利用抽余碳五馏份制备TAME

探索了以抽余Ｃ５为原料经与甲醇醚化制ＴＡＭＥ的过程。试验表明，在国产催化剂Ｄ５４型大孔阳离子交换树脂存在下，在反应温度６０℃、ＬＨＳＶ２．４ｈ－１、甲醇／异戊烯物质的量比１．００、反应压力０．２ＭＰａ的条件下，抽余Ｃ５中的异戊烯可与甲醇反应生成醚，异戊烯的转化率达６３．２６％，ＴＡＭＥ的选择性可达９９．６１％。     

球状碳单质分子的发现,研究现状及应用前景

综述了碳的第三种同素异形体──球状碳单质分子的发现、结构、性质及其应用前景。     

Adsorption and decomposition of NO on carbon and carbon-supported catalysts

The interactions of NO with carbon and carbon-supported catalysts have been investigated by means Fourier transform infrared spectroscopy. Nitric oxide direct decomposition over carbon-supported catalysts (Cu, Pt) was studied in a temperature ranging from 473 to 623 K. NO conversion increased with increasing reaction temperature in the whole temperature range. The carbon-supported Pt catalyst has a very high activity for the decomposition of NO in the absence of oxygen. As a result of NO chemisorption isocyanate (-NCO) species on the surface of carbon containing Cu were observed. When the reaction temperature was increased, the -NCO band at 2229 cm⁻¹ became more intense.     

Structure of carbon nanotubes probed by local and global probes

A review is proposed of different techniques available today for the characterization of the atomic structure of carbon nanotubes. This review covers the electron microscopies, various diffraction techniques, scanning probe microscopies, and optical spectroscopies, including Raman scattering. The advantages and limitations of the characterization techniques are discussed.     

基于WEB和C/S的教务管理系统的分析与设计

本文是以河南经贸职业学院教务管理工作实现网络化管理的需求为背景而展开讨论的。文中详细阐述了基于WEB和C/S模式相结合的总体设计方案,通过分析系统功能的需求,阐述了系统功能模块的设计思想。     

EBSD investigation of SiC for HTR fuel particles

Electron back-scattering diffraction (EBSD) can be successfully performed on SiC coatings for HTR fuel particles. EBSD grain maps obtained from thick and thin unirradiated samples are presented, along with pole figures showing textures and a chart showing the distribution of grain aspect ratios. This information is of great interest, and contributes to improving the process parameters and ensuring the reproducibility of coatings.     

抽余C_4烃中异丁烯催化逆流水合制叔丁醇

采用大颗粒离子交换树脂催化剂,在φ100mm×10m的反应器中进行了异丁烯催化逆流水合制叔丁醇的中间试验。考察了反应温度、水油体积比和抽余C4烃的流速等对异丁烯转化率的影响。试验结果表明,异丁烯催化逆流水合制叔丁醇的适宜操作条件为:反应温度80~90℃,水油体积比为4~5,抽余C4烃的流速为0.45~0.55mm/s。在此条件下,异丁烯的转化率可达88.8%。工业装置运转结果表明,异丁烯转化率大于75%。     

用C语言链表解决大整数运算的精度问题

介绍用C语言链表解决大整数运算的精度问题的方法。     

Prediction of the elastic behaviour of hybrid and non-hybrid woven composites

A micromechanical model called MESOTEX is presented for prediction of the elastic behaviour of composites reinforced with non-hybrid weave (plain weave, satin weave and twill weave) and hybrid weave (hybrid plain weave and hybrid twill weave) fabrics. By using the classical thin laminate theory applied to each woven structure, this analytical model takes into account the strand undulations in the two directions and also integrates the geometrical and mechanical parameters of each constituent (resin, fill and warp strands). A representative volume is chosen for each woven composite and the fibre architecture is described by several functions. To determine the effectiveness of this analysis, the elastic properties predicted for each woven composite are compared with experimental results and results extracted from the literature. This correlation shows excellent agreement between measured and predicted values, with a very low calculation cost (CPU time of less than 0·01 s).     

基于AP2DR2指挥信息系统的安全防护体系研究

本文首先介绍了指挥信息系统安全防护的基本概念和特点,然后从网络安全技术和网络安全管理等方面分析了如何实现指挥信息系统完全,提出了一种基于AP2DR2模型的指挥信息系统安全防护体系,论述了AP2DR2安全模型是一个多层次、全方位的动态防御体系,指挥信息系统安全防护体系从静态、被动向动态、主动转变,有效地保障了指挥信息系统信息的安全。