Electron beam evaporated carbon nanotube dispersed SnO2 thin film gas sensor

Carbon nanotube (CNT) is a useful material for gas-sensing applications because of its high surface to volume ratio structure. In this work, multi-wall CNTs are incorporated into tin oxide thin film by means of powder mixing and electron beam evaporation and the enhancement of gas-sensing properties is presented. The CNTs were combined with SnO₂powder with varying concentration in the range of 0.25–5% by weight and electron beam evaporated onto glass substrates. From AFM and TEM characterization, CNT inclusion in SnO₂thin film results in the production of circular cone protrusions of CNT clusters or single tube coated with SnO₂layer. Experimental results indicate that the sensitivity to ethanol of SnO₂thin film increases by the factors of 3 to 7, and the response time and recovery time were reduced by the factors of 2 or more with CNT inclusion. However, if the CNT concentration is too high, the sensitivity is decreased. Moreover, the CNT doped film can operate with good sensitivity and stability at a relatively low temperature of 250–300^∘C. The improved gas-sensing properties should be attributed to the increasing of surface adsorption area of metal oxide produced by CNT protrusion.     

DTM320／580型磨煤机传动齿轮轴断裂原因分析及防范措施

介绍了DTM580/320型磨煤机传动齿轮轴断裂的情况,并进行了分析;找到了断裂的原因,提出了防范措施。     

暗室中的几种废品处理方法

本文介绍了暗室操作中产生的几种废品处理方法。采用正确的废品处理方法可以节约资源，减少环境污染。     

Investigation of failure mechanism and modification for film-lubricated precise angular-contact ball bearing

This paper describes an experimental investigation into the performance and lubrication failure mechanism of precise angular-contact ball bearings treated with MoS₂-sputtered film, etc. As an important executive component of various spacecrafts, there are some strict requirements on the lubrication performance of angular-contact ball bearing, but the related experimental data are rare to see in literatures. In this experiment, the lubrication performances of MoS₂-sputtered ball bearing pairs were evaluated by using lifetime test as a main method, and the topographies and compositions of working surfaces were investigated through SEM, AES and EDS. The systematical experiment results reveal that the degradation and failure process of solid lubrication for such ball bearing is divided into three stages with different characters. A supposed failure mechanism has been proposed. An improved lubrication treatment based on above mechanism was conducted for the precise ball bearings, and a later test showed that long endurance life with more than 10⁸ revolutions has been reached.     

非晶Fe-Zr-B薄膜穆斯堡尔谱学研究

用X射线衍射分析、X射线光电子能谱(XPS)和穆斯堡尔谱学研究了直流磁控溅射法制备的Fe-Zr-B薄膜。X射线衍射分析结果表明制备态的薄膜是非晶的;X射线光电子能谱(XPS)结果表明样品表面氧化较明显,深层部分Fe, Zr, B结合占主导地位;穆斯堡尔谱学结果表明薄膜中Fe原子周围Zr、B原子的存在使Fe原子核内场值有所下降并导致超精细场分布P(H)出现双峰结构,薄膜中存在两种不同的局域微结构。     

Monte Carlo Simulation of Electron Swarm in the Diamond Film Growth via EACVD

Monte Carlo simulations are adopted to study the electron transport porcess in the non-uniform electric field.Some important parameters of electrons in diamond films dynamic process at low temperature via EACVD such as angle distribution,energy distribution,average energy of electrons are given.The results indicate that the electron scattering near the substrate is mainly of a large-angle scattering,exhibiting a double-peaking distribution .All of the conclusions provide some theoretical data referential to the vapor dynamic model of diamond film growth at low temperature via EACVD.     

Effects of Deposition Temperature on the Properties of Fluorinated Amorphous Carbon Films

Fluorinated amorphous carbon films (a-C:F) were prepared at different temperatures using a microwave electron cyclotron resonance chemical vapor deposition (ECR-CVD) reactor with CHF3 and C2H2 as source gases. Films were annealed at 500℃ in vacuum ambience inorder to investigate the relationship of their thermal stability, optical and electrical propertieswith deposition temperature. Results indicate that the films deposited at high temperature have a less CFx bonding and a more cross-linking structure thus a better thermal stability. They also have a lower bandgap, higher dielectric constant and higher leakage current.     

电网继电保护及故障信息处理系统关键技术的探讨

根据湖南电网继电保护及故障录波信息处理系统的开发与应用实践 ,以及对国内现有模式和应用情况的分析 ,对该系统中子站设计、远程数据传输、信息组织和高层应用等关键技术问题进行了探讨 ,并给出了部分试验数据和试验结论     

电容器用双向拉伸聚丙烯薄膜打滑试验研究

电容器用双向拉伸聚丙烯薄膜的打滑现象 ,是影响薄膜电容器制造质量的关键因素之一。本文分析了薄膜打滑机理、薄膜粗化机理 ,并进行了大量工艺试验 ,研究了影响薄膜打滑的主要因素 ,并提出了解决方法。优化合理的加工温度工艺是改进薄膜打滑的关键     

高纯金属与聚合物膜pH电极的研制

介绍以纯金属为基体,PVC为载体,α-萘胺为活性物质,三氯甲烷为溶剂研制成的聚合物膜电极,将它用于测定溶液的pH,取得了一些成效。