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71.
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均匀设计法分析制备过程对钴钼硫化物催化剂机械强度的影响 总被引:1,自引:1,他引:0
建立了CoMoP/Al2O3加氢精制催化剂机械强度及其可靠性在制备过程中的数学模型,采用均匀设计考察了浸渍、干燥、煅烧、硫化4个制备过程中,浸渍时间、干燥温度、干燥时间、煅烧温度、煅烧时间、硫化温度和硫化升温速率7个实验因子对催化剂强度均值、Weibull模量的影响,同时考察了这些因素对颗粒密度的影响。方差分析表明所有模型都是充足的。实验结果表明,硫化过程是影响催化剂强度均值的主要过程。在实验范围内提高硫化温度、降低硫化时的升温速率有利于提高催化剂的强度。影响催化剂Weibull模量的因素主要为各个制备过程的交互效应。要提高催化剂强度的可靠性就必须全面考虑催化剂制备的各个过程,特别是各个制备过程的交互效应。 相似文献
74.
主要研究了Cr对低碳Si-Mn系TRIP钢组织与力学性能的影响。首先利用Formastor-F型膨胀仪测定了含Cr和不含Cr两种低碳钢的连续冷却转变(CCT)曲线,分析指出了Cr对连续退火工艺的潜在影响;然后采用Gleeble-3800热/力模拟试验机对两种钢的薄板试样进行了连续退火模拟实验,并通过拉伸试验测定了力学性能;最后采用金相、扫描电镜、X-射线衍射分析等技术考察分析了两种钢的显微组织。结果表明:含Cr的TRIP钢的组织比较细小,铁素体晶粒近似等轴分布;两种TRIP钢的残余奥氏体含量相近,但含Cr钢的残余奥氏体中的含碳量较高。分析认为这是由于含Cr钢在热轧阶段较易生成细小的组织,而在热处理阶段则抑制贝氏体的生成,最终获得稳定的残余奥氏体。 相似文献
75.
76.
Preparation and Properties of Rare Earth Modified Carbon Black/Natural Rubber Composites 总被引:2,自引:2,他引:0
Lin Yaling Xiao Kongqing Zhang Anqiang Wang Lianshi 《中国稀土学报(英文版)》2005,23(6):720-720
The oxides Eu, Ho, Er and Dy were used to prepare the hydroxides of rare earth modified carbon black. Then natural rubber latex (NRL) was added into the reactor. The system reacted at 85 ℃ with stirring for 1 h to prepare powdered HAF-Ln(OH)3/NR composites. The effects of the kind and content of Ln on the particle size distribution of P [ NR/HAF-Ln (OH)3 ] and mechanical properties of its vulcanizate were studied respectively. It is found that rare earth can help to get the powder of the composite, the product particle with a diameter less than 0.9mm will be get when the composites containing the compound of Ho, Er and Dy with dosage of 1.0, 1.0, O. 5 percent, respectively. The adding of Ln can improve the tensile strength and tear strength of the vulcanizate effectively, what's more, Er and Dy can decrease the permanent set of vulcanizate significantly. The SEM studies shows that P[ NR/HAF-Dy (OH)3 ] vulcanizate shows superior mechanical properties that depend primarily on the absence of free carbon black, the fine dispersion of carbon black in the rubber matrix and better polymer-filler interaction. 相似文献
77.
The effects of moisture, temperature, and ultraviolet (UV) light on performance of natural‐fiber–plastic composites (NFPC) were assessed. We conducted short‐term tests in the laboratory and long‐term tests under natural exposure and measured changes in mechanical properties and color in samples of the composite. Chemical changes of the composite's materials were measured by X‐ray photoelectron spectroscopy to elucidate the mechanisms of chemical transformations on the material surface. Relative humidity highly affected the modulus of rupture (MOR) and the modulus of elasticity (MOE), and had a greater effect than temperature and UV exposure on performance of the composite. The lightness of the composite was increased by the UV effect in the short‐ and the long‐term tests. The X‐ray photoelectron spectroscopy (XPS) analysis suggested that the composite was protected by the UV absorber. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 99: 2570–2577, 2006 相似文献
78.
Javier Roca-Pardiñas Carmen Cadarso-Suárez María J. Lado 《Computational statistics & data analysis》2008,52(4):1958-1970
In many applications, the joint effect of two continuous covariates on the target binary response may vary across groups defined by levels of a given factor. A testing procedure that would enable this type of surface-by-factor interactions to be detected has been designed. To accomplish this goal, a logistic generalized additive model (GAM) with bivariate continuous interactions varying across groups defined by levels of a factor is considered. A local scoring algorithm based on local linear kernel smoothers was implemented to estimate the proposed logistic GAM. Bootstrap resampling techniques were used for the purpose of testing for factor-by-surface interactions. Given the high computational cost involved, binning techniques were used to speed up computation in the estimation and testing processes. The adequacy of the bootstrap-based test was assessed by means of a simulation study. If a factor-by-surface interaction is detected in the model, it is then established that the use of the odds-ratio curves is very useful in obtaining a direct interpretation of the fitted model. The benefits of using this methodology when analyzing real data are illustrated by applying the technique to the outputs produced by a computerized system dedicated to the early detection of breast cancer. 相似文献
79.
Prasad S Thenkabail Eden A Enclona Mark S Ashton Christopher Legg 《Remote sensing of environment》2004,90(1):23-43
The goal of this research was to compare narrowband hyperspectral Hyperion data with broadband hyperspatial IKONOS data and advanced multispectral Advanced Land Imager (ALI) and Landsat-7 Enhanced Thematic Mapper Plus (ETM+) data through modeling and classifying complex rainforest vegetation. For this purpose, Hyperion, ALI, IKONOS, and ETM+ data were acquired for southern Cameroon, a region considered to be a representative area for tropical moist evergreen and semi-deciduous forests. Field data, collected in near-real time to coincide with satellite sensor overpass, were used to (1) quantify and model the biomass of tree, shrub, and weed species; and (2) characterize forest land use/land cover (LULC) classes.The study established that even the most advanced broadband sensors (i.e., ETM+, IKONOS, and ALI) had serious limitations in modeling biomass and in classifying forest LULC classes. The broadband models explained only 13-60% of the variability in biomass across primary forests, secondary forests, and fallows. The overall accuracies were between 42% and 51% for classifying nine complex rainforest LULC classes using the broadband data of these sensors. Within individual vegetation types (e.g., primary or secondary forest), the overall accuracies increased slightly, but followed a similar trend. Among the broadband sensors, ALI sensor performed better than the IKONOS and ETM+ sensors.When compared to the three broadband sensors, Hyperion narrowband data produced (1) models that explained 36-83% more of the variability in rainforest biomass, and (2) LULC classifications with 45-52% higher overall accuracies. Twenty-three Hyperion narrowbands that were most sensitive in modeling forest biomass and in classifying forest LULC classes were identified and discussed. 相似文献
80.
介绍了用自然澄清法降低、回收旋涡炉渣中的铜的方法。该方法工艺简单。操作方便,不仅降低冶炼成本,同时提高了经济效益。 相似文献