异形柱框架结构设计方法分析与参数控制

近年来,异形柱框架结构(框轻结构体系),因其能较好地满足建筑使用上和结构性能上的要求,而逐步得到了推广应用,并被列为建设部首批住宅建设新技术推荐目录。但异形柱框架结构设计目前还没有可依据使用的国家标准和行业标准。本文根据对江苏省地方标准《钢筋混凝土异形柱框架结构技术规程》(DB32/512-2002)的理解,结合笔者设计实践经验,提出个人看法,供同行参考。     

Some aspects of the electrochemistry of the flotation of pyrrhotite

The iron sulfide mineral, pyrrhotite (Fe_(1–x)S), has long been known to be more difficult to recover by flotation from alkaline slurries than many other base metal sulfide minerals. This paper summarizes the results of an electrochemical study of the surface reactions that occur during the flotation of nickeliferous pyrrhotite in the recovery of nickel and the platinum group metals. Mixed potential measurements conducted with natural pyrrhotite electrodes in various stages of an operating flotation plant showed that the mineral potential is positive to the equilibrium potential of the xanthate/dixanthogen couple. Similar results were obtained during batch flotation experiments and in synthetic solutions in the laboratory. Cyclic voltammetric and potentiostatic current/time transient experiments were used to investigate the oxidation of pyrrhotite under various conditions. In addition, the reduction of oxygen, the reaction of copper ions and the oxidation of xanthate ions at the mineral surface were investigated. The formation of dixanthogen on pyrrhotite surfaces is thermodynamically favourable in plant flotation slurries. However the interaction with xanthate at pH values above 7 is inhibited by a surface species formed during the conditioning prior to xanthate addition. In acidic solutions copper ions react readily with pyrrhotite to form a species, possibly CuS that can be oxidized at potentials above 0.4 V. At pH 9 this species does not form and there is no electrochemical reaction between pyrrhotite and copper ions. The beneficial effects of copper ions to flotation performance appear to be related to an enhancement of the oxidation of xanthate.     

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油管柱作为油气生产中的重要工具，它的使用寿命一直是工程技术人员关注的焦点。文章从动力学中固液耦合振动的角度出发，研究了油管柱内流体不稳定流动引起的油管柱振动问题。考虑液动压力对油管柱纵向振动的影响，建立了油管柱纵向振动微分方程，并给出了这种情况下油管柱纵向振动的频率方程。通过大天池构造上一口高压气井的实例计算分析，指出井内流体不稳定流动时，油管柱会产生相当高的附加动载。这个动载是造成油管柱在生产过程中发生疲劳破坏的主要原因之一，在今后的油管柱设计中应考虑这一动载的影响     

Split and collectorless flotation to medium coking coal fines for multi-product zero waste concept

The medium coking coal fines of − 0.5 mm from Jharia coal field were taken for this investigation. The release analysis of the composite coal reveals that yield is very low at 10.0% ash, about 25% at 14% ash and 50% at 17% ash level. The low yield is caused by the presence of high ash finer fraction. The size-wise ash analysis of − 0.5 mm coal indicated that − 0.5 + 0.15 mm fraction contains less ash than − 0.15 mm fraction. Thus, the composite feed was split into − 0.5 + 0.15 mm and − 0.15 mm fractions and subjected to flotation separately. The low ash bearing fraction (− 0.5 + 0.15 mm) was subjected to two stages collectorless flotation to achieve the concentrate with 10% ash. The cleaner concentrate (18.9%) with 10% ash was recovered which has an application in metallurgical industries. The concentrate of 30.2% yield with 12.5% ash could be achieved in one stage collectorless flotation which is suitable for use in coke making as sweetener. As the − 0.15 mm fraction contains relatively high ash, collector aided flotation using sodium silicate was performed to get a concentrate of 23.6% yield with about 17% ash. The blending of this product with cleaner tail obtained from − 0.5 + 0.15 mm produces about 35.0% yield with 17% ash and that can be utilized for coke making. The reject from the two fractions can be used for conventional thermal power plant or cement industries using a 23.5% ash after one stage collector aided flotation and the final tailings produced content ash of 61.6% can be used for fluidization combustion bed (FBC). This eventually leads to complete utilization of coal.     

应用硫酸铵提高乌拉嗄金矿石浮选回收率试验研究

经试验发现应用一种化学肥料硫酸铵可以显著提高乌拉嘎金矿石的浮选回收率。闭路试验尾矿工艺矿物学鉴定证明，以硫酸铵作为调整剂的浮选过程中，微细粒单体金和金与石英边生体被有效回收。     

圆形离心浮选机的研究与应用

圆形离心浮选机是由自吸式气泡发生器和圆柱—圆锥形分选槽体组成的浮选设备 ,利用矿浆射流形成的离心力场强化了重力场中的气泡碰撞矿化和泡沫析出过程。工业试验结果表明 :圆形离心浮选机对煤泥特别是细煤泥的浮选效果好 ,具有浮选速度快 ,分选选择性好 ,单位容积处理能力大等优点 ,是实现微细矿物分选的有效设备     

转向柱管承载能力的试验研究

在分析转向柱管花键部位应力集中情况的基础上,通过对某厂生产的转向柱管扭转破坏的试验研究,得到如下结论:①转向柱管的承载能力与其外花键齿与方向盘中心内花键齿之间的非接触区长度有关,以花键端部过渡圆弧的直径大小为宜;②安装方向盘总成时所施加在安装螺母上的拧紧力矩在70N.m左右时,转向柱管的承载能力最大。     

Improvement of oxygen mass transfer estimation from oxygen concentration measurements in bubble column reactors

An original procedure has been established for estimating the overall volumetric mass transfer coefficient using the oxygen concentration curves resulting from the usual gassing-in and gassing-out method. This procedure was applied to experimental data obtained in a small scale bubble column using both tap water and a coalescence-inhibiting liquid mixture that represents the coalescence behavior of biological media. It is based on the analysis of the characteristics times of the system, including those of the hydrodynamics of the two phases, the sensor dynamics and the system inertia when the gas composition is modified. A numerical procedure was developed to estimate the characteristic time of the system inertia t_i, using the assumption that this inertia is nearly independent of superficial gas velocity U_G. The calculations confirmed that the optimized t_i value was nearly independent of U_G and of the coalescence behavior of the liquid phase. Additionally, the resulting K_La_L values for tap water were closer to the correlation of Shah et al. [1982. Design parameters estimations for bubble column reactors. A.I.Ch.E. Journal 28, 353-379] than those of other conventional models. Finally, the original procedure was also reported to reduce significantly the square sum deviation between the predicted and the measured oxygen response curves.     

基于变轴力和定轴力试验对比的钢筋混凝土柱恢复力滞回特性研究

在讨论了框架柱在地震作用下轴力变化规律的基础上,通过由变轴力柱和定轴力柱的低周交变加载试验获得的恢复力滞回曲线对比,给出了用各个“轴力变化半周”的“等效滞回轴力”修正恢复力骨架曲线,和用“等效累积滞回轴力”随时间步长调整累积强度退化系数从而修正恢复力滞回曲线的再加载刚度的建议。该建议能更有效、更方便地反映轴力变化的整个历程对变轴力柱恢复特征的影响,有利于提高钢筋混凝土杆系结构非弹性地震反应分析的有效性。     

精馏塔静态仿真：Ⅰ.静动态混合数学模型的应用

本文为了克服精馏塔静态仿真不易收敛和初值难以给定等难题，巧妙地利用隐含数值积分方法的特点，将稳态与动态数学模型耦合起来，用以求解高难度的非理想精馏塔静态仿真问题。所得静动态混俣模型大大提高了精馏塔静态仿真的鲁棒性，对于高度非理想精馏塔的仿真尤为有效。通过对某丙烯腈萃取精馏塔的静态仿真，充分证明了这种混合模型化方法的可行性。