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161.
A centrifugal partition chromatograph (CPC) was used as a liquid-liquid catalytic reactor for the isomerisation of hexen-3-ol into ethylpropylketone with a water soluble rhodium catalyst. Global mass transfer coefficients were measured and shown to depend on both the nature of the solute and the flow rate. Liquid-liquid partition isotherms were also determined with the CPC using elution chromatography. Finally, a reactor model was derived to account for the experimental results obtained both under stationary and transient (pulse) conditions. A parameter sensitivity evaluation is also presented. 相似文献
162.
碾压混凝土坝施工进度与质量控制的新措施 总被引:1,自引:1,他引:0
碾压混凝土重力坝和拱坝由于连续施工的坝体混凝土体积大,施工期间需要采取较为严格的温度控制措施,而所采取的温控措施是否有效,目前尚没有一个能够用于实际施工过程的快速有效的评估方法和方式,不能根据已施工坝体内的实际情况来控制施工进度和质量。利用分布式光纤温度测量系统来快速地获得坝体混凝土内部的大量温度信息,进而实际标定温度仿真程序并通过标定过程模拟拟施工的连续碾压层,以检验其温控措施的有效性。通过坝体内部的温度、温度变化速率和梯度来达到实时控制坝体碾压上升速度、坝面和仓面养护、以及冷缝灌浆处理等目的。 相似文献
163.
164.
This paper presents a highly stable steady-state torque control system with a feedback of a secondary current signal. The torque control system is constructed with a feedback of the secondary current (I2) signal using a quick response magnetic-field sensor constructed with an amorphous core multivibrator bridge, which can solve the secondary resistance change problem for temperature variation in the IM. Moreover, we added a state feedback to the system to improve the response speed for the unit step function of a torque order. The I2 sensor method has advantages especially at a low-speed range, in which conventional method using an integrator shows control errors. 相似文献
165.
步进式加热炉炉温优化设定模型及软件开发 总被引:1,自引:0,他引:1
针对线材厂步进式加热炉实际工况,提出了基于经验规则的炉温优化设定模型和在线自学习获取知识的思想,并以炉温优化设定模型为核心,开发出加热炉计算机控制系统的优化运行软件。 相似文献
166.
167.
J. G. Blencoe S. E. Drummond J. C. Seitz B. E. Nesbitt 《International Journal of Thermophysics》1996,17(1):179-190
A vibrating U-tube apparatus has been developed for determining the densities of pure fluids and fluid mixtures at 10-200 MPa and 323-773 K. Measured parameters areP,T, andr (period of vibration). Fluids are injected into the U-tube at constantP andT. Three or more reference fluids are used to calibrate the response of the instrument. Fluid mixtures are produced by pumping pure fluids into T-junctions on the upstream side of the U-tube using high accuracy syringe pumps. An automated syringe pump is used to maintainP at setpoint ±0.01 MPa.T is controlled to ±0.01 K using a closed-loop, electronic signal amplification/feedback system. For mixtures, a statistically significant number of measurements of r are obtained to account for the effects of small heterogeneities in fluid composition (generally <0.005X;). Typically, density data for 15 fluids can be obtained in a 6- to 8-h period. Considering all of the potential sources of error in the experimentation, conservative estimates of uncertainty are as follows:P, ±0.02 MPa;T, ±0.05 K;p (pure fluids), ±0.0005g.cm–3; andp (fluid mixtures), ±0.0005-0.0010g-cm–3.Paper presented at the Twelfth Symposium on Thermophysical Properties, June 19–24, 1994, Boulder, Colorado, U.S.A. 相似文献
168.
169.
StudyonFactorsAffectingtheStructureofHighSpeedSteelIngotProducedbyESRLiZhengbang;CheXiangqianAbstract:Theinfluenceofthemetalp... 相似文献
170.
V. N. Parmon 《Catalysis Letters》1996,36(3-4):195-199
A series of vanadium-tin mixed oxide catalysts have been prepared by the solid-state reaction of V2O5 and SnO2 at 1250°C. The fresh and the used catalysts have been characterized by X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR). High temperature oxygen chemisorption (HTOC) has been employed to titrate the coordinatively unsaturated vanadia sites. Ammoxidation of mesitylene has been carried out on these catalysts and an optimum composition of vanadium is arrived at. Better yields of tricyanobenzene (TCB) compared to literature values are obtained. A good correlation between the oxygen uptake and the TCB yield extends the applicability of HTOC to the fused oxide system.IICT Communication No. 3507. 相似文献