铠装硅酸钾胶黏剂在特殊工况下的绝缘失效分析

为探索铠装硅酸盐胶黏剂在特殊环境下的绝缘特性，本文制备不同碱金属离子含量及固液配比的硅酸钾胶黏剂样品，将其固封于不锈钢管体中，在潮湿环境与高温条件下分析其绝缘性能并进行失效分析。结果表明：在潮湿环境中，胶体中的固液配比及碱金属（K⁺）含量会影响铠装试样的整体绝缘性能，当固液配比为2∶1时，硅酸钾与硅溶胶质量比在（2～1）∶1之间时，其绝缘效果较佳；在高温条件下，随着温度的升高及保温时间的延长，铠装壳体中部分合金元素渗入胶体表面，造成样品绝缘性能较大幅度的下降。     

Quality-by-design approach for the development of telmisartan potassium tablets

A quality-by-design approach was adopted to develop telmisartan potassium (TP) tablets, which were bioequivalent with the commercially available Micardis^® (telmisartan free base) tablets. The dissolution pattern and impurity profile of TP tablets differed from those of Micardis^® tablets because telmisartan free base is poorly soluble in water. After identifying the quality target product profile and critical quality attributes (CQAs), drug dissolution, and impurities were predicted to be risky CQAs. To determine the exact range and cause of risks, we used the risk assessment (RA) tools, preliminary hazard analysis and failure mode and effect analysis to determine the parameters affecting drug dissolution, impurities, and formulation. The range of the design space was optimized using the face-centered central composite design among the design of experiment (DOE) methods. The binder, disintegrant, and kneading time in the wet granulation were identified as X values affecting Y values (disintegration, hardness, friability, dissolution, and impurities). After determining the design space with the desired Y values, the TP tablets were formulated and their dissolution pattern was compared with that of the reference tablet. The selected TP tablet formulated using design space showed a similar dissolution to that of Micardis^® tablets at pH 7.5. The QbD approach TP tablet was bioequivalent to Micardis^® tablets in beagle dogs.     

Investigation of Alkali‐Ion (Li,Na, and K) Intercalation in KxVPO4F (x ∼ 0) Cathode

This work compares the intercalation of K, Na, and Li in K_xVPO₄F (x ～ 0). The K_xVPO₄F (x ～ 0) cathode delivers reversible capacities of ≈90–100 mAh g^?1 in K, Na, and Li cells, at an average voltage of ≈4.33 V for K, ≈3.98 V for Na, and ≈3.96 V for Li. This is so far the highest average voltage known for a K‐intercalation cathode. The lower voltage of Li insertion compared to Na is attributable to undercoordinated Li ions in the K_xVPO₄F (x ～ 0) framework. While the material shows high rate capability for all the alkali ions, Li migration in K_xVPO₄F (x ～ 0) is more difficult than with Na and K. This work suggests that a large cavity is not always good for insertion of alkali ions and cathode materials need to be suitably tailored to each intercalating ion species.     

Effects on milk urea concentration,urine output,and drinking water intake from incremental doses of potassium bicarbonate fed to mid-lactation dairy cows

Large variation exists in the potassium content of dairy cow feeds and also within a feed type due to soil type and fertilization. Increased ration K concentration causes a subsequent increase in urinary volume and could be expected to also lower milk urea concentration. Six multiparous mid-lactation Swedish Red dairy cows, all fitted with rumen cannulas, were subjected to 3 different levels of K intake in a Latin square experiment with three 2-wk periods to evaluate the effects on concentrations of milk urea and rumen ammonia, urinary output, and drinking water intake. The treatments were achieved by K supplementation on top of a low-K basal ration fed at individual allowances fixed throughout the experiment. The basal ration, consumed at 20.2 kg of dry matter (DM)/d, provided 165 g of crude protein/kg of DM and consisted of grass silage, concentrates, and urea in the proportions 39.3:60.0:0.7 on a DM basis. Potassium bicarbonate supplementation was 0, 616, and 1,142 g/d, respectively, to give total ration K concentrations that were low (LO; 12 g/kg of DM), medium (MED; 23 g/kg of DM), or high (HI; 32 g/kg of DM). Production and composition of milk was not affected by treatment. A linear effect on milk urea concentration was detected, being 4.48, 4.18, and 3.77 mM for LO, MED, and HI, respectively, and a linear tendency for rumen ammonia concentration with 6.65, 6.51, and 5.84 mg of NH₃-N/dL for LO, MED, and HI, respectively. Milk urea concentration peaked about 3 h after the rumen ammonia peak from the morning feeding, at a level 1.3 mM over the baseline. Urinary urea excretion declined linearly (105, 103, and 98 g of urea-N/d for LO, MED, and HI, respectively). Linear increases occurred in urinary output (0.058 ± 0.001 kg of urine/g of K intake; no intercept; coefficient of determination = 0.997) and drinking water intake (65.9 ± 2.02 + 0.069 ± 0.004 kg of water/g of K intake; coefficient of determination = 0.95). Urinary K concentration leveled off at 12.4 g/L. Urinary creatinine excretion was not affected by K addition, but allantoin excretion increased linearly by 27% from LO to HI, suggesting increased rumen microbial growth. Rumen pH, acetate proportion of total volatile fatty acids, and digestibility of DM, organic matter, and neutral detergent fiber increased linearly with increasing potassium intake. We concluded that increased ration K concentration lowers milk urea concentration with a magnitude significant for the interpretation of milk urea values, but other sources of variation, such as sampling time relative to feeding, may be even more important.     

Partial replacement of sodium chloride with potassium chloride in marinated rabbit meat

This study was aimed at evaluating the consequences of sodium chloride reduction by potassium chloride up to 50% on technological, sensorial and microbiological traits of marinated rabbit meat. In total, 226 rabbit loin meat samples were obtained and subjected to vacuum tumbling using solutions with different NaCl/KCl ratios. Replacing of sodium chloride up to 30% by potassium chloride did not change microbiological traits (total aerobic mesophilic and lactic acid bacteria maximum cell loads), sensorial acceptability (perceived saltiness and overall liking) and technological traits (pH, colour, texture, cooking loss and yield). Otherwise, reduction in sodium chloride to 50% significantly decreased perceived saltiness (4.15 vs. 4.73; P < 0.05) and reduced microbial shelf life by 1 day when compared to control, even if there was still no effect on technological traits. In conclusion, it is feasible imparting an added value for processed rabbit meat products by reduction in sodium content that could increase market interest.     

Multi-scale characteristics of magnesium potassium phosphate cement modified by metakaolin

Workability and early-ages mechanical properties are important indicators of magnesium potassium phosphate cement (MKPC) as a repair material. The effect of metakaolin (MK) on the setting time, fluidity and early-ages strength of MKPC paste was studied, and its influence mechanism was analyzed through pore structure, microstructure and nanomechanical properties. The results show that 10% and 20% of MK prolong the setting time of MKPC paste, but excessive MK shortens the setting time of MKPC paste. Meanwhile, incorporating MK reduces the fluidity of MKPC paste, and the early-ages strength of MKPC specimens increases when the substitution ratio of MK is 10%. When 10% of MK is incorporated to the MKPC paste, the 30-d shrinkage of the sample is only 69% of the control group. Meanwhile, a proper amount of MK can improve the pore structure of the MKPC specimen and make its microstructure denser by generating amorphous aluminosilicate phosphate gel. It is observed from the nano-scale characteristics that incorporating 10% MK can reduce the content of pore phase and unreacted MgO phase, and increase the volume fraction of hydration products.     

基于集成构架的智能MCC在钾肥项目中的应用

结合国投新疆罗布泊钾盐有限责任公司年产120万吨钾肥项目,介绍了集成架构理念,智能MCC控制方式,从顶层工作站对底层电机监控的实现.     

Application of three xanthates collectors on the recovery of nickel and pentlandite in a low-grade nickel sulfide ore using optimum flotation parameters

One of the challenges encountered when processing nickel ore is the presence of other minerals like chalcopyrite, pyrrhotite, pyrite and amphiboles in mineral dressing. Hence, there is need to investigate the selectivity of some collectors at optimum flotation parameters (particle size, milling time, pH and flotation cell) to maximize nickel and pendlandite recovery. Three xanthate collectors, namely potassium amyl xanthate (PAX), sodium isobutyl xanthate (SIBX) and sodium ethyl xanthate (SEX), were investigated in this study. In order to achieve this aim, the physical treatment of nickel sulfide ore and percentage chemical composition of nickel sulfide ore were investigated. The analyses of the concentrates were done using x-ray diffraction (XRD) and x-ray fluorescence spectroscopy (XRF). The optimum nickel and pentlandite recovery was achieved at particle size of 64.73 µm milled for 1.5 h, pH of 9.65 and using a new flotation cell. Also, SEX collector recovered more nickel and pentlandite contents compared to PAX and SIBX collectors when optimum parameters of particle size, milling time, pH and flotation cell were considered. In conclusion, the results showed that the selectivity of SEX is the strongest and will recover more pentlandite in a complex and low-grade nickel sulfide ore.