真空吸附在薄型铝材零件加工中的应用

公司新产品试制过程中有一批导烟板系列零件,外形纤薄且为铝合金材料,无法完全使用传统夹具装夹或磁性吸附方式固定零件来完成零件数控成形加工。我们通过真空吸附装夹加工的应用,最终完成了零件试制加工任务。该套真空吸附加工方案的应用,为其他薄型铝材零件装夹加工提供了有益的借鉴。     

肟交换法制备乙醛肟工艺的研究

肟交换法是一种制备乙醛肟的新兴工艺,但反应过程存在乙醛肟易被空气氧化等问题,且反应液中存在多组共沸物,分离提纯得到高纯度的乙醛肟较为困难。以丁酮肟为原料,通过向反应器内充入0.2 MPa的氮气,有效避免了乙醛肟氧化与原料乙醛、丁酮肟的挥发,乙醛肟反应选择性达96.12%。开发了产物的提纯工艺,通过Aspen Plus模拟,初步确定减压精馏分离反应液的基本流程,考察了压力、塔板数、回流比、进料位置等操作参数对分离过程的影响。在此基础上,依据模拟确定的操作参数进行实验,确定最优分离提纯工艺,得到纯度为95.33%的乙醛肟产品,收率可达94.31%。本研究可为肟交换法制备乙醛肟的工业化提供一定的指导。     

真空渗流法制备泡沫铝及其动态力学性能的研究

以真空渗流法制备陶瓷中空球泡沫铝,研究了应变率对吸能量和吸能效率的影响、相对密度对屈服强度的影响,并与普通泡沫铝进行比较。结果表明,工艺简单可行,所制备的泡沫铝的动态压缩应力-应变曲线只有弹性变形区和塑性变形区;随应变率的增大,屈服强度和吸能效率变化规律不明显,吸能量增大;随相对密度的增大,屈服强度增大,吸能量增大,吸能效率也增大;动态压缩时两种泡沫铝的吸能效率均较高,最大吸能效率大于0.9,是良好的吸能材料。     

真空压铸的发展

真空系统是压铸过程中排除气体的最有效的方法之一。然而，真空压铸的发展几经起伏，现在则发展到一个新的阶段。从模具中抽出气体是几种抽气方法中较为简便的一种。真空气道的设计与常规气道则有所不同     

VOD工艺在冶炼Z5CN12-04-M钢上的应用

简要介绍了VOD工艺在冶炼ZSCN12—04—M叶片钢上的成功应用。通过采用吹氧精炼和真空氧脱碳等工艺方法“保铬降碳”效果显著。结果表明:产品最终[C]=0.025％,VOD过程降C速率达到每分钟0.012％,总体Cr回收率达到87％,气体含量也达到了较低水平。     

Microstructures and properties of coating from cemented carbide by vacuum powder sintering

In this paper, the microstructures and properties of coating from cemented carbide of WC–Fe–Co–Ni on the substrate 45 steel are studied. The effects of sintering temperature on the microstructures of coating, the interface structures between coating and the substrate, the microhardness distribution and its wear resistance in the coating are investigated. The results indicate that the coating is strongly metallurgical bonded with the substrate by the mutual diffusion and penetration of Fe towards the coating and W, Co, Ni towards the substrate at sintering temperature ranging from 1280 °C to 1300 °C. The coating obtained exhibits compact structure and uniformly distribution of WC with fine grain and porosity free from defects, having high microhardness and preferable wear resistance.     

牙科烤瓷炉在高温下的真空密封措施

介绍了自动可编程真空烤瓷炉在烤瓷工艺过程中，温度对真空度及密封的影响，以及相应所采取的有效的真空密封措施。运行实践表明：该密封措施稳定、可靠，简单易行，便于实现烤瓷过程的自动化。     

The effect of vacuum evaporation plating on phase structure and electrochemical properties of AB5–5 mass% LaMg3 composite alloy

In this paper, Cu, Al and Ni were plated on the AB₅–5 mass% LaMg₃ composite hydrogen storage alloy using a vacuum evaporation plating method. The phase structure and the electrochemical properties were investigated. The X-ray diffraction (XRD) analysis shows that the phase structure is not changed obviously after the plating Cu, Al and Ni on the composites. The electrochemical tests show that maximum discharge capacity, high rate dischargeability (HRD), dischargeability at low temperature and cyclic stability was improved by vacuum evaporation plating Cu, Al and Ni. Maximum of discharge capacity of the AB₅–5 mass% LaMg₃ composite alloy plating Ni can reach 351 mAh/g, which is 3.5% higher than that of the untreated. HRD at I_d = 1200 mA/g of the composite alloy plating Cu is 45.0% of that at 60 mA/g, which is 20.4% higher than the untreated. Discharge capacity of the composite alloy plating Cu at low temperature 233 K is 205 mAh/g, which is 57.3% of that at 298 K, and it is much higher than 36.8% of the untreated composites. The discharge capacity retention of the composite alloy plating Al after 200 cycles is 7.8% higher than the untreated.     

气提式双锥干燥机的开发

介绍了双锥回转真空干燥机的一种改良型机种——气提式双锥干燥机。这种干燥机不但具有原机的优点，并且有效地解决了原机在干燥中易结块成团和大型化困难等问题     

Drying characteristics of porous material immersed in a bed of hygroscopic porous particles fluidized under reduced pressure

A relatively large wet material was immersed in a fluidized bed of hygroscopic porous particle (silica gel beads) under reduced pressure. And then the drying characteristics were compared with those in the case of inert particle (glass beads). The comparison of drying characteristics is performed experimentally and theoretically. In calculation, the water transfer from the sample to the fluidized bed was considered. The calculation results are in good agreement with the experimental data. The effects of the operational conditions (the pressure in the drying chamber and the temperature of the drying gas) on the drying characteristics were also examined in both fluidizing particles.The drying finishes earlier in the case of hygroscopic porous particle than in the case of inert particle regardless of pressure in the drying chamber, since the water transfer from the sample facilitates the drying in the case of hygroscopic porous particles. The temperature decrement in drying appears in the case of inert particle. This phenomenon is also observed in the case of hygroscopic porous particle, but the decrement degree of the temperature is much smaller than that in the case of inert particle. The difference of the minimum temperature in the sample in drying between the cases of hygroscopic porous particle and inert particle is very slight for different pressures in the drying chamber.