氯化丁基橡胶阻尼材料动态力学性能的影响因素研究

利用DMA242热机械分析仪,研究了增粘树脂类型、高耐磨炉黑用量、测试频率等因素对氯化丁基橡胶阻尼材料动态力学性能的影响。结果表明,增粘树脂对材料动态力学性能具有显著影响,加入3^#增粘树脂材料的损耗因子峰值最大,损耗因子峰值温度最高;随着高耐磨炉黑用量增大,材料的损耗因子峰值降低、损耗因子峰值温度升高;随着测试频率由3．33Hz到1．66Hz逐渐减小,材料的损耗因子峰值温度逐渐降低,损耗因子峰值逐渐减小。     

类金刚石膜超低摩擦行为的研究进展

近年来,高硬度、低摩擦、高耐磨性的类金刚石(Diamond like carbon,DLC)膜引起了国内外学术界和工业界极大的研究兴趣,尤其是它的超低摩擦行为。首先从宏观和微观角度分析了DLC膜超低摩擦的起源,研究发现DLC膜的微观结构和测试环境是影响DLC膜实现超低摩擦的主要因素,而DLC膜的微观结构由其制备工艺决定。然后系统讨论了制备工艺(包括制备方法、反应气源、掺杂元素和基体材料等)和测试环境(包括真空与干燥惰性气体环境、潮湿环境、高温环境、载荷和滑动速度等)对DLC膜超低摩擦行为的影响规律。最后归纳分析了目前对DLC膜超低摩擦机理的几种解释,指出DLC膜作为超低摩擦材料仍需解决的问题及未来的研究趋势。     

喷嘴洗涤器弯头开孔结构有限元分析及强度评定

由于弯头开孔结构无法按常规设计方法进行开孔补强计算,故对弯头接管开孔区域建立了三维有限元力学分析模型。利用三维实体模型,真实地模拟了特殊结构的形状、载荷分布、边界条件,计算出最接近真实状况的应力分布情况;根据有限元分析结果,按JB4732-1995《钢制压力容器——分析设计标准》进行了应力强度评定,为详细工程设计提供了弯头开孔补强计算方法。     

锅炉飞灰含碳量检测技术的发展和现状

锅炉飞灰含碳量是反映火力发电厂燃煤锅炉燃烧效率的一项重要指标,精确和实时地监测飞灰含碳量有利于提高锅炉燃烧控制水平,降低发电成本,提高机组运行的经济性,同时也有利于提高煤灰的品位,促进煤灰的商品化。综述了飞灰含碳量检测技术的发展和现状,分析了存在的问题,提出了改进的建议,对飞灰含碳量检测技术的发展具有一定的参考价值。     

石油产品运动粘度测定的影响因素

文章对石油产品运动粘度测定的影响因素进行了分析,探讨了计量器具、试验浴的温度、试油流经粘度计的时间、粘度计的位置等因素,通过试验找到了影响粘度测定的主要因素是毛细管粘度计常数和温度计示值以及设备的控温精度,其次是试验人员的操作及仪器的安装。并分析了这些影响因素的应对措施。     

安全仪表系统的功能安全测试研究

阐述了安全仪表系统投入运行前与运行后进行的测试内容和要求,给出安全仪表功能(SIF)各组成部分的离线测试和在线测试的内容和指导原则,对实施离线测试和在线测试的流程、测试要求及方法等方面进行了详细的分析和讨论。所提出的系统和各部件的测试内容、测试要求以及测试流程和技术方法等为规划和管理安全仪表系统SIF整体安全生命周期的功能安全测试与验证提供有力的指导,也为安全仪表系统的分析、设计、开发、运行和维护等各阶段活动提供参考。     

Cathodic delamination: Quantification of ionic transport rates along coating–steel interfaces

So-called cathodic delamination is one of the major modes of failure for organic coatings immersed in electrolyte solutions (e.g. seawater). Cathodic delamination occurs as a result of the electrochemical reactions, which takes place on a corroding steel surface. This means that reactants must continuously be transported from the bulk solution to the cathodic areas. The transport of sodium ions from a defect in the coating to the cathodic areas is generally considered the rate-determining step for cathodic delamination because the transport of oxygen and water through the coating is sufficient for the corrosion processes. In this work, a novel practical method, which allows direct estimation of the apparent diffusion coefficient of sodium ions in the ultrathin aqueous layer at the coating–steel interface, is described. The apparent diffusion coefficients estimated are of similar magnitude as previously reported values and show an acceptable repeatability. The method was used to obtain the apparent diffusion coefficients of sodium ions in the coating–steel interface for three commercial inert-pigmented epoxy coatings. The delamination rates predicted using the apparent interfacial diffusion coefficients and Fick's second law, under the assumption of a transport controlled mechanism, show qualitative agreement with the observed delamination rates in 0.5 M sodium chloride. This confirms that the rate-determining step of cathodic delamination is the transport of sodium ions along the coating–steel interface.     

新型电液比例阀的计算机性能测试方法及其实现

为了降低新型电液比例阀的检测费用,提高液压系统可靠性,给设备的检修和维护提供可靠的技术保障,针对新型电液比例阀的性能检测问题,研究其静态及动态特性的测试方法,设计计算机测试系统,开发相应的性能测试软件.应用情况表明:所开发的系统提高了新型电液比例阀的利用率和可靠性,解决了该类电液比例阀难以维修的难题.     

Investigation of the influence of iron-containing abrasives on the corrosion behaviour of the aluminium alloy AlSi1.2Mg0.4

The corrosion resistance of aluminium surfaces is closely linked to the surface state after a grinding process. For years, iron-containing abrasive materials were suspected to lead to increased corrosion susceptibility after processing of aluminium surfaces. To prove a possible correlation between the iron content of an abrasive and the corrosion behaviour of aluminium components, scientific investigations and experimentally practical corrosion tests are necessary. For the current investigation, specimens of a technical Al-Si alloy from the same batch were used. The test specimens were mechanically ground with various resin-bonded model abrasives containing different iron contents. The performed corrosion tests did not reveal a negative influence of the different iron-containing abrasives on the corrosion behaviour of the Al–Si alloy. However, the most sensitive measuring method (electrochemical noise) showed differences in the surface activity depending on the type of abrasive.     

Anticorrosive effectiveness of coatings with reduced content of Zn pigments in comparison with zinc-rich primers

ABSTRACT

Typically, an anticorrosive coating system for long-term protection consists of a primer, one or several intermediate coats, and a topcoat. In such systems, zinc-rich primers are often used as they ensure good adhesion to the substrate and protect it from corrosion. Such coatings are very highly pigmented, which sometimes leads to losses in cohesive strength and deterioration of mechanical properties. Furthermore, Zn is known to be harmful to the environment. In this work we present Zn primers with reduced Zn content and better protective properties than traditional zinc-rich primers. The formulations of different Zn pigments in the epoxy matrix were developed with the concentration of zinc particles reduced to about 50% in the dry coating. To evaluate the distribution of pigments scanning electron microscopy has been employed. The anticorrosive properties were tested using the salt spray test and electrochemical impedance spectroscopy. The mechanical properties of the coatings were also tested.