Effects of Light, Oxygen, and pH on the Absorbance of 2,2-Diphenyl-1-picrylhydrazyl

ABSTRACT: The absorbance of 2,2-diphenyl-1-picrylhydrazyl (DPPH) at 517 nm in methanol and acetone decreased by 20 and 35% for 120 min at 25 °C under light, respectively; in the dark it did not change significantly for 150 min. Decomposition of DPPH under 21% oxygen after 90 min under light was significantly higher than that under 1% oxygen. Absorbance of DPPH in pH 4 buffer solution in methanol, and in pH 10 buffer solution in acetone, decreased by 55 and 80%, respectively, under light for 120 min. The evaluation of antioxidant activity by the changes of DPPH absorbance should be carefully interpreted since the absorbance of DPPH at 517 nm is decreased by light, oxygen, pH, and type of solvent in addition to the antioxidant.     

测量不确定度计算与实验方案的恰当选择

文章介绍了不确定度的定义及其一般计算公式，通过具体实例介绍了实验后不确定度的计算和实验前的误差估计。并对有多种可能的实验方案，利用误差估计的方法，选择出最佳的实验方案，使其不确定度最小。     

碾压混凝土坝施工进度与质量控制的新措施

碾压混凝土重力坝和拱坝由于连续施工的坝体混凝土体积大，施工期间需要采取较为严格的温度控制措施，而所采取的温控措施是否有效，目前尚没有一个能够用于实际施工过程的快速有效的评估方法和方式，不能根据已施工坝体内的实际情况来控制施工进度和质量。利用分布式光纤温度测量系统来快速地获得坝体混凝土内部的大量温度信息，进而实际标定温度仿真程序并通过标定过程模拟拟施工的连续碾压层，以检验其温控措施的有效性。通过坝体内部的温度、温度变化速率和梯度来达到实时控制坝体碾压上升速度、坝面和仓面养护、以及冷缝灌浆处理等目的。     

Speakers gaze at objects while preparing intentionally inaccurate labels for them.

When describing scenes, speakers gaze at objects while preparing their names (Z. M. Griffin & K. Bock, 2000). In this study, the authors investigated whether gazes to referents occurred in the absence of a correspondence between visual features and word meaning. Speakers gazed significantly longer at objects before intentionally labeling them inaccurately with the names of similar things (e.g., calling a horse a dog) than when labeling them accurately. This held for grammatical subjects and objects as well as agents and patients. Moreover, the time spent gazing at a referent before labeling it with a novel word or accurate name was similar and decreased as speakers gained experience using the novel word. These results suggest that visual attention in speaking may be directed toward referents in the absence of any association between their visual forms and the words used to talk about them. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Procedure for Measuring Low Concentrations of H2 and H2S Above a Water Surface

A simple measuring procedure for low concentrations of H₂ and H₂S (at the level of ppm fractions) above the surface of water by using sensitive gas analyzers is suggested. The procedure is easily accomplished in conditions outside the laboratory (under field conditions).     

单线复用技术在水文巡测设备中的应用

为了解决水文巡测设备中数据传输的可靠性，电力载波通讯中的单频阻波器技术被应用到巡测设备上。此法简单易行，稳定可靠。     

汽车摩擦片厚度测量装置驱动电路的研究

本文通过对摩擦片厚度在线测量装置系统构成的全面分析，对其驱动电路子系统进行了理论探索和技术研究，完成了相应的电路设计、误差分析及器件选择等工作，并进行了具体的实验验证，证明该驱动电路具有良好的性能，可圆满实现摩擦片厚度在线检测和实时分析的工作任务。     

十三陵蓄能电站上水库自动监测系统的设计及运行

由于十三陵蓄能电站上水库地处蟒山之巅，所在山体地质条件复杂。施工期埋设了大量的监测仪器，原有人工监测系统效率低、资料分析的同步性差。2002年5月，对其进行了自动化改造，现已有一套符合其特点的自动化监测系统。十三陵上水库水工建筑自动监测系统已正常运行了三年，同时也存在着问题，有待于进一步的探讨和改进。     

光测遥测数据联合计算速度的方法

提出了利用遥测的过载、俯仰角信息和光测的坐标联合计算弹道关机段速度的方法，从遥测结果的系统误差、随机误差和数值积分的截断误差三万面对剩余误差的影响进行了精度分析，并给出了速度精度的算法。