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61.
The carburization of NiCr 32 20 and NiCrSi 60 16 has been studied in CH4-H2 mixtures in the temperature range 900–1100°C. The methods included thermogravimetric measurements and studies on reacted specimens by X-ray diffraction, metallographic, and chemical analysis. Upon carburization internal carbides M7C3 and M23C6 are formed (M=mainly Cr); the rate of carburization is determined by carbon diffusion in the Fe-Ni matrix with carbide precipitations. The effect of the alloying elements Ni and Si on the carburization resistance of austenitic alloys is explained. By the same methods the oxidation and carburization in CO-H2O-H2 mixtures have been studied. The important role of a stable chromium oxide layer for the carburization resistance was confirmed. Creep tests at 1000°C in a CO-H2O-H2 atmosphere where Cr2O3 is stable showed carburization occurring through cracks in the oxide layer. At high strain rates premature failure occurs by carburization, which is followed by internal oxidation and formation of cracks, voids, and holes. 相似文献
62.
Constant elongation rate tests (CERTs) were carried out to investigate the effects of environmental factors of dissolved oxygen and temperature on the stress corrosion cracking (SCC) susceptibility of 3.5NiCrMoV turbine steels. Tests were conducted in pure water of various dissolved oxygen concentrations at temperatures of 50 °C-200 °C in the range of strain rates from 5 × 10−8/s to 1 × 10−6/s. Dissolved oxygen significantly affected the SCC susceptibility of turbine steels in water. The SCC susceptibility of the turbine steels increases as the dissolved oxygen concentration in water increases. The elongation of the turbine steels tested in aerated water at 150 °C at a strain rate of 1 × 10−7/s decreased to half of that of the steels tested in deaerated water in the same test condition. And the SCC susceptibility of the steels increased with decreasing strain rate, and with increasing temperature. The increase of the SCC susceptibility of the turbine steels in the higher dissolved oxygen environment is considered to be due to the higher content of dissolved oxygen enhancing the reduction reactions of oxygen on the metal surfaces (cathode) and accelerating the dissolution rate at the crack tips (anode) by galvanic attack of an aeration cell. 相似文献
63.
Spheroidization experiments were made on a medium- carbon AISI 4037 steel, using both intercritical and subcritical annealing
cycles. The results indicate that in the subcritical cycle the spheroidization occurred much more quickly than expected, so
that shorter times were sufficient to achieve high formability. On the other hand, the hardness dropped faster in the intercritical
cycle. Although more work needs to be done, these results suggest that using a subcritical spheroidization process instead
of an intercritical process could achieve considerable savings in time, energy, and cost. 相似文献
64.
304不锈钢精铸件点缺陷的形成与控制 总被引:1,自引:0,他引:1
针对典型304不锈钢精密铸件内出现的黑色点缺陷,对其表面形貌、成分进行了分析,并在此基础上总结了缺陷的形成机制,确定了相应的防止措施。研究结果表明,铸件内的点缺陷可以划分为两类:一类具有不规则截面,为脱蜡过程中剩余腊料的燃烧残留物;另一类为熔炼过程中,由于脱氧剂和除渣剂的去除不彻底而引入的夹杂。通过优化脱蜡和熔炼工艺,使得铸件内的点缺陷得到了很好的控制。 相似文献
65.
66.
G. X. Zhao M. Zheng X. H. Lv X. H. Dong H. L. Li 《Metals and Materials International》2005,11(2):135-140
The corrosion behavior of 13Cr martensitic stainless steel in a CO2 environment in a stimulated oilfield was studied with potentiodynamic polarization and the impedance spectra technique. The
results showed that the microstructure of the surface scale clearly changed with temperature. This decreased the sensitivity
of pitting corrosion and increased the tendency toward general (or uniform) corrosion. The capacitance, the charge transfer
resistance, and the polarization resistance of the corrosion product scale decrease with increasing temperature from 90 to
120 °C, and thus the corrosion is a thermal activation controlled process. Charge transfer through the scale is difficult
and the corrosion is controlled by a diffusion process at a temperature of 150 °C. Resistance charge transfer through the
corrosion product layer is higher than that in the passive film. 相似文献
67.
采用恒载荷试验方法及慢应变速率试验(SSRT)方法研究了渗铝304奥氏体不锈钢在沸腾42%MgCl2溶液中的应力腐蚀破裂(SCC)性能,分析了渗铝不锈钢SCC机理,讨论了不同试验方法对渗铝不锈钢SCC敏感性评价的影响.试验表明:渗铝处理可明显提高304钢抗SCC性能,其机理为渗铝层的环境遮断作用及对基体的电化学保护作用.两种方法在评价各种渗铝钢材料SCC性能方面有统一性:恒载荷试验中SCC敏感性指标σth高的材料,SSRT中SCC敏感性指标δi也相对较高.但两种方法中渗铝试样的断口形态表现出差异:恒载荷试验为穿晶型SCC断口,而SSRT无SCC断口特征,为韧性断口。 相似文献
68.
Austenitic Mn-Al alloys (20–32 W/O Mn, 7–10 Al, 2–3 Si, 1C) were found to have satisfactory oxidation resistance up to 950°C under isothermal conditions in air. Surface enrichment of aluminum is a necessary condition for obtaining an almost pure alumina scale for uses at higher temperatures. Four different Mn-steels were Al-coated by the Capuano electroplating process. In all the steels there was an increase in the hot-oxidation resistance. The best results were obtained with steels containing both Al and Si, and this for temperatures up to 1100°C. No spalling was noticed during rapid cooling of the test pieces. Silicon was found to act as a diffusion barrier to outward iron diffusion. It appears that there is formation of a pure, thin film of alumina from the matrix which interacts with the aluminum diffusing from the superimposed, coating for the formation of good bonds. 相似文献
69.
70.