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121.
Analysis of lipid classes by solid-phase extraction and high-performance size-exclusion chromatography 总被引:1,自引:0,他引:1
Anu I. Hopia Vieno I. Piironen Pekka E. Koivistoinen Lea E. T. Hyvönen 《Journal of the American Oil Chemists' Society》1992,69(8):772-776
An improved method to analyze lipid classes of edible oils and fats by solid-phase extraction (SPE) and high-performance size-exclusion chromatography (HPSEC) is presented. A mixture of lipid standards was fractionated by the solid-phase extraction procedure (NH2 phase) into polar and nonpolar fractions; these were then submitted to analysis by HPSEC. The size-exclusion chromatographic columns were three styrene/divinylbenzene columns with pore sizes of 100 Å and 50 Å. Light-scattering was used for the detection system, and the parameters of the detector were optimized to minimize the difference between the responses of the compounds studied. With this procedure it was possible to separate the following lipid classes: triacylglycerols, diacylglycerols, monoacylglycerols and free fatty acids, sterols, sterol esters, tocopherols and carotenoids. Quantitative analysis was studied for a light-scattering detector with several lipid standards of different molecular weights and unsaturation levels. 相似文献
122.
M. Saaoudi E. Chassaing M. Cherkaoui M. Ebntouhami 《Journal of Applied Electrochemistry》2002,32(12):1331-1336
Electroless NiP films, with 12 to 16 wt % P, were deposited from a moderately acid solution. Thermogravimetric analysis indicates the presence of occluded hydrogen in the layers, which desorbs upon heating. The amount of incorporated hydrogen decreases when the pH of the solution or the nickel sulfate concentration is increased; by contrast it increases with hypophosphite concentration. Cyclic voltammetry, using an electrochemical quartz crystal microbalance, confirms the existence of parasitic reactions, namely the reduction of protons of the solvent during the cathodic process and oxidation of hydrogen during the dissolution of the layers. This behaviour is in qualitative agreement with the proposed reaction scheme. 相似文献
123.
Abstract— We have developed a process to fabricate optical components, such as a lens, prism, or diffuser, directly on to a glass substrate. Processes include precision mastering by diamond cutting and multi‐layer photopolymer (2P) molding to realize flat surfaces and the integration of multiple components with an alignment within a few micrometers. 相似文献
124.
微波萃取在食品化学中的应用 总被引:16,自引:0,他引:16
介绍了微波萃取技术在食品化学中的应用。其实质是用微波对萃取溶剂及物料加热,使溶剂的渗透率和扩散率大大提高,因此对食品营养成分或风味物质可以有铲地萃取分离。 相似文献
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128.
通过XDCAM、P2HD在大洋D^3-edit、D^3-edit HD、苹果非编上的测试,分析各自的特点,总结出相应的工作流程,为下一步的设备选型和应用打下基础。 相似文献
129.
R.A. Jacques J.G. Santos C. Dariva J. Vladimir Oliveira E.B. Caramo 《The Journal of Supercritical Fluids》2007,40(3):354-359
This work presents a study concerning the chemical characteristics and analytical separation process of the essential oil obtained from high-pressure carbon dioxide extraction of Ilex paraguariensis. The experiments were performed in a laboratory-scale unit in the temperature range of 20–40 °C, from 100 to 250 bar. A blend of the I. paraguariensis extracts was percolated through a preparative chromatographic column, containing silica gel, and successively eluted with 150 mL of each of the following solvents: hexane, toluene, dichloromethane, ethyl acetate, acetone and methanol. The raw extract and its fractions were analyzed by gas chromatography coupled to mass spectrometry detection (GC/MS). The fractionation procedure showed to be a good clean up technique due to the isolation of different classes of compounds in each fraction. Chromatographic analyses allowed the identification of caffeine, fatty acids and esters, phytol, squalene, Vitamin E, stigmasterol derivatives and saturated hydrocarbons. 相似文献
130.