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101.
Synthesis of lanthanum hydroxide and lanthanum oxide nanoparticles by sonochemical method 总被引:1,自引:0,他引:1
Masoud Salavati-Niasari Ghader HosseinzadehFatemeh Davar 《Journal of Alloys and Compounds》2011,509(10):4098-4103
In this work lanthanum hydroxide nanoparticles were synthesized by sonochemical method. La2O3 nanoparticles were obtained after calcination of the La(OH)3 nanoparticles precursor in air at 600 °C for 2 h. The effect of some parameters such as concentration of precursors, pulse time of sonication, time of sonication, and addition of PEG as surfactant on the morphology and the particle size were studied. The as-prepared products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray photoelectron spectrum (XPS) and Fourier transform infrared (FT-IR) spectra. 相似文献
102.
103.
Li Yan Yu Chunjiang Luo Zhongyang Xu Zhu'an Cen Kefa 《中国稀土学报(英文版)》2006,24(4):407-407
Compositely doped oxide La0.5Sr0.5CoO2.91 (LSC) was synthesized using solid state reaction and citric acid-nitrate low temperature self-propagating combustion methods. The crystal structure and the particle size micrograph of LSC powders synthesized by different methods were investigated with XRD and SEM. The experimental results show that the single perovskite phase of LSC can be synthesized by solid state reaction method, but LaSrCoO4 phase appears in LSC powder synthesized by citric acid-nitrate low temperature self-propagating combustion method. The LSC particle by citric acid-nitrate low temperature self- propagating combustion method has smaller size. To analyze the character of cathode material based on Ceo.gGdo.101.95(GDC) electrolyte, two types of cathode wafers were fabricated with the two kinds of LSC and GDC powders at the mass rate of 6:4, respectively. The electrical conductivity of the sintered samples was measured by four probe DC method from 300 to 800 ℃. The cathode with LSC particle by citric acid- nitrate low temperature self-propagating combustion method has higher electrical conductivity. In order to investigate the stability, the two samples were put into the muffle furnace to heat up in air at 800℃for 800 h. To analysis the reason for reduced electrical conductivity, the crystal structure and the particle micrograph of the cathode wafers before and after an exposure were investigated with XRD and SEM. The result shows that new crystal structure appears in both the two kinds of cathode wafers and crystal micrographs change a lot. 相似文献
104.
105.
Won-Jae Lee Guoxia Liu Byoung-Chul Shin Geun-Hyoung Lee Il-Soo Kim Nam-Yeal Lee Sang-Ouk Ryu Woong-Chul Shin Jae-Man Lee Jindong Kim 《Journal of Electroceramics》2004,13(1-3):71-75
The phase formation and electrical properties of (Bi, La)4Ti3O12 (BLT) thin film and V-, Sm-doped BLT thin films prepared by the chemical solution deposition method on Pt/TiO2/SiO2/Si substrates have been investigated. It was observed that the microstructure and electrical properties of BLT thin films dramatically varied with V- and Sm-doping. The crystallinity and grain size of BLT thin films were definitely increased by V- and Sm-doping into BLT films, which resulted in the enhancement of remanent polarization in doped BLT films. The remanent polarization (Pr) of Sm-doped BLT films annealed for 3 min by an RTA system was about 9 C/cm2. The V- and Sm-doped BLT films also exhibited good fatigue characteristics under bipolar stressing to 1010 cycles. 相似文献
106.
107.
采用大气等离子喷涂了一种新型的纳米La2Zr2O7热障涂层,比较了纳米La2Zr2O7和纳米ZrO2涂层的隔热性能.结果表明,与纳米YPSZ涂层相比,纳米结构的La2Zr2O7具有更好的隔热性能.并讨论了涂层显微组织对涂层隔热性能的影响. 相似文献
108.
Recent studies have shown that heavy metals havebecome the most important contaminants in the environ-ment.Some heavy metals ,such as Pb, Cd, Hg, As ,Co,and Cr have genetic toxicity. They disturb DNAmetabolismand lead to aberrance of chromosome andDNA[1].… 相似文献
109.
110.
Effects of La2O3/Li2O/TiO2- Coating on Electrochemical Performance of LiCoO2 Cathode 总被引:1,自引:0,他引:1
Conventional cathode material (LiCoO2) was modified by coating with a thin layer of La2O3/Li2O/TiO2 for improving its performance for lithium ion battery. The morphology and structure of the modified cathode material was characterized by SEM, XRD, and Auger electron spectroscopy. The performance of the cells with the modified cathode material was examined, including the cycling stability, the diffusion coefficient under different voltages, and the C-rate discharge. The results showed that the cell composed of the coated cathode material discharged at a large current density, and possesses a stable cycle performance in the range from 3.0 to 4.4 V. It was explained that the rate of Li ion diffusion increased in the cell while using La2O3/Li2O/TiO2-coated LiCoO2 as the cathode and the coating layer may act as a faster ion conductor (La2O3/Li2O/TiO2). 相似文献