电解法合成高铁酸钠的实验研究

通过改变传统电极设置位置,评定影响电解效率的各因素以实现电流效率的最大化.在简化电解装置的同时,不影响电流效率的提高.实验结果表明,将传统左右式设置电极改为上下式设置电极,阴极距液面2cm,阳极距底面4cm,电流密度2mA/cm2,NaOH浓度14mol/L,温度60℃,电解1.5h,并加入搅拌的情况下电流效率最大达到58%.     

模拟抗原（Ac-NK16-Ahx-3）免疫反应抗体ELISA检测方法研究

为满足实验室单克隆抗体的制备研究,本实验特对实验室常用的制备单抗的模拟抗原（Ac-NK16-Ahx-3）进行ELISA间接法检测,进而建立一种高效的检测方法。通过对不同稀释度待测抗体的免疫吸附测定,检测出它的最终灵敏度为0.078mg/mL,最佳二抗稀释倍数为300倍,其最佳拟合曲线为y=-0.0732x＋0.6875,R2=0.8619。并且,通过统计学方法进行统计分析,确定出各实验组的相关性及变异系数,从而排除实验中的操作误差,最终可确定最佳的实验条件,并保证实验的准确性。     

Model test of helical angle effect on coal loading performance of shear drum

The work presented in this paper focuses on improving coal loading performance of shear drum.Employing the similarity theory,we carried out a dimensional analysis of the correlation parameters which in...     

广东省电网建设与经济发展关系实证研究

以广东省1993--2011年相关时间序列数据为基础,建立了反映电网建设水平与社会经济发展关系的向量自回归（VAR）模型,在VAR模型的基础上,分析了广东省电网建设指标与社会经济发展指标的格兰杰因果关系,运用脉冲响应函数和方差分解方法分析了电网建设与社会经济发展之间的动态影响。研究结果表明,电网建设是经济增长的基础条件之一,在电网建设与经济增长的相互作用中,电网建设对经济增长的促进作用更为显著。     

铁磁材料磁滞回线的Matlab分析方法设计

铁磁材料的磁特性常用磁滞回线来描述,而剩磁及矫顽力是铁磁材料磁滞回线上的重要参数。就如何使用M atlab来处理磁滞回线的数据给出了处理方法,并予以验证,结果表明所设计的方法处理结果精度高,拟合效果良好,并有较强的程序通用性。     

过硼酸钠在有机合成中的应用

过硼酸钠（ＳＰＢ）是一种安全、稳定、方便、价廉的理想氧化剂，本文综述了它对各类有机化合物的氧化反应。     

Round-Robin Test on methods for determining chloride transport parameters in concrete

This paper presents the results of a Round-Robin Test on methods for determining chloride transport parameters in concrete, carried out by the Technical Committee TC 178-TMC: “Testing and Modelling Chloride Penetration in Concrete” in which 27 different laboratories around the world have participated, using 13 different methods, in triplicate specimens, for 4 different mixes of concrete cast with different binders. Four different groups of methods have been tested: Natural diffusion methods (D), Migration methods (M), Resistivity methods (R) and Colourimetric methods (C). The statistical treatment of the data has been carried out according to the International Standard ISO 5725-2:1994 for the determination of the accuracy (trueness and precision) of measurement methods and results. Part 2: Basic method for the determination of the repeatability and reproducibility of a standard measurement method. In order to make an evaluation of these methods, four indicators have been identified and within each of them, several sub-indicators have been assigned. According to this system of classification, the methods have been classified following each indicator (trueness, precision, relevance and convenience), and also globally, by assigning different factors of importance, F.I., to the different indicators.     

Leakage tests for Am solid sources used for liquid xenon detector monitoring

Experimental tests are described to check solid ²⁴¹Am radioactive sources used to monitor operation of liquid xenon detectors. In particular, radioactive leakage was tested in extreme temperature conditions following immersion in liquid nitrogen for different time periods. No radioactivity loss was detected from the sources considered. The paper describes the source characteristics, test methods and results obtained.