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51.
The modification in the polymeric membrane combined with metallic film as well as composites with inorganic nanofiller can be used for separation of various gases, with hydrogen gas as it is widely used as fuel material. The change in free volume due to modification in polymer chains alters the transport mechanism. In this work, the transport behaviour of H2 across the different metal coated and nanocomposite membrane has been studied and compared with that of standard polycarbonate membrane. Transport properties changes due to the modification in the composition of nanofiller. A PtPd alloy thin film and iridium thin film of around 8–10 nm was coated on polycarbonate substrate using sputtering technique to make layered polymer nanocomposite membrane. Moreover, SiO2 nanocomposites with 10 wt% and 15 wt % were prepared by solution casting method and the uniform dispersion of silica nanoparticles was obtained by sonication before casting the membrane. Further, the tests were carried at constant upstream pressure 30 psi and at constant temperature 35 °C using constant volume/variable pressure method. 相似文献
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Sung Mook Choi 《Electrochimica acta》2008,53(19):5804-5811
Platinum nanowires were prepared via a template-synthesis method by electrodeposition of platinum within pores of a track-etched polycarbonate (PCTE) membrane, followed by chemical etching to separate the Pt nanowires from the polymer. The structure and morphology of the Pt nanowires were characterized by X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), and transmission electron microscopy (TEM), revealing a polycrystalline phase with nanowire dimension up to 6 μm long and ca. 47 ± 9.8 nm of diameter. The unsupported Pt nanowires showed the better electrochemical mass activities over the methanol electro-oxidation than supported or unsupported Pt nanoparticles under the high Pt content-loaded conditions that is typically required for direct methanol fuel cells. This enhancement could be rationalized by its unique physicochemical and electrical properties arising from the inherent anisotropic one-dimensional (1D) nanostructure, such as charge transfer facilitation by reducing number of particle interfaces and more efficient use of Pt by alleviating fraction of embedded catalysts. 相似文献
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简述了目前聚碳酸酯挤出吹塑机头存在的常见缺陷,自行设计一套新型的螺旋式挤出吹塑机头,并用于挤出吹塑聚碳酸酯饮水桶。研究发现,该新型的螺旋式挤出吹塑机头具有清洁性好、无熔合线、无黑点、壁厚均匀以及生产损耗小的优点。 相似文献
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