the interface between the oxidation products and the diffusion aluminide bond coat or the PSZ coating.