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41.
Hydrogen evolution during formaldehyde oxidation in alkaline solution has been monitored by Differential Electrochemical Mass Spectrometry on Au(111) and polycrystalline gold. The current efficiency for hydrogen evolution increases with higher concentration and is in the same range on both, polycrystalline Au and Au(111) electrode. The onset potentials and half-wave potentials are higher on Au(111). Reaction orders for the faradaic current on the bare gold electrodes have been determined as 0.21 for higher and 0.76 for lower concentrations. Reaction orders for hydrogen evolution during formaldehyde oxidation are 1.4 times higher in each case. Tafel slopes in the range of 140-160 mV are found. This signifies that the first reaction step involving the formation of adsorbed hydrogen is largely determining the overall reaction rate. In the presence of thallium adlayers hydrogen evolution from formaldehyde oxidation is largely suppressed. On the thallium modified polycrystalline Au, formaldehyde oxidation is shifted for 100 mV to higher potentials where Tl is partially desorbed and hydroxide is coadsorbed on the modified surface. On thallium modified Au(111), a similar process takes place, but in the same potential region as the onset of formaldehyde oxidation on the bare surface and therefore the formaldehyde oxidation is only slightly shifted. Tafel slopes are decreased to 80 mV/dec in the presence of thallium. In the presence of adsorbed thallium, the first reaction step is in equilibrium, the coverage with adsorbed hydrogen is smaller and its recombination to H2 is largely suppressed. 相似文献
42.
43.
S. Vorotilo A.Yu. Potanin Yu.S. Pogozhev E.A. Levashov N.A. Kochetov D.Yu. Kovalev 《Ceramics International》2019,45(1):96-107
This study focuses on the investigation of the macrokinetic features of SHS (combustion synthesis) of elemental mixtures Mo–Hf–Si–B, in particular the mechanisms of structure and phase formation in the combustion front as well as the structure and properties of consolidated ceramics. Two routes for the fabrication of the composite SHS powder in system MoSi2–HfB2–MoB were used: (1) synthesis using Mo–Si–B and Hf–B mixtures followed by mixing of the combustion products and (2) synthesis using the four-component Mo–Hf–Si–B mixture. Dense ceramic samples with a homogeneous structure and low residual porosity (0.8–3.6%) were prepared by hot pressing of SHS powders. Although the particles size distribution and phase composition of SHS powders are similar for both synthesis routes, the structure and properties of both the composite SHS powders and hot-pressed ceramics differ considerably. Synthesis using the four-component Mo–Hf–Si–B mixture allows one to produce hierarchically ordered nanocomposite material with improved mechanical properties: hardness up to 17.6?GPa and fracture toughness up to 7.16?MPa?m1/2. 相似文献
44.
《Expert systems with applications》2014,41(14):6131-6137
Face recognition demonstrates the significant progress in the research field of biometric and computer vision. The fact is due to the current systems perform well under relatively control environments but tend to suffer when the present of variation in pose, illumination, and facial expression. In this work, a novel approach for face recognition called Symmetric Local Graph Structure (SLGS) is presented based on the Local Graph Structure (LGS). Each pixel is represented with a graph structure of its neighbours’ pixels. The histograms of the SLGS were used for recognition by using the nearest neighbour classifiers that include Euclidean distance, correlation coefficient and chi-square distance measures. AT&T and Yale face databases were used to be experimented with the proposed method. Extensive experiments on the face database clearly showed the superiority of the proposed approach over Local Binary Pattern (LBP) and LGS. The proposed SLGS is robust to variation in term of facial expressions, facial details, and illumination. Due to good performance of SLGS, it is expected that SLGS has a potential for application implementation in computer vision. 相似文献
45.
以易熔粘土为基,并引入难熔粘土和熔剂成分,合成了地砖坯料。经研究确定,只要遵循一定的条件,是可以用上述原料生产出优质产品的。指出了制品结构和相组成的形成特点。 相似文献
46.
《数据结构与算法》是理论与实践并重的计算机专业的核心课程,该课程理论和实践知识体系难度均较大,学生反映课程枯燥难学、兴趣匮乏。针对目前学生的学习过程中遇到的困难,结合应用型人才培养目标、学生及课程的特点,对教学方法进行多方面的探讨,提出案例教学、加强学生课堂参与度、重视理论与实践紧密结合、多种手段辅助教学、以赛促学、上机考试考核制度等教学方法。 相似文献
47.
袁静珍 《电脑与微电子技术》2014,(15):44-47
利用VC++开发平台,以《数据结构》课程的重要章节二叉树遍历算法为例,论述二叉树遍历算法演示软件的设计和关键技术并实现整个系统。系统使得学生加深算法的理解,取得良好的教学效果。 相似文献
48.
张红霞 《电脑与微电子技术》2014,(16):51-54
《数据结构》精品资源共享课作为服务于高校师生和社会学习者的平台之一,其建设内容主要由基本资源、拓展资源、师生互动组成。在《数据结构》精品资源共享课建设中,明确建设目标,着重进行课程体系及课程资源建设。通过精心组织课程资源,优化师资队伍以及制定科学的课程管理办法等措施,实现资源共享。 相似文献
49.
修学强 《自动化与仪器仪表》2014,(8):111-112
根据教学实验需要,创新设计了一种双色染料搅拌机的主体结构,为保证设备的有效使用,将其中的主要支承部件利用Solidworks进行了三维造型设计,并运用SimulationXpress分析向导对其应力状态、安全系数进行仿真优化,最后通过Siemens S7-200 PLC对其整体结构进行控制,能够完全的满足需要.本装置有控制过程简单方便、结构新颖、占用空间小等优点,具有良好的推广与应用价值. 相似文献
50.
自行设计了一台单填料函滑动管板式换热器代替进口设备,运转良好。本文着重介绍该设备密封结构的设计。 相似文献