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91.
Atomic Insights into Phase Evolution in Ternary Transition‐Metal Dichalcogenides Nanostructures 下载免费PDF全文
Phase engineering through chemical modification can significantly alter the properties of transition‐metal dichalcogenides, and allow the design of many novel electronic, photonic, and optoelectronics devices. The atomic‐scale mechanism underlying such phase engineering is still intensively investigated but elusive. Here, advanced electron microscopy, combined with density functional theory calculations, is used to understand the phase evolution (hexagonal 2H→monoclinic T′→orthorhombic Td) in chemical vapor deposition grown Mo1− x W x Te2 nanostructures. Atomic‐resolution imaging and electron diffraction indicate that Mo1− x W x Te2 nanostructures have two phases: the pure monoclinic phase in low W‐concentrated (0 < x ≤ 10 at.%) samples, and the dual phase of the monoclinic and orthorhombic in high W‐concentrated (10 < x < 90 at.%) samples. Such phase coexistence exists with coherent interfaces, mediated by a newly uncovered orthorhombic phase Td′. Td′, preserves the centrosymmetry of T′ and provides the possible phase transition path for T′→Td with low energy state. This work enriches the atomic‐scale understanding of phase evolution and coexistence in multinary compounds, and paves the way for device applications of new transition‐metal dichalcogenides phases and heterostructures. 相似文献
92.
A scanning electron microscope (SEM) is a sophisticated equipment employed for fine imaging of a variety of surfaces. In this study, prediction models of SEM were constructed by using a generalized regression neural network (GRNN) and genetic algorithm (GA). The SEM components examined include condenser lens 1 and 2 and objective lens (coarse and fine) referred to as CL1, CL2, OL-Coarse, and OL-Fine. For a systematic modeling of SEM resolution (R), a face-centered Box–Wilson experiment was conducted. Two sets of data were collected with or without the adjustment of magnification. Root-mean-squared prediction error of optimized GRNN models are GA 0.481 and 1.96×10-12 for non-adjusted and adjusted data, respectively. The optimized models demonstrated a much improved prediction over statistical regression models. The optimized models were used to optimize parameters particularly under best tuned SEM environment. For the variations in CL2 and OL-Coarse, the highest R could be achieved at all conditions except a larger CL2 either at smaller or larger OL-Coarse. For the variations in CL1 and CL2, the highest R was obtained at all conditions but larger CL2 and smaller CL1. 相似文献
93.
为满足非接触化、小型化、集成化、数字化、智能化等现代检测技术的发展要求,从成本、工作原理、灵敏度等方面综合考虑,现采用以光电定位模块为核心的光电定位技术,以无线传感器网络作为数据传输与管理的技术手段,构建了无线光电定位网络,并进行了实验分析.可实现多点实时监测、异地显示测量数据、数据网络化管理等特殊需求;涵盖了多学科领... 相似文献
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Distributed uplink scheduling in OFDMA systems is considered. In the proposed model, mobile terminals have the responsibility of making their own transmission decisions. The proposed scheme is based on two dimensional reservation in time and frequency. Terminals use channel state information in order to favor transmissions over certain subchannels, and transmission is done in a probabilistic manner. The proposed approach provides more autonomy to mobile devices in making transmission decisions. Furthermore, it allows avoiding collisions during transmission since it leads to collision detection during the resource reservation phase. The proposed approach is compared to other random access methods and shown to be superior in terms of increasing sum-rate, reducing the number of users in outage, and reducing the collision probability in the reservation phase. 相似文献
97.
朴光秉 《数字社区&智能家居》2008,3(12):1604-1605
该文在介绍国外农业电子商务发展的背案下,对我国农业电子商务发展的现状作了实例的分析和对策研究。 相似文献
98.
Malatesta M Frigato E Baldelli B Battistelli S Foà A Bertolucci C 《Microscopy research and technique》2007,70(7):578-584
Reptiles represent an interesting animal model to investigate the influence of temperature on molecular circadian clocks. The ruin lizard Podarcis sicula lives in a continental climate and it is subjected to wide range of environmental temperatures during the course of the year. As consequence, ruin lizard daily activity pattern includes either the hibernation or periods of inactivity determined by hypothermia. Here we showed the rhythmic expression of two clock genes, lPer2 and lClock, in the liver of active lizards exposed to summer photo-thermoperiodic conditions. Interestingly, the exposition of lizards to hypothermic conditions, typical of winter season, induced a strong dampening of clock genes mRNA rhythmicity with a coincident decrease of levels. We also examined the qualitative and quantitative distribution of lPER2 and lCLOCK protein in different cellular compartments during the 24-h cycle. In the liver of active lizards both proteins showed a rhythmic expression profile in all cellular compartments. After 3 days at 6 degrees C, some temporal fluctuations of the lCLOCK and lPER2 are still detectable, although, with some marked modifications in respect to the values detected in the liver of active lizards. Besides demonstrating the influence of low temperature on the lizard liver circadian oscillators, present results could provide new essential information for comparative studies on the influence of temperature on the circadian system across vertebrate classes. 相似文献
99.
A technique to segment pores from a normal backscattered electron (BSE) image of cement-based materials is presented. The upper threshold grey level for porosity is determined from the inflection point of the cumulative brightness histogram of the BSE image. This represents a critical point where a small incremental grey value will cause a sudden increase in thresholded area, a condition termed as overflow. The proposed technique was found to be more consistent and reliable than existing methods. Significantly fewer images are required to achieve a satisfactory level of statistical confidence for quantifying porosity. 相似文献
100.