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61.
Quantification of the layer dispersion degree in polymer layered silicate nanocomposites by transmission electron microscopy 总被引:1,自引:0,他引:1
As the performance of polymer layered silicate nanocomposites strongly depends on their interior layer dispersion, quantification of the layer dispersion degree is needed. In this work, a new methodology was developed to determine the dispersion parameter D0.1, based on the measurement of the free-path spacing distance between the single clay sheets from the transmission electron microscopy (TEM) images. Several examples of exfoliated, intercalated, and immiscible composites were studied. It was found that the exfoliated composites had D0.1 over 8%, while that of intercalated composites were between 4 and 8%. In the case of intercalation, a high frequency peak appeared at a short spacing distance in the histogram, which was a characteristic of the intercalation, distinct from the exfoliation. The main utility of this TEM methodology is for the quantification of exfoliated or intercalated samples with small number of layers with stacks. The dispersion parameter D0.1 below 4% was suggested to classify as immiscible. A unique advantage of the TEM measurement is that the dispersion degree of different fillers can be counted individually. 相似文献
62.
结合具体工程实例,进行了CFG复合地基作为一种高层建筑地基处理方法的研究,对加固机理和设计步骤作了阐述,并对加固效果进行了检测分析,可供类似工程地基处理作参考。 相似文献
63.
硬质合金与铁基复合材料热等静压扩散连接 总被引:3,自引:0,他引:3
以烧结结态硬质合金和粉末态铁基复合材料为连接对象,研究了两种材料的热等静压扩攻连接工艺,获得了直接连接接头和加镍作中间过渡层的间接连接接头,考察了接头的结合界面形貌,界面的元素扩散和界面结合强度。 相似文献
64.
M.F. Pinnell 《Composites Science and Technology》1996,56(12):1405-1413
The effect of matrix and fiber properties on the strengths and failure processes of notched, continuous-fiber composite specimens has been investigated. Bearing, open and filled hole tension and compression tests were conducted on AS-4/3501-6, IM-8/3501-6, AS-4/APC-2 and IM-8/APC-2 specimens. Failure characteristics of tested specimens were studied by fractographic techniques. Failure progression was tracked by means of incremental loading, radiography and fractographic inspection. 相似文献
65.
Al2O3/TiB2/SiCw三元复合材料的力学性能及显微结构 总被引:3,自引:0,他引:3
以Al2O3为基体,SiC晶须和TiB2颗粒两种增韧剂,采用热压烧结工艺制备了Al2O3/TiB2/SiCw三元复合陶瓷材料。研究了热压工艺参数对材料致密度的影响和晶须含量对该复合材料的力学性能和显微结构的影响。结果表明;随晶须含量的增加,该复合材料的热压温度和保温时间需要相应的增加;晶须拔出、裂纹偏转和晶须的桥接为该复合材料的主要增韧机理;随晶须含量的增加,该材料的室温断裂韧性增加;该材料的断裂韧性随温度的升高而呈增大趋势,并且晶须含量越高,材料的高温断裂韧性增幅越大。 相似文献
66.
An electrically conductive plastic material was obtained by the polymerization of pyrrole on insulating polymeric materials
and nylon cloth impregnated with the oxidant by vapour phase technique, resulting in a uniform, smooth and adherent coating
of conducting polymer having a surface resistance ranging from 200 Ω/□ to 20 kΩ/□, which makes it suitable for applications
as an antistatic material. 相似文献
67.
本文从C/C复合材料的基体入手,研究了基体沥青、焦炭中添加氧化物的工艺条件及其在复合材料中的作用.结果表明,添加氧化物对基体改性,不仅能提高C/C复合材料的高温抗氧化性,也能对其它性能带来很大影响.只要控制适当的工艺条件,就可以得到高性能的C/C复合材料. 相似文献
68.
Experiments have been carried out on relatively wide angle-ply laminate samples with very short gauge lengths. These proved to be very much stronger than samples tested in earlier work, and which form the basis for our present design with these materials. It is highly likely that the early results for strength were more indicative of edge effects than true laminate strength. This is confirmed by data from tests on pressurized tubes. A review of the literature on this shows that such tests produced results which can be an order of magnitude higher than the early laminate tests. Thus our design calculations could well be severely underestimating the potential strength of angle-ply laminates. This may be having serious consequences for the aerospace industry, through the use of design criteria for strength which may be too conservative. Single-fibre experiments may pave the way for more realistic estimates of angle-ply laminate strengths. These indicate that a simple one-third power rule can be used to estimate the potential strength. However, this is purely ad hoc at present, and needs to be put on a firmer footing through both theoretical and experimental studies. Furthermore, if this approach is adopted, edge effects will still have to be allowed for, and estimated on the basis of the aspect ratio of the part. 相似文献
69.
This paper presents a novel process for the fabrication of pultruded polyurethane (PU) composites. The effects of the processing parameters on the mechanical properties (flexural strength and flexural modulus, etc.) and thermal properties (HDT) of the fibre reinforced PU composites by pultrusion have been studied. The processing parameters investigated include pulling rate (in-line speed), die temperature, filler type and content, and post-cure time and temperature. Results show that the composites possessed various optimum pulling rates at different die temperatures. On the basis of the DSC diagram, the swelling ratio, the mechanical properties and the thermal properties of composites, the optimum die temperature can be determined. It is found that the mechanical and thermal properties increase with filler content for various types of filler. The mechanical and thermal properties increase at a suitable post-cure temperature and time. Furthermore, the properties which decreased due to the degradation of composite materials for a long post-cure time will be discussed. 相似文献
70.