404铝合金箔材的工艺研究

w(Si)=8.0%～9.4%的404铝合金,主要用作铝合金焊接的钎焊板,由于Si含量高,目前所生产的404高硅合金箔工艺并不完善.通过调整工艺试验,最终确定坯料退火的温度为420℃,成品道次轧制油采用添加十二醇的火油,轧制工艺采用坯料退火→0.5 mm→0.18 mm→0.085 mm.     

Removal of polonium from stainless steel surface contaminated by neutron irradiated lead-bismuth eutectic

Lead-bismuth eutectic (LBE) has good characteristics for the coolant and/or target of various nuclear systems, but it also has a problem of polonium contamination. In the study, baking experiment was performed to remove polonium contamination on type 316 stainless steel plate that was originated from neutron irradiated LBE. The contaminated type 316 stainless steel plate was baked in a vacuum condition at various temperatures from 200°C to 600°C. In the previous preliminary study, the effect of short time baking was investigated. In the study, the effect of long time baking was investigated. The detail of the experimental method was also described. The result of long time baking experiment showed that the baking method was effective for removal of polonium from stainless steel surface contaminated by neutron irradiated LBE, if the baking was performed at 500°C and higher in a vacuum condition. The obtained result was consistent to the previous preliminary study.     

Determination of thermal conductivity from specific heat and thermal diffusivity measurements of plasma-sprayed cermets

The thermal conductivities of three plasma-sprayed cermets have been determined over the temperature range 23–630°C from the measurement of the specific heat, thermal diffusivity, and density. These cermets are mixtures of Al and SiC prepared by plasma spray deposition and are being considered for various applications in magnetic confinement fusion devices. The samples consisted of three compositions: 61 vol% Al/39 vol% SiC, 74vol% Al/26vol% SiC, and 83 vol% Al/17 vol% SiC. The specific heat was determined by differential scanning calorimetry through the Al melt transition up to 720°C, while the thermal diffusivity was determined using the laser flash technique up to 630°C. The linear thermal expansion was measured and used to correct the diffusivity and density values. The thermal diffusivity showed a significant increase after thermal cycling due to a reduction in the intergrain contact resistance, increasing from 0.4 to 0.6 cm²·^–1 at 160°C. However, effective medium theory calculations indicated that the thermal conductivities of both the Al and the SiC were below the ideal defect-free limit even after high-temperature cycling. The specific heat measurements showed suppressed melting points in the plasmasprayed cermets. The 39 vol% SiC began a melt endotherm at 577°C, which peaked in the 640–650°C range depending on the sample thermal history. Chemical and X-ray diffraction analysis indicated the presence of free silicon in the cermet and in the SiC powder, which resulted in a eutectic Al/Si alloy.Paper presented at the Ninth Symposium on Thermophysical Properties, June 24–27, 1985, Boulder, Colorado, U.S.A.     

快速凝固条件下的共晶生长理论

本文通过理论分析,导出了共晶生长条件下液相中溶质分布规律的一般表达式。理论结果表明,在快速生长条件下,λ~2V 不为常数,与生长速度 V、分配系数 K 和相体积比 f 等因素有关。Jackson—Hunt 模型中的λΔT、(ΔT~2)/V 关系在一般条件下应为λ(ΔT-ms)、(ΔT-ms)~2/V。在快速凝固条件下λ(ΔT-ms)和(ΔT-ms)~2/V 均不为常数,与 V、K、f 等因素有关。     

ZM5铸镁激光填丝补焊工艺特性与组织分析

针对ZM5铸镁缺陷补焊难题,开展光纤激光填丝焊接工艺特性研究,并采用SEM及EDS对焊缝组织进行分析。结果表明,激光束离焦量增加至20 mm时,由激光深熔焊变为热导焊模式,焊缝变宽,熔深变小,稀释率降至0.65,焊缝成形良好;随激光功率增加,稀释率变大,润湿角变大;焊接速度减小,稀释率变小。激光功率为2.1 k W,焊接速度v=0.5 m/min,稀释率为0.52,焊缝成形良好。激光热导焊接热输入小,焊缝组织晶粒细化,先析出α-Mg相基体弥散分布β-Mg17Al12与δ-Mg共晶相。     

封装优态盐同心套管储冷特性试验研究

通过自行建立的试验台,对封装优态盐同心套管式相变储冷单元的蓄冷、释冷特性进行试验研究。主要研究了制冷剂的蒸发温度对蓄冷特性的影响及载冷剂的温度和流量对释冷特性的影响。结果表明,制冷剂的蒸发温度对蓄冷的影响较大,制冷剂的蒸发温度越低,结冰越快,结冰率越大,达到同样的结冰率需要的时间也越短;载冷剂的进口温度对释冷过程的影响较大,相比之下载冷剂的流量对蓄冷和释冷过程的影响要小。在试验条件下,蓄冷时较合理的制冷剂蒸发温度和载冷剂流量分别为1℃和0.241m3/h,释冷过程较合适的载冷剂进口温度和载冷剂流量分别为10℃和0.283m3/h。     

Sn-Cu codeposition from a non-aqueous solution based on ethylene glycol for wafer-bonding applications: direct and pulse electroplating

Metal wafer bonding is being investigated in industry and research fields due to the relatively low process temperatures (T?相似文献   

红枣冻干预冻工艺优化研究

采用电阻法测量了红枣的共晶点温度,其值为-32℃。在实验室冻干机上分别进行了单因素和正交实验,研究了冻结速度、枣片厚度、冻结温度和冻结时间对红枣预冻结的影响情况,得到了红枣冻干过程的冻结工艺最优参数为：冻结速度-1.0℃/min,枣片厚度8 mm,冻结温度-38℃,冻结时间210 min。