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51.
LiNi0.5Mn1.5O4 powder was synthesized via sol-gel method and coated with ZnO in order to test the electrochemical cyclability of the material as a cathode for the secondary Li battery in the 5 V range at 55 °C. The ZnO-coated LiNi0.5Mn1.5O4 powder nearly maintained its initial capacity of 137 mA h g−1 after 50 cycles whereas the uncoated powder was able to retain no more than 10% of the initial capacity after 30 cycles. TEM analysis of the cycled cathodes suggests that the formation of the graphitic surface phase, hindering the Li migration, may be responsible for the rapid capacity loss of the uncoated material while no such phase was observed on the surface of the ZnO coated LiNi0.5Mn1.5O4 powder. 相似文献
52.
David Mills 《Granular Matter》2004,6(2-3):173-177
For fine powdered materials, capable of being conveyed in dense phase, a conveying region exists in which instability in flow and pipeline blockage can occur if the pressure gradient available is insufficient to maintain a minimum value of solids loading ratio. A reduction in material flow rate can also lead to pipeline blockage in this region. Conveying trials under-taken with cement are used to illustrate the nature of the problem. 相似文献
53.
棒状液晶分子相变问题的机械旋转模型研究 总被引:2,自引:1,他引:1
综述一种关于棒状液晶材料的分子结构与液晶相的相关关系的研究成果。介绍了有关液晶分子的机械旋转模型。该模型将液晶分子视作一种高速旋转的转子,通过分子参数计算,对液晶材料的相变温度和分子结构之间的关系给出了一种全新的解释。最新研究表明,含氟三苯液晶材料的分子结构中存在slim和fat现象,能够对液晶材料的相变进行合理解释。该模型能够通过简单的模型方法对新型液晶材料的分子设计与合成提供有用的信息。 相似文献
54.
尺度目标识别中的若干技术问题 总被引:1,自引:0,他引:1
从工程应用的角度阐述了现代鱼雷常用的尺度目标识别原理,讨论了影响识别距离的若干因素和措施,提出了小尺度模拟靶通过亮点延时算法以弥补尺度不足及其试验技术,试验结果表明,该方法可以获得良好效果。 相似文献
55.
On the basis of new concept using a solid disperse phase we have developed an efficient catalytic solid-phase-system for epoxidations of alkenes using urea–hydrogen peroxide (urea–H2O2) complex and cetylpyridinium dodecatungstate ((CetylPy)10[H2W12O42]) catalyst on fluorapatite (FAp). The recovered solid catalyst phase was reused to keep the catalytic activity after several times. In the conceptual idea it is a key point that in situ solid-phase-activation of the catalyst with urea–H2O2 proceeds to form microcrystals of the active species dispersed on the solid phase. The dispersion of the catalyst on FAp in the case of tungstic acid (H2WO4) was suggested by EPMA analysis. We proposed the peroxo type of species keeping the parent polyoxometalate framework as novel active species from FT-IR spectroscopic studies. FAp phase plays important roles of dispersing the active species on its surface to have high catalytic activity and of stabilizing the active species to lead to high reusability. 相似文献
56.
STUDY ON PHASE PERCEPTION IN SPEECH 总被引:4,自引:0,他引:4
Tong Ming Bian Zhengzhong Li Xiaohui Dai Qijun Chen Yanpu 《电子科学学刊(英文版)》2003,20(5):387-392
The perceptual effect of the phase information in speech has been studied by auditory subjective tests. On the condition that the phase spectrum in speech is changed while amplitude spectrum is unchanged, the tests show that: (1) If the envelop of the reconstructed speech signal is unchanged, there is indistinctive auditory perception between the original speech and the reconstructed speech; (2) The auditory perception effect of the reconstructed speech mainly lies on the amplitude of the derivative of the additive phase; (3) td is the maximum relative time shift between different frequency components of the reconstructed speech signal. The speech quality is excellent while td <10ms; good while 10ms< td <20ms; common while 20ms< td <35ms, and poor while td >35ms. 相似文献
57.
Kenzo Kitayama 《Journal of the American Ceramic Society》1992,75(6):1447-1451
Phase equilibria in the Ta-Co-O and Nb-Co-O systems have been studied at 1200°C at oxygen partial pressures from 10−0.68 to 10−13.50 atm for the former and from 10−0.68 to 10−13.30 atm for the latter. In both systems, M2 CoO6 and M2 Co4 O9 are stable ternary compounds under the experimental conditions, and a new phase, Nb5 Co2 O14 , has been identified. The Ta-Co-O system is simple, whereas the Nb-Co-O system is somewhat more complicated because of the extra phase. The lattice constants of the ternary compounds have been determined and compared with previous values. The standard Gibbs energies of reactions have been determined using oxygen partial pressures in equilibrium with three solid phases. 相似文献
58.
Ahluwalia Jasjit S.; Nollen Nicole; Kaur Harsohena; James Aimee S.; Mayo Matthew S.; Resnicow Ken 《Canadian Metallurgical Quarterly》2007,26(2):214
Objectives: Examine the effectiveness of an intervention to increase fruits and vegetables (FV) consumption among smokers. Design: Cluster-randomized trial of 20 public housing developments; 10 randomly assigned to an FV intervention and 10 to a smoking cessation intervention. Main outcome measures: Usual (past 7 days) and past 30 days change in daily FV intake at 8 weeks and 6 months postbaseline. Results: Greater increases were seen in the FV group. At Week 8 and Month 6, the FV group had consumed 1.58 (p = .001) and 0.78 (p = .04), respectively, more daily FV servings in the past 7 days than the cessation group. At the same time points, the FV group had consumed 3.61 (p = .01) and 3.93 (p = .01), respectively, more FV servings in the past 30 days than the cessation group. Completing more motivational interviewing sessions (p = .02) and trying more recipes (p = .02) led to significantly greater increases at Month 6 among FV participants. Conclusions: Motivational interviewing counseling and lifestyle modification through trying out healthy recipes may be effective in helping a high-risk population increase their FV intake. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
59.
激光冲击诱发相变的实验研究 总被引:3,自引:0,他引:3
本对激光冲击是否可以诱发相变进行了试验研究。用功率密度为1.06×10^8W/cm^2的激光器冲击T8钢表面。实验结果表明激光冲击处理使T8钢的表面显微硬度有所提高并可以发生马氏体相变。冲击处理后材料表面硬度提高了两倍,认为相变是T8钢表面硬度提高的原因之一。 相似文献
60.
Recent research suggests that implementing information systems presents considerable difficulties and that many implementations are total or partial failures. This paper argues that what both practitioners and students require are richer and more acceptable models of information systems implementation. Accordingly, case study data concerning the introduction of manufacturing resource planning (MRP II) are used to illustrate five patterns of behaviour (rites) which capture important social actions; and four components of changing psychological orientation. It is argued that appreciation of the rites and psychological developments identified here will support effective change programmes. Guidelines based on our model are provided for practitioners. 相似文献