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11.
杨文江 《武汉大学学报(工学版)》1989,(4)
本文对碳钢蒸汽管道石墨化常用的诊断方法——金相分析法、化学分析法、机械性能试验法进行了探讨。并将密度法、超声波法应用于石墨化的诊断,实验证明密度法和超声波法用于石墨化的诊断是可取的。 相似文献
12.
《Ceramics International》2020,46(5):5733-5744
To improve the self-adaptability of MoS2 coating in different environments, the coatings were doped with functional C and Ti by unbalanced magnetron sputtering system. The clear superlattice structure with minimal modulation period was investigated by High Resolution Transmission Electron Microscope (HRTEM). The co-doped coatings have better mechanical properties due to the special structure and the formation of C–Mo, Ti–S and Ti–O bonds, and better lubrication performance in both high humidity and vacuum than those of the single-doped ones. The doped Ti not only facilitates the formation of the MoS2 (002) basal plane, but also improves the oxidation resistance of the composite film. The degree of friction-induced graphitization on the wear tracks and the quality of transfer films on the wear scars are key factors affecting the lubrication performance of the composite film. In the high-humidity environment, the reasonable doping elements can promote the formation the high-quality transfer film by interacting with H2O water molecules, which will benefit the lubrication of the coating better. Our findings deepen the understanding of MoS2 composite coating and provide a new solution for improving the self-adaptability of the coating. 相似文献
13.
炭素制品在石墨化过程中时常会出现导致大量裂纹废品的"Puffing"现象,严重影响了产品的质量,本文旨在探讨引起"Puffing"现象的因素、产生机理以及介绍几种在石墨制品生产过程中已经被广泛采用的抑制、减少该现象产生的有效措施,以提高石墨制品的质量及成品率指标。 相似文献
14.
优质阳极的生产技术探讨 总被引:4,自引:0,他引:4
从阳极生产装备和工艺两方面分析了影响预焙阳极质量的主要因素,提出了有利于提高阳极质量的一些想法,并建议减少或停止出口阳极的生产,把相关技术转向自用阳极,提高我国电解铝的生产技术水平。 相似文献
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The process of electrodepositing Fe-Cr2O3 composite coating on polyacrylonitrile(PAN)-based carbon fibers and its catalytic graphitization were studied.Carbon fibers with and without electrodeposited Fe-Cr2O3 composite coating were heat treated at different temperatures and the structural changes were characterized by XRD,Raman spectroscopy and SEM.The results indicate that Fe-Cr2O3 composite coating exhibits a significant catalytic effect on graphitization of carbon fibers at low temperatures.When the Fe-Cr2O3-coated carbon fibers were heat treated at 1 300°C,the interlayer spacing(d002) and ratio of relative peak area(AD/AG) reach 3.364-and 0.34,respectively.Whereas,the extent of graphitization of pristine carbon fibers is comparatively low even after heat treatment at 2 800°C and the values of d002 and AD/AG are 3.414 and 0.68,respectively.The extent of graphitization of carbon fibers increases not only with the increase of the catalyst gross but also the Cr2O3 content in Fe-Cr2O3 coating.The catalytic effect of Fe-Cr2O3 composite coating accords with the dissolution precipitation mechanism. 相似文献
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18.
典型碳纤维连接件微观结构分析 总被引:1,自引:0,他引:1
金属连接件连接较为受限,需要利用碳纤维材料与金属材料共同连接才可满足实际应用,而碳纤维的微观结构对其性能影响较大,针对上述问题对碳纤维的微观结构进行了研究.制备了PAN100、PAN200型碳纤维材料,并以其作为研究对象进行微观结构分析.结果表明,PAN100碳纤维表面部分区域的纤维束之间出现交联、粘结或磨损现象,而PAN200碳纤维相比PAN100碳纤维更为光滑,表面结构比较均匀,纤维较为细密,且无裂纹和孔洞.PAN200碳纤维的物理性能优于PAN100碳纤维,且PAN200结构相比PAN100碳纤维更适合用作碳纤维连接件. 相似文献
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20.
To investigate the effects of introducing the iron compound on the carbonization behavior polyacrylonitile (PAN)-based electrospun nanofibers were carbonized with or without iron(III) acetylacetonate (AAI) over the temperature range of 900–1500 °C in nitrogen atmosphere. The morphological characteristics of the carbon nanofibers were investigated using X-ray diffractometer (XRD), Raman spectroscopy, field emission scanning electron microscopy, and transmission electron microscopy. The electrical conductivity of the carbon nanofiber web was measured by four-point probe method. The iron catalyst had a profound effect on the crystal structure of the carbonized nanofiber. In the presence of AAI the nanofibers carbonized at 1300 °C developed graphite structure, which could be obtained at the temperature higher than 2000 °C in the absence of the catalyst. The in-plane size of the graphite crystals (La) was measured to be about 6.5 nm by Raman spectroscopy and the (0 0 2) spacing by XRD was 0.341 nm. 相似文献