Microwave permeability of single cobalt nanotube studied by micromagnetics simulations and generalized Snoek’s law

Microwave permeability spectra of single Co nanotube under equilibrium state have been studied by micromagnetics simulation.More than four obvious resonance peaks have been found(11.72,24.20,33.18 and 39.55 GHz).Such large resonance frequency cannot be found in other traditional magnetic materials.The configurations of magnetic moments along the nanotube have been simulated.The results show that the top end of nanotube has a"flow-out"pattern of magnetic moments configuration.The bottom end has a"flow-in"pattern of magnetic moments configuration.The magnetic moments within the main body of nanotube are aligned perfectly along the length of nanotube.The magnitude of natural resonance peak is strongly related to the volume fraction of a zone,which has the same orientation of magnetic moments.Large microwave permeability values have been found for single nanotube.The generalized Snoek’s law has been used to validate the micromagnetics simulations in this paper.     

微波渗硼机理研究

利用渗硼介质吸收微波的特性成功地实现了钢铁表面渗硼层的制备，并与常规渗硼进行了比较，结果表明：微波场下渗层生长的硼原子来源于介质分解的硼原子及气态硼化物。渗层生长与常规渗层生长一样表现〈002〉晶向取向生长特征，微波渗硼的渗层生长速率比常规快，除温度效应外，还与微波提高硼原子活性加速硼原子在渗层的扩散有关。     

The Metal-Dielectric Resonator Method of Measuring the Parameters of Radio Materials

The use of symmetrical H- and E-modes and asymmetrical E-modes in a longitudinally anisotropic dielectric cylinder with metal mirrors at the ends to measure its permittivity and dielectric loss tangent is considered. It is shown that the method has wider possibilities compared with the IEC-61338 recommendations. The results of a measurement of the dielectric parameters of a number of materials in the 2–78 GHz frequency band, including the permittivity tensor of sapphire, are presented. __________ Translated from Izmeritel'naya Tekhnika, No. 9, pp. 65–70, September, 2005.     

快速测定化学需氧量的方法

利用分光光度法、微波密封消解法测定水样中的化学需氧量，并把测定的精密度、准确度与国标回流法相比较，结果证明：分光光度法、微波消解法是测定化学需氧量的快捷方法，具有省时、省试剂、工作效率高的特点。     

微波除冰方法研究

为解决我国北方寒冷地区冬季道路积冰不易清除的问题,提出了应用微波加热清除道路积冰的设想.通过实验证实了冰不易吸收微波,而路面材料能够吸收大量微波.因此,微波能够透过冰层加热路面,使贴近路面的冰层融化,消除冰层与路面之间的结合力,然后就可以很容易地利用除冰机械对其清除,这样,就消除了纯机械除冰的弊病.     

A comparison of 18 winter seasons of in situ and passive microwave-derived snow water equivalent estimates in Western Canada

The Meteorological Service of Canada (MSC) has developed an operational snow water equivalent (SWE) retrieval algorithm suite for western Canada that can be applied to both Scanning Multichannel Microwave Radiometer (SMMR) and Special Sensor Microwave/Imager (SSM/I) data. Separate algorithms derive SWE for open environments, deciduous, coniferous, and sparse forest cover. A final SWE value represents the area-weighted average based on the proportional land cover within each pixel. The combined SSM/I and SMMR time series of dual polarized, multichannel, spaceborne passive microwave brightness temperatures extends back to 1978, providing a lengthy time series for algorithm assessment. In this study, 5-day average (pentad) passive microwave-derived SWE imagery for 18 winter seasons (December, January, February 1978/79 through 1995/96) was compared to SWE estimates taken from a distributed network of surface measurements throughout western Canada.Results indicated both vegetative and snowpack controls on the performance of MSC algorithms. In regions of open and low-density forest cover, the in situ and passive microwave SWE data exhibited both strong agreement and similar levels of interannual variability. In locations where winter season SWE typically exceeded 75 mm, and/or dense vegetative cover was present, dataset agreement weakened appreciably, with little interannual variability in the passive microwave SWE retrievals. These results have important implications for extending the SWE monitoring capability of the MSC algorithm suite to northern regions such as the Mackenzie River basin.     

土壤样品的微波消解及其痕量铀的分析

对3个土壤样和2个放射性河床沉积物的国家标准物质进行了微波消解，又采用TOPO萃取和液体荧光法分析了样品中的铀含量，并将分析结果与国家标准方法GB11220．2-89的分析结果进行了比较。结果表明，微波消解法与国家标准方法一样，均不能实现土壤的全部消解，但与国家标准方法相比较，微波消解速度快，所需试剂量少，且易于实现定量控制，铀回收率高，分析精度高。对不溶物进行X射线能谱分析发现，其主要组成为铝、钛及过渡金属的氟化物或氧化物。同位素质谱分析表明，国家标准物质GBW08304中的^234U，^235U均比天然丰度低，另一个国家标准物质GBW08304a中铀的同位素分布与天然组成基本一致。     

在线测量煤粉中含碳量的方法研究

首先介绍了在线煤质分析的现状及其紧迫性,然后分析了国内外常用的几种在线测量煤中含碳量的方法,最后提出微波测量技术可以用于在线测量煤粉中的含碳量.通过电磁场与电磁波理论,论证了采用微波技术测量煤粉中含碳量的原理.     

用活化焙烧-硫酸浸出-溶剂萃取法从钴渣中提取硫酸钴的试验研究

研发了一种从钴渣中提取硫酸钴的新工艺,即钴渣活化焙烧-硫酸浸出-溶剂萃取工艺.在活化焙烧温度900 ℃,活化剂添加量2∶1(添加剂与钴渣的质量比),焙烧时间1 h;硫酸浸出液固体积质量比5∶1,硫酸浓度20%,浸出温度90 ℃,浸出时间1.5 h条件下,钴浸出率为98.8%.然后采用P204萃取除杂-P507萃取分离钴、镍工艺得到纯净的高浓度钴溶液,蒸发结晶后得到质量符合HG3-914-78化学纯度要求的硫酸钴.     

铁尾矿为原料微波法制备介孔分子筛

以鞍山铁尾矿为硅源,CTAB为模板剂,采用微波辐照法合成出全硅介孔分子筛MCM-41。用N2低温吸附、FT-IR、XRD和TEM等表征手段考察了其比表面积、孔径分布、晶体形貌等特性。结果表明:微波辐射法合成的MCM-41分子筛诱导期极短,晶化速度很快,具有典型的按六方对称性排列的孔道结构,FT-IR证明了分子筛具有硅氧四面体骨架。