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11.
Fei Li Xin-Gang Wang Xiao Huang Ji-Xuan Liu Weichao Bao Guo-Jun Zhang Hongzhi Wang 《Journal of the European Ceramic Society》2018,38(14):4806-4813
We present a straightforward method via sol-gel process using polyethylene glycol (PEG) as phase separation inducer to prepare zirconium carbide/silicon carbide (ZrC/SiC) porous monoliths. Organic/inorganic hybrid gels are prepared using zirconium oxychloride, furfuryl alcohol, and tetraethyl orthosilicate as major starting materials. In the presence of PEG, crack-free hybrid monoliths are obtained by drying the wet gels under ambient pressure, whereas in the absence of PEG, the wet gels break into pieces as expected. PEG plays a key role in maintaining the macroscopic shape of the monoliths. After ceramization at 1300–1500?°C, ZrC/SiC porous monoliths are obtained. SEM and mercury intrusion porosimetry data show that PEG also has strong influence on the microstructures of the monoliths. The compressive strengths of the ceramic monoliths are in the range of 0.3 to 0.7?MPa. And their compressive behavior starts to differ due to the changes in their microstructures, especially the pore structure. 相似文献
12.
I. Shepa E. Mudra M. Vojtko P. Tatarko V. Girman O. Milkovic T. Sopcak V. Medvecka J. Dusza 《Ceramics International》2018,44(15):17925-17934
The aim of the present contribution is to study the influence of the post-spinning heat - treatment of single TiO2/PVP precursor fibers on the properties and morphology of the final titanium-based microfibers. The post-spinning treatment conditions were: calcination in air at 450–600?°C and pyrolysis in argon at 1000–1700?°C. Calcination resulted in a production of anatase-rich and pure rutile fibers. The use of an alternative sintering method, the low-temperature plasma treatment, led to the crystallization of the composite Magnéli phases/polymer fibers. As a result of the same one precursor, pyrolysis at 1000?°C, the Carbon/TiO2 composite fibers were obtained. Rising the treatment temperature in inert atmosphere led to the formation of the titanium carbide fibers. The formation process and all the obtained products were characterized by differential scanning calorimetry accompanied with thermogravimetric analysis (DSC/TGA), scanning and transmission electron microscopy (SEM, TEM), X-ray diffraction (XRD), and image analysis techniques. 相似文献
13.
《Journal of the European Ceramic Society》2020,40(13):4396-4402
The response of nanocrystalline silicon carbide (nc-SiC) to nanoindentation is investigated using molecular dynamics (MD) simulation. It is found that the hardness of the nc-SiC decreases with decreasing grain size, showing an inverse Hall-Petch relationship. The behavior is primarily attributed to the reduced number of intact covalent bonds with grain refinement. Dislocation nucleation and growth in nc-SiC are strongly suppressed by the grain boundaries (GBs). In addition to the dislocation region in the grains, the indentation-induced amorphization of nanograins proceeds preferentially from the GBs, leading to grain shrinkage until the grains are fully amorphized. The results provide an improved understanding of the mechanical properties in nc-SiC and other nanostructured covalent materials. 相似文献
14.
Hiromichi Ichinose Masanori Taira Sachiko Furuta Hiroaki Katsuki 《Journal of the American Ceramic Society》2003,86(9):1605-1608
Niobium- or vanadium-doped anatase sols were prepared by hydrothermal treatment of 0.1 mol/dm3 peroxotitanium complex aqueous solutions dissolving 0–10 mol% niobium or vanadium at 100°C for 8 h. Niobium-doping caused the increase of lattice constants of anatase and the shape change of anatase crystal from spindle-like to cubic-like structure, but no change of the optical absorbance. Vanadium-doping caused the decrease of lattice constant of c -axis, the miniaturization of anatase crystal and the increase of optical absorbance at the wavelength from 350–700 nm. 相似文献
15.
P. G. Muzykov Y. I. Khlebnikov S. V. Regula Y. Gao T. S. Sudarshan 《Journal of Electronic Materials》2003,32(6):505-510
To establish fast, nondestructive, and inexpensive methods for resistivity measurements of SiC wafers, different resistivity-measurement
techniques were tested for characterization of semi-insulating SiC wafers, namely, the four-point probe method with removable
graphite contacts, the van der Pauw method with annealed metal and diffused contacts, the current-voltage (I-V) technique,
and the contactless resistivity-measurement method. Comparison of different techniques is presented. The resistivity values
of the semi-insulating SiC wafer measured using different techniques agree fairly well. As a result, application of removable
graphite contacts is proposed for fast and nondestructive resistivity measurement of SiC wafers using the four-point probe
method. High-temperature van der Pauw and room-temperature Hall characterization for the tested semi-insulating SiC wafer
was also obtained and reported in this work. 相似文献
16.
采用浸渍法制备了Nb2O5/α-A l2O3催化剂(简称催化剂)并用于环氧乙烷水合制乙二醇的反应,通过控制α-A l2O3载体中致孔剂的含量来调变载体的孔径、孔分布及比表面积;采用吡啶吸附红外光谱、氨程序升温脱附法研究了载体的比表面积及孔径对催化剂酸性及反应性能的影响。实验结果表明,产物的选择性受扩散因素及催化剂酸性的影响,而催化剂的酸量、酸密度可以通过载体的孔径及比表面积的变化加以调控。比表面积较小及孔径较大的载体对催化剂催化环氧乙烷水合制乙二醇的反应较为有利。当载体的比表面积小于0.80m2/g、孔径为4.00~8.00μm时,在反应温度160℃、反应压力1.5M Pa、n(H2O)∶n(EO)=22、液态空速25h-1的条件下,环氧乙烷的转化率大于99.8%,乙二醇的选择性超过89.9%。 相似文献
17.
A critical review of the current status of tungsten resources, of state-of-the-art processing technology and of product development
in India vis-a-vis the world scenario is presented. An attempt has been made to identify technology gap areas requiring attention. 相似文献
18.
SiC(w)/TZP+mullite陶瓷复合材料界面和组成设计与力学性能 总被引:2,自引:1,他引:1
本文从理论上分析了SiC(w)TZP+mullite(p)复合材料界面残余热应力及其在基质内的分布规律。提出在SiC(w)表面涂复Al2O3和在PZT中加入mullite(p)联合作用来降低晶须/基质界面残余热应力的界面设计方案,导出SiC(w)和mullite(p)协同补强PZT的匹配条件。制备了SiC(w)/TZP+mullite(p)复合材料并了SiC(w)表面涂层Al2O3厚度和SiC(w 相似文献
19.
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