全文获取类型
收费全文 | 3661篇 |
免费 | 471篇 |
国内免费 | 156篇 |
专业分类
电工技术 | 29篇 |
综合类 | 281篇 |
化学工业 | 1982篇 |
金属工艺 | 117篇 |
机械仪表 | 61篇 |
建筑科学 | 77篇 |
矿业工程 | 103篇 |
能源动力 | 38篇 |
轻工业 | 600篇 |
水利工程 | 16篇 |
石油天然气 | 142篇 |
武器工业 | 32篇 |
无线电 | 105篇 |
一般工业技术 | 294篇 |
冶金工业 | 335篇 |
原子能技术 | 44篇 |
自动化技术 | 32篇 |
出版年
2024年 | 11篇 |
2023年 | 47篇 |
2022年 | 82篇 |
2021年 | 111篇 |
2020年 | 120篇 |
2019年 | 110篇 |
2018年 | 70篇 |
2017年 | 119篇 |
2016年 | 128篇 |
2015年 | 111篇 |
2014年 | 222篇 |
2013年 | 227篇 |
2012年 | 278篇 |
2011年 | 268篇 |
2010年 | 198篇 |
2009年 | 185篇 |
2008年 | 146篇 |
2007年 | 238篇 |
2006年 | 229篇 |
2005年 | 192篇 |
2004年 | 179篇 |
2003年 | 130篇 |
2002年 | 152篇 |
2001年 | 124篇 |
2000年 | 102篇 |
1999年 | 83篇 |
1998年 | 85篇 |
1997年 | 48篇 |
1996年 | 58篇 |
1995年 | 40篇 |
1994年 | 37篇 |
1993年 | 22篇 |
1992年 | 20篇 |
1991年 | 24篇 |
1990年 | 16篇 |
1989年 | 12篇 |
1988年 | 9篇 |
1987年 | 11篇 |
1986年 | 10篇 |
1985年 | 4篇 |
1984年 | 8篇 |
1983年 | 6篇 |
1982年 | 4篇 |
1981年 | 4篇 |
1980年 | 3篇 |
1979年 | 1篇 |
1977年 | 1篇 |
1976年 | 1篇 |
1959年 | 1篇 |
1951年 | 1篇 |
排序方式: 共有4288条查询结果,搜索用时 187 毫秒
11.
文章采用氢氧化钠碱熔试样,经硫酸中和后,在1+1盐酸介质中蒸馏分离锗,使大部分干扰元素经蒸馏分离,并在1+1盐酸介质中用碘酸钾容量法滴定锗。该法滴定终点明显,准确率高。标准回收率为95.52%~105.78%,变异系数为3.18%~4.42%。适用于锗渣中高含量的锗的测定分析。 相似文献
12.
本文报导了甲基环氧丙酸钾的合成方法、农田应用,IR、NMR分析数据及与环氧丙酸钾的性能比较。 相似文献
13.
高岭土生产硫酸铝及沉淀法除铁的研究 总被引:4,自引:0,他引:4
对工业品硫酸铝的制备及沉淀法除铁的工艺进行了研究。实验结果表明,硫酸原料的质量分数可提高至63%,用高锰酸钾作为除铁剂可除去产品中45%~50%的铁。 相似文献
14.
对KCl与NaCl在低盐固态酱油发酵中的应用进行了比较研究。结果表明:用KCl代替NaCl,KCl的浓度要高于NaCl才能抑制发酵期间杂茵的污染,且使用KCl的发酵效果比NaCl要好。 相似文献
15.
Karen S. Servilla Antonios H. Tzamaloukas Charles Carter Glen H. Murata 《Hemodialysis international. International Symposium on Home Hemodialysis》2002,6(1):35-39
We developed a composite compliance index as the sum of the compliance scores for interdialytic weight gain (IDWG), pre‐dialysis serum potassium and phosphorus concentrations (each scored from zero to 3, with 3 indicating the poorest compliance), and skipping hemodialysis sessions (scored from zero to 9, with 9 indicating the poorest compliance). We used this composite score to prospectively evaluate compliance in 25 prevalent hemodialysis patients over a period of 1 year. We then followed these patients for another 3.5 years. The patients studied were divided into two groups: group A (poor compliance) consisted of 9 subjects with composite score ≥ 9 (13.2 ± 3.2); group B (better compliance) consisted of 16 subjects with composite score < 9 (4.7 ± 1.8). Age, duration of hemodialysis, and frequency of diabetes mellitus did not differ between the groups. Group A contained higher fractions of subjects with history of alcoholism (66.7% vs 12.5%, p = 0.010), other substance addiction (44.4% vs 0%, p = 0.010), and severe psychosocial problems (88.9% vs 18.8%, p = 0.002). Mean survival from the beginning of observation, estimated by actuarial life‐table survival analysis, was 1.19 years in group A and 2.60 years in group B (p = 0.0265). A composite compliance index incorporating domains indicating adherence to diet, medications, and dialysis schedule identified other behavioral problems in poorly compliant patients. Hemodialysis patients characterized by this composite index as poorly compliant had shortened survival. 相似文献
16.
Rubina H. Shreiner 《Journal of research of the National Institute of Standards and Technology》2002,107(5):393-399
The stability of solutions having an electrolytic conductivity, κ, of 5 μS/cm to 100 000 μS/cm packaged in glass screw-cap bottles, glass serum bottles, and glass ampoules was monitored for 1 year to 2 years. The conductivity was determined by measuring the ac resistance of the solution. Mass loss was also monitored for solutions packaged in bottles. The solutions were prepared using KCl in water (κ ≥100 μS/cm) or KCl in 30 % (by mass) n-propanol 70 % (by mass) water (κ ≤ 15 μS/cm). The conductivity changes were compared by packaging type and by nominal κ. The main causes of the κ changes are evaporation (screw-cap bottles) and leaching (screw-cap bottles, serum bottles, and ampoules). Evaporation is determined from mass loss data; leaching occurs from the glass container with no change in mass. The choice of optimal packaging, which depends on the conductivity level, is the packaging in which κ changes the least with time. Ampoules are the most suitable packaging for standards having nominal κ values of 500 μS/cm to 100 000 μS/cm. Screw-cap bottles are most suitable for standards having a nominal κ of 5 μS/cm to 100 μS/cm. 相似文献
17.
At high temperatures in clean oxidizing environments, SiC forms a very protective SiO2 film, but, in environments containing low levels of gaseous alkali salt contaminants or where condensed salts may deposit on the surface, the resistance of the film is significantly reduced. Oxidation kinetics of SiC were measured by continuous thermogravimetric analysis in a controlled environment containing CO2 , H2 O, and O2 plus low levels of potassium-containing salts. Potassium was found to be incorporated into the SiO2 scale and to significantly change its transport properties and its morphology. The rate of scale formation was found to increase directly in proportion to K in the scale. A change in mechanism was observed when water vapor was added to the reacting gas stream. 相似文献
18.
P Pramanik 《Bulletin of Materials Science》1995,18(6):819-829
Ultrafine (⩽ 150 nm) powders of spinels [MFe2O4 where M = Ni(II), Co(II) and Zn(II)]; rare-earth orthoferrites [RFeO3 where R = Sm, Nd and Gd], and rare-earth garnets [R3Fe3O12 where R = Sm, Nd and Gd] with good purity and chemical homogeneity were prepared through two new versatile chemical routes.
The first route involved the coprecipitation of the desired metal nitrates from their aqueous solution, in presence of a water
soluble polymer-polyvinyl alcohol (PVA), by triethyl ammonium carbonate solution. The other process involved complete evaporation
of a mixture of optimum amounts of PVA and the desired aqueous metal nitrate solutions, with and without the addition of optimum
amounts of urea when the mixture was evaporated to a pasty mass. In addition, detailed study on the reported potassium ferricyanide
route was also carried out for the production of the rare-earth orthoferrite powders. The various precursor as well as the
heat-treated mixed-oxide powders, prepared through each of the routes, were compared by the physical characterization studies
involving thermal gravimetry and differential scanning calorimetry, infrared spectroscopy, X-ray powder diffraction, transmission
electron microscopy, and room temperature magnetic measurements. 相似文献
19.
20.