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71.
The effect of a range of organic additives on the thermal stability of poly(vinyl chloride), both with and without a chloroparaffin extender, was studied using a number of experimental techniques. Of the additives used the best overall balance was provided by pentaerythritol, which increased stability when the extender was present and had no effect when it was absent. The congo red test emerged as the most suitable technique, being consistent and inexpensive and able to screen several additives simultaneously. Isothermal differential thermal analysis correlated with the congo red test but required more expensive equipment, was time-consuming and demanded good mixing of the poly(vinyl chloride) compound to give reproducible results. Thermogravimetry was not sufficiently sensitive and the heat stability test was the least useful of all. 相似文献
72.
73.
F. D. McDaniel B. L. Doyle C. H. Seager D. S. Walsh G. Vizkelethy D. K. Brice C. Yang P. Rossi M. Nigam M. El Bouanani G. V. Ravi Prasad J. C. Schwartz L. T. Mitchell J. L. Duggan 《Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms》2002,190(1-4):1-10
A new ion beam analysis-based, single ion technique called the time to first photon has been developed to measure the decay of the luminescence signal of phosphors. Such measurements are currently needed to study luminescence decay mechanisms following high-density excitations and to identify strongly luminescent phosphor coatings with short lifetimes for ion photon emission microscopy (IPEM). The samples for this technique consist of thin phosphor layers placed or coated on the surface of PIN diodes. Single ions from an accelerator strike this sample and simultaneously create ion beam induced luminescence (IBIL) from the phosphor that is measured by a single-photon-detector, and an ion beam induced charge collection (IBICC) signal in the PIN diode. In this case, the IBICC signal provides the start pulse and the IBIL signal the stop pulse to a time to amplitude converter. It is straightforward to show that this approach also measures a signal proportional to activity versus time with an accuracy of 5% as long as the number of detected photons per ion is less than 0.1, which usually requires the use of absorbers for the IBIL detector or electronic discrimination for the IBIL signals. Details of the new analysis are given together with examples of luminescence decay measurements of several ceramic phosphors being considered to coat IPEM samples. IPEM is currently being developed at Sandia National Laboratory (SNL), the University of North Texas in Denton, and the Universities and INFN of Padova and Torino. 相似文献
74.
云南省水环境状况及问题分析 总被引:2,自引:0,他引:2
根据2000年云南省主要河流水质监测评价结果,全省评价河段总长9280km中,水质为Ⅰ-Ⅲ类的河长占76.3%,总体上,云南省内各大水系水质良好,但水污染总体上正在加重,从1985-2000年,Ⅰ类河长年均减少2.3%,V类河长年均增长0.6%,废污水直接排入江河是引起污染的重要原因。水环境问题已成为社会经济可持续发展的关键问题,要切实加强水资源的保护,科学地开发利用水土资源,为了有效地改善水环境的质量,污染控制应从源头开始并采取综合治理措施。 相似文献
75.
76.
Optimizing of laminar viscous flow through a pipe by two dimensionless values is investigated analytically. Dimensionless entropy generation and pumping power to heat transfer rate ratio are used as basis for constant viscous and the temperature dependence on the viscosity. For this matter we calculate entropy generation and pumping power for a fully developed in a pipe subjected to constant wall temperature for either constant viscosity and the variable viscosity. The variation entropy generation increase along the pipe length for viscous fluid is drawn, either the variation summation dimensionless entropy generation and the pumping power to heat transfer rate ratio are varying the fluid inlet temperature for fixed pipe length and are varying pipe length for fixed fluid inlet temperature are drawn. For low heat transfer conditions the entropy generation due to viscosity friction becomes dominant and the dependence of viscosity with the temperature becomes essentially important to be considered. 相似文献
77.
二次型时频分析技术的开发与应用 总被引:1,自引:1,他引:0
基于二次型的时频分析是高分辨率时频分析技术的有效方法之一,该项技术能够有效反映时变信号的频谱特性,具有分辨率高、能量集中和跟踪瞬时频率的特点。从时变信号的特点出发,阐述了二次型时频分析技术的基本方法原理,采用正演模型分析验证了该方法的有效性,并在实际地震资料中应用于识别物源方向、划分沉积相带、预测储层结构以及相对厚度等诸多方面,均取得了较好的效果。 相似文献
78.
EFFECTOFTHERATIOTh/UONTLDATINGACCURACY¥P.L.Leung(梁宝鎏);MichaelJ.Stokes(DepartmentofPhysicsandMaterialsScience,CityPolytechnico... 相似文献
79.
The compaction properties of an investigational drug are studied by the use of a compaction simulator. The effects of punch velocity over the range of 30-640 mm-1 on the compaction properties of the pure drug and a variety of formulas incorporating a high dose of the active compound have been investigated. The data were analyzed by applying the Heckel equation. The pure drug was found to have a high yield pressure at a relatively low punch velocity of 31 mm-1. As the punch velocity was increased there was a decrease in crushing strength, primarily as a result of increasing yield pressure. These findings indicate that the pure drug predominantly consolidated by fragmentation and elastic deformation, with a slow plastically deforming component. The information obtained on the consolidation mechanism of the pure drug and, subsequently, on model formulas were instrumental in the design and selection of a robust formula and granulation process. The advantages of conducting dosage form design and characterization studies during the early phase of tablet formulation using means such as a compaction simulator are emphasized in this investigation. 相似文献
80.
External magnetic disturbance influences the quality of the image obtained with a magnetic resonance imaging (MRI) system because it causes magnetic resonance frequency drift. When a superconducting magnet in persistent current mode operation is exposed to external magnetic disturbance coil current varies to keep linkage flux constant. Conventional analysis is usually formulated with constant current and does not provide correct evaluation of drift of magnetic field in the magnet. This paper proposes a method of numerical analysis of magnetic field considering conservation of linkage flux in a superconducting magnet under a persistent current mode operation. This method is applied to evaluate drift of the magnetic field in a superconducting magnet for magnetic resonance imaging due to external magnetic disturbance. Analysis results show good agreement with the experimental results. 相似文献