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51.
ZhangBaoji WangXieqing 《中国炼油与石油化工》2003,(3):49-52
A Ti/Si complex zeolite has been prepared. X-ray diffraction and infrared spectrometry study has shown that two structures, namely the ZSM-5 and MCM-41, exist in the sample. BET tests have revealed that the complex zeolite contains regular mesopores of 2.6 nm. Ultraviolet spectrometry analysis has shown that the Ti species exist in the zeolite skeleton in the form of tetra-coordinate valence. The Ti/Si complex zeolite (TS-1/Ti-MCM-41) has apparently improved catalytic activity with respect to the macromolecular organic compound oxidation as compared to individual components of either Ti or Si containing zeolites (TS-1 and Ti-MCM-41). 相似文献
52.
53.
海洋钻井液有机物添加剂生物降解性评价 总被引:1,自引:0,他引:1
随着海洋石油的勘探开发,钻井液有机添加剂不可避免地进入海洋.因此在海洋勘探开发过程中应选择环保性能好,即生物降解性能好的有机物添加剂。用累计耗氧量法测定了海洋钻井液有机添加剂的生物降解性,研究评价了有机添加剂的生物降解规律和机理,探讨了有机物生物降解性同其化学结构的内在联系,为海洋勘探开发过程中选择环保性能好的有机物添加剂提供理论依据。总结实验结果发现:淀粉类(如DFD-140和FI-E1等)最容易生物降解;其次是纤维素类(如MV-CMC等)和烯类单体聚合物(如PAM和PHP);而沥青类、两性离子类则难以生物降解,有的甚至对生物降解起抑制作用。 相似文献
54.
简要介绍了全板电镀镍金加工过程中镀金面发白现象及改善措施。特别是针对高位发白(或粗糙)的产生原因和处理过程进行较为详细的描述,并对工艺在此处理过程中存在问题进行了简要剖析。 相似文献
55.
S.K. Lee D.‐H. Hwang B.‐J. Jung N.S. Cho J. Lee J.‐D. Lee H.‐K. Shim 《Advanced functional materials》2005,15(10):1647-1655
By using Ni0‐mediated polymerization, we have systematically synthesized a series of fluorene‐based copolymers composed of blue‐, green‐, and red‐light‐emitting comonomers with a view to producing polymers with white‐light emission. 2,7‐Dibromo‐9,9‐dihexylfluorene, {4‐(2‐[2,5‐dibromo‐4‐{2‐(4‐diphenylamino‐phenyl)‐vinyl}‐phenyl]‐vinyl)‐phenyl}‐diphenylamine (DTPA), and 2‐{2‐(2‐[4‐{bis(4‐bromo‐phenyl)amino}‐phenyl]‐vinyl)‐6‐tert‐butyl‐pyran‐4‐ylidene}‐malononitrile (TPDCM) were used as the blue‐, green‐, and red‐light‐emitting comonomers, respectively. It was found that the emission spectra of the resulting copolymers could easily be tuned by varying their DTPA and TPDCM content. Thus with the appropriate red/green/blue (RGB) unit ratio, we were able to obtain white‐light emission from these copolymers. A white‐light‐emitting diode using the polyfluorene copolymer containing 3 % green‐emitting DTPA and 2 % red‐emitting TPDCM (PG3R2) with a structure of indium tin oxide/poly(3,4‐ethylenedioxythiophene):poly(styrene sulfonic acid)/PG3R2/Ca/Al was found to exhibit a maximum brightness of 820 cd m–2 at 11 V with Commission Internationale de L'Eclairage (CIE) coordinates of (0.33,0.35), which are close to the standard CIE coordinates for white‐light emission (0.33,0.33). 相似文献
56.
S.‐C. Lo G.J. Richards J.P.J. Markham E.B. Namdas S. Sharma P.L. Burn I.D.W. Samuel 《Advanced functional materials》2005,15(9):1451-1458
We describe the preparation of a dendrimer that is solution‐processible and contains 2‐ethylhexyloxy surface groups, biphenyl‐based dendrons, and a fac‐tris[2‐(2,4‐difluorophenyl)pyridyl]iridium(III ) core. The homoleptic complex is highly luminescent and the color of emission is similar to the heteroleptic iridium(III ) complex, bis[2‐(2,4‐difluorophenyl)pyridyl]picolinate iridium(III ) (FIrpic). To avoid the change in emission color that would arise from attaching a conjugated dendron to the ligand, the conjugation between the dendron and the ligand is decoupled by separating them with an ethane linkage. Bilayer devices containing a light‐emitting layer comprised of a 30 wt.‐% blend of the dendrimer in 1,3‐bis(N‐carbazolyl)benzene (mCP) and a 1,3,5‐tris(2‐N‐phenylbenzimidazolyl)benzene electron‐transport layer have external quantum and power efficiencies, respectively, of 10.4 % and 11 lm W–1 at 100 cd m–2 and 6.4 V. These efficiencies are higher than those reported for more complex device structures prepared via evaporation that contain FIrpic blended with mCP as the emitting layer, showing the advantage of using a dendritic structure to control processing and intermolecular interactions. The external quantum efficiency of 10.4 % corresponds to the maximum achievable efficiency based on the photoluminescence quantum yield of the emissive film and the standard out‐coupling of light from the device. 相似文献
57.
深基坑土钉支护的有限元分析 总被引:14,自引:3,他引:11
本文阐述了土钉支护的发展简史,针对济南济享大厦土钉支护开挖深基坑进行有限元分析并取得较准确的结果,说明在深基坑土钉支护设计中应注意的问题. 相似文献
58.
利用Love波特性计算地基动力响应 总被引:5,自引:2,他引:3
本文利用Love波弥散特性在频域上对地基出平面振动及扭振问题进行了研究。在计算区域内结构将采用有限单元划分,而在边界上则根据Love 面波特性使用传递边界有限单元。本文同时讨论了不同模态波对结构动力响应的贡献。本文方法也适合于静力分析。 相似文献
59.
Per Axel Clausen 《Indoor air》1993,3(4):269-275
A waterborne paint was applied to tin plated steel sheets with three different film thicknesses. The emission of volatile and semivolaile organic compounds ((S) VOCs) from the samples was measured in small climatic chambers under standard conditions over a two-week period. The purpose of the study was to evaluate the effect of the film thickness on the emission rate decay. First order decay models, including sink effects for the high boiling (S) VOCs, were fitted to the concentration versus time data. The results showed that the first order rate constants decrease with increasing film thickness. In uddition, the results indicated that the emissions of the (S)VOCs in the waterborne paint film seemed to be controlled by evaporation. The thicknesses of paint films used in climatic chamber tests to estimate emission rates for product compurison or emission prediction must be known in order to prevent erroneous conclusions 相似文献
60.
水保种草有山地治理、改土开发、松林改造、封禁培育四种类型,是水土保持主要植物措施之一,见效快,效果好,效益显著。要提高认识,建立基地。做好草的转化利用. 相似文献