深冲汽车簿钢板织构的表述方法

利用晶体学性质,将深冲汽车薄板的两种主要特征织构表述于反极图之中,再利用织构定量技术便能简捷地分析深冲钢板的织构与深冲性能的关系。经验证,此法与ODF定量分析所得的结果一致。     

Effect of oxygen precipitates in solar grade silicon on minority carrier lifetime and efficiency of solar cells

The effect of oxygen precipitates on minority carrier lifetime and performance of solar cell was studied by means of Fourier Transform Infrared Spectroscopy (FTIR), quasi-steady state photoconductance (QSSPCD), optical microscope, spectrumresponse and solar cell efficiency test. The minority carrier lifetime and performance of solar cell reduced depend on oxygen precipitates. A few of oxygen precipitates have formed after single-step annealing; and they do not impact the efficiency dramatically. Pre-annealing at 650 ℃ for 4 h enhances the oxygen precipitation when it is subjected to middle temperature annealing. The solar cells performance decayed sharply. Especially annealing at 950 ℃ for 3 h, the V os and I sc of cells decrease 12% and 25% respectively. Few oxygen precipitates have formed in silicon after high temperature annealing at about 1050 ℃ whether pre-annealing is used or not, and the performance of cells is notbe affected.     

铸铁溶液中氧的含量及形态

本文研究了铸铁溶液中全氧量的变化,并用定氧探头检测了溶解氧量。研究表明,铁水中全氧量随冲天炉送风湿度增加而明显增大。铁水含氧量增高主要是化合氧增多。而溶解氧变化很小。     

TC11钛合金中氧铝偏析与脆性断裂

借助ＳＥＭ及ＥＤＡＸ、ＡＥＳ对某些ＴＣ１１钛合金棒材机械性能差的原因进行了研究。。结果表明材料延伸率、断面收缩率及冲击值低，显微硬度值高的拉伸和冲击断口上都呈现脆性解理断裂的断裂源，源区显微组织为条状α及空洞，且氧铝偏高。氧铝偏高造成α＋β→β相变温度和再结晶温度升高，使加工变形中形成的条状α在随后的热处理中得不到改变，并导致拉伸、冲击时的脆性断裂     

金属材料中微量氢和氧的分析

叙述了惰性气氛熔化法测定金属材料中微量氢和氧的条件和方法。着重研究影响分析限的空白因素及降低空白的方法和分析限，制定出了Ｔｉ，Ｚｒ，Ｈｆ，Ｔａ，Ｎｂ，Ｗ，Ｍｏ，Ａｌ，Ｃｕ等及其合金中微量氢和氧的分析方法。     

HVOF喷涂NiCr-Cr3C2过程中Laval管壁结瘤成因的探讨

围绕超音速火焰喷涂NiCr-Cr3C2涂层时在Laval管内壁产生结瘤的问题，在分析结瘤产物显微结构的基础上探讨了形成结瘤的原因。研究发现，结瘤产物具有层状组织结构，说明结瘤的形成机制与涂层形成机制相似；在HVOF喷涂时，导致Laval管内壁结瘤的原因主要包括：喷涂材料、喷涂粉末颗粒粒度、喷涂工艺参数、Laval管的内表面粗糙度。     

Fatigue crack growth resistance of SiC<Subscript>p</Subscript> reinforced Al alloys: Effects of particle size,particle volume fraction,and matrix strength

The main aim of this work was to study the effects of particle size, particle volume fraction, and matrix strength on the long fatigue crack growth resistance of two different grades of Al alloys (Al2124-T1 and Al6061-T1) reinforced with SiC particles. Basically, it was found that an increase in particle volume fraction and particle size increases the fatigue crack growth resistance at near threshold and Paris regimen, with matrix strength having a smaller effect. Near final failure, the stronger and more brittle composites are affected more by static modes of failure as the applied maximum stress intensity factor (K _max) approaches mode I plane strain fracture toughness (K _IC).     

Water vapor and oxygen permeability of wax films

The water vapor (WVP) and oxygen (O₂P) permeabilities of beeswax (BW), candelilla wax (CnW), carnauba wax (CrW) and microcrystalline wax (MW), formed as freestanding films, were determined. CnW and CrW both had small values for O₂P (0.29 and 0.26 g·m⁻¹·sec⁻¹·Pa⁻¹ × 10⁻¹⁴, respectively), which are less than half the value for high-density polyethylene and about a decade greater than the value for polyethylene terephthalate. O₂P values for BW and MW were about 6−9× greater than those of CnW and CrW. WVP of CnW was 0.18 g·m⁻¹·sec⁻¹·Pa⁻¹ × 10⁻¹², which is about one-half the value for CrW and MW and about one-third the value for BW. The WVP of CnW was somewhat less than that of polypropylene and somewhat greater than that of high-density polyethylene. Differences in permeabilities among the wax films are attributed mainly to differences in chemical composition and crystal type as determined by X-ray diffraction.     

氧泵型催化膜反应器中甲烷氧化偶联反应(Ⅰ)——氧泵型催化膜的制备及其反应性能

本文采用1％Sr/La_2O_3-Ag-YSZ氧泵型催化膜反应器进行了甲烷氧化偶联反应研究。比较了不同制备方法的催化膜的反应性能,结果发现浸涂法(Ag-YSZ管随旋转轴转动涂制)制备的膜性能最佳。研究了操作条件对甲烷氧化偶联反应的影响。研究证明,传递氧与气相氧同时进料是一种较好的反应方式。结果表明,利用该反应器不仅可以简化分离过程,而且还可得到更高的C_2烃选择性。     

Miniemulsion and conventional emulsion copolymerization of styrene and butadiene: Effect of process on gel content

The properties of styrene/butadiene copolymers obtained by conventional emulsion and miniemulsion polymerizations were studied. Thin layer chromatography with flame ionization detection was used to determine the gel fraction of the copolymer in the latex particles as a function of conversion. It was found that the gel formation began at a higher conversion in the miniemulsion polymerization when compared with that in the conventional process. Also, a lower glass transition temperature was noted at the lowest conversion sampled (～25%), implying a higher initial butadiene monomer concentration within the nucleated miniemulsion monomer droplets when compared with particles formed conventionally. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4616–4622, 2006