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51.
讨论了直流法在线测量钯氢化物电极电阻时的电化学效应,计算了电解液的共导、测量电流与电解电流引起的浓差电池效应以及电极作为集流体引起的电阻贡献。结果表明:当电极具有高的长度与半径比值、粗糙的表面、高的溶液电导以及大的电解电流时容易引起显著的附加电阻。 相似文献
52.
磷矿中七种金属元素的光谱法测定 总被引:2,自引:0,他引:2
研究了磷矿样品中7种金属元素锰、钴、镍,锌、铬、钼及铋的分析方法,选择了灵敏度高干扰少的谱线,绘制出工作曲线,对样品进行了科学处理,不必进行化学分离即可对七种元素同时测定,经合成样分析、回收实验及样品测定,证明此方法精确可靠,其回收率在98%-102%之间。 相似文献
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55.
P.-Y. CHANG J.-M. YANG H. SEO H. T. HAHN 《Fatigue & Fracture of Engineering Materials & Structures》2007,30(12):1158-1171
The off‐axis fatigue cracking behaviour of notched fibre metal laminates under constant amplitude loading conditions was investigated experimentally and numerically. It was found that the off‐axis fatigue crack initiation life decreased as the off‐axis angles increased. This indicated that the off‐axis laminates raised the applied stress level in the aluminium (Al) layer and subsequently resulted in earlier cracking in the Al layer. The off‐axis fatigue crack initiation lives of notched fibre metal laminates were predicted using lamination theory and an energy‐based critical plane fatigue damage analysis from the literature. After a crack initiated in the Al layer, it was observed that the crack path angles of the off‐axis specimens were neither perpendicular to the fibre nor to the loading direction. A finite‐element model was established for predicting the crack path angles. 相似文献
56.
Crack closure in fibre metal laminates 总被引:1,自引:0,他引:1
H.M. PLOKKER R.C. ALDERLIESTEN R. BENEDICTUS 《Fatigue & Fracture of Engineering Materials & Structures》2007,30(7):608-620
GLARE is a fibre metal laminate (FML) built up of alternating layers of S2-glass/FM94 prepreg and aluminium 2024-T3. The excellent fatigue behaviour of GLARE can be described with a recently published analytical prediction model. This model is based on linear elastic fracture mechanics and the assumption that a similar stress state in the aluminium layers of GLARE and monolithic aluminium result in the same crack growth behaviour. It therefore describes the crack growth with an effective stress intensity factor (SIF) range at the crack tip in the aluminium layers, including the effect of internal residual stress as result of curing and the stiffness differences between the individual layers. In that model, an empirical relation is used to calculate the effective SIF range, which had been determined without sufficiently investigating the effect of crack closure. This paper presents the research performed on crack closure in GLARE. It is assumed that crack closure in FMLs is determined by the actual stress cycles in the metal layers and that it can be described with the available relations for monolithic aluminium published in the literature. Fatigue crack growth experiments have been performed on GLARE specimens in which crack growth rates and crack opening stresses have been recorded. The prediction model incorporating the crack closure relation for aluminium 2024-T3 obtained from the literature has been validated with the test results. It is concluded that crack growth in GLARE can be correlated with the effective SIF range at the crack tip in the aluminium layers, if it is determined with the crack closure relation for aluminium 2024-T3 based on actual stresses in the aluminium layers. 相似文献
57.
Effect of Rare Earth Element Cerium on Mechanical Properties and Morphology of TiN Coating Prepared by Arc Ion Plating 总被引:7,自引:0,他引:7
TiN coatings were deposited on polished substrates of W18Cr4V high speed steel by means of vacuum arc ion plating. The effect of cerium on adhesion between TiN coating and substrate was studied. The microstructures and composition of TiN coatings were also investigated by means of scanning electron microscope (SEM), Auger electron spectroscopy (AES), and X-ray diffraction (XRD) technique. It was found that cerium is an effective modifying agent and the addition of suitable amount of cerium to TiN coatings can produce relatively excellent properties such as micro-hardness, wear resistance, oxidation resistance and porosity. The experimental results show that the added cerium in TiN coatings makesa contribution to form the preferred direction along with a (111 ) or (222) close packed face, which may be one of the reasons that improves some properties mentioned above. 相似文献
58.
Silver and copper nanowires have been synthesized using a scalable method of AC electrodeposition into porous aluminum oxide templates, which produces gram quantities of metal nanowires ca. 25 nm in diameter and up to 5 and 10 μm in length for Ag and Cu, respectively. The nanowires have been used to prepare polystyrene nanocomposites by solution processing. Electrical resistivity measurements performed on polymer nanocomposites containing different volume fractions of metal indicate that low percolation thresholds of nanowires are attained between compositions of 0.25 and 0.75 vol %. 相似文献
59.
A. Andreev L. Prahov M. Gabrovska A. Eliyas V. Ivanova 《Applied catalysis. B, Environmental》1996,8(4):365-373
The catalytic activity of a wide range of transition metal oxides in oxidation of sulphide ions by air in aqueous medium was studied. Some specific features of the reaction mechanism on some of the studied oxides were considered. The transition metal oxides are promising catalysts for practical application. Some of these oxides will allow the preparation of catalysts possessing activity comparable to that of the cobalt phthalocyanine based catalysts, popular in industrial practice. 相似文献
60.
添加剂对尖晶石型锰酸锂性质表征的影响 总被引:1,自引:0,他引:1
以LiOH·H_20和MnO_2为原料,分别掺入H_2BO_3、Al_2O_3、SiO_2和P_2O_5等添加剂,用固相分段法制备尖晶石型锰酸锂。结果表明,SiO_2和P_2O_5可以有效地改善LiMn_2O_4的电化学性能,H_3BO_3对锰酸锂的电化学性能影响不大,而Al_2O_3破坏了LiMn_2O_4的电化学性能。面扫描结果显示,Si或P元素各自都均匀地分散于LiMn_2O_4的物相中。从元素电负性和原子半径的角度分析了B、Si、P和Al元素对尖晶石型LiMn_2O_4结构和性能的影响。 相似文献