连续碳分CO2吸收率分析及探讨

本文简述了CO2 气体吸收率的测定原理 ,着重分析了影响连续碳分CO2 气体吸收率的因素 ,提出了提高连续碳分CO2 气体吸收率的途径     

形核剂成分对高碳钢凝固过程的影响

高碳钢连铸坯存在的最大质量问题是中心缩松、中心偏析严重.解决这一问题的关键是扩大铸坯等轴晶区比例,细化晶粒.本文以Fe-C合金作为形核剂,研究了形核剂含碳量对高碳钢凝固过程的影响机理.研究结果表明,向钢液中加入形核剂可有效地扩大等轴晶区.对高碳钢,中碳铁合金形核剂既可扩大等轴晶区,又可细化晶粒;而低碳形核剂可以扩大等轴晶区,但细化晶粒效果差.为有效地发挥形核剂的作用,对不同钢种要合理地选择形核剂含碳量.     

Resistance welding of carbon fibre reinforced polyetheretherketone composites using metal mesh and PEI film

Weldability of polyetheretherketone( PEEK) with polyetherimide( PEI) is tested. And carbon fiber reinforced PEEK laminates are resistance welded using stainless steel mesh heating element. The effects of the welding time and welding pressure on the lap shear strength of joints are investigated. Results show that PEEK can heal with PEI well in welding condition and the lap shear strength of PEEK/CF(carbon fibre) joint increases linearly with welding time, but reaches a maximum value when welding pressure ranging from 0.3 MPa to 0.5 MPa with constant welding time. The fracture characteristics of surface are analyzed by SEM techniques, and four types of fracture modes of lap shear joints are suggested.     

等离子体浸没离子注入改善45钢的摩擦学性能

采用灯丝放电和射频(RF)辉光放电等离子体浸没离子注入(PⅢ)工艺对45钢表面进行了氮离子注入强化处理。通过X射线光电子能谱(XPS)、扫描电子显微镜(SEM)、显微硬度、针-盘磨损和电化学腐蚀试验等测试手段，分析比较了经灯丝放电PⅢ和RF辉光放电PⅢ改性后试样表面元素的浓度分布、显微硬度、摩擦磨损性能和耐腐蚀性能。结果表明：不同条件下的氮离子注入均能提高45钢表面的显微硬度、耐磨性和抗腐蚀性能；且RF辉光放电PⅢ处理后试样的显微硬度提高了76．8％，摩擦系数下降到0．3，与灯丝放电PⅢ处理后的试样相比，其表面强化效果更加明显。     

K2ZrF6助浸SiC涂层碳纤维增强Al复合材料的研究

研究了用K_2ZrF_6助浸法制造C/Al复合材料的工艺和K_2ZrF_6的助浸机理结果表明:K_2ZrF_6处理后,C,Al间的润湿性仍比SiC,Al间的差C,Al间的润湿主要靠大量的界面化学反应、这使得复合材料的制造十分困难;而SiC、Al间的润湿靠微量的SiC在Al中的溶解K在纤维或涂层中的扩散也可能起助浸作用Al液在极短时间内对SiC涂层后的纤维束或纤维预制件浸渍良好同时,将基体Si合金化后,获得了完整的CF/SiC/Al界面,圆满解决了C/Al复合材料的界面相容性和制造中的问题     

硬质合金注射成形脱脂工艺与碳含量控制

将传统蜡基粘结剂和油＋蜡改进粘结剂体系分别与粒度为1．97μm的WC-8Co硬质合金粉末混合采用注射成形法制备了全致密高强度的硬质合金。研究了注射坯在Hz中的热脱脂工艺和溶剂脱脂与其后补充热脱脂工艺，和不同脱脂工艺对脱脂坯碳含量的影响。结果表明：油＋蜡改进粘结剂体系具有更好的热脱脂和溶剂脱脂行为。通过工艺优化和碳含量控制，在真空气氛下1400℃烧结80min制备出高抗弯强度的全致密硬质合金烧结制品。     

Chemically functionalized carbon nanotubes and their characterization using thermogravimetric analysis, fourier transform infrared, and raman spectroscopy

This article reports key findings on the chemical functionalization of carbon nanotubes (CNT). The functionalization of chemical vapor-deposited CNT was carried out by treating tubes with polyvinyl alcohol through ultrasonication in water with the aid of a surfactant. The surfactant is expected to promote the unbundling of aggregated CNT. The characterization of functionalized samples using thermogravimetric analysis, Fourier transform infrared spectroscopy, and Raman spectroscopy revealed that the CNT were functionalized by the interaction of carboxylic acid and hydroxyl groups. From the characterization studies, it is apparent that there is a strong interaction between these functional groups and the covalently bonded carbon in the CNT network. The functionalization process enabled good CNT dispersion in the solution, and the CNT remained in suspension for many days. To support the effective functionalization of the tubes, the interaction of functionalized CNT with Ni ions is also demonstrated. This paper was presented at the fourth International Surface Engineering Congress and Exposition held August 1–3, 2005 in St. Paul, MN.     

对接接头横向残余应力调控技术

分析了现有消除和调控焊接残余应力的常用措施所依据的原理，认为在不考虑材料相变的前提下，减轻对焊缝金属冷却收缩的制约可以有效地调控实际焊接接头上的残余应力。分析了纵向残余应力和横向残余应力之间的内在关系，在遵循虎史定律和考虑到金属形变时保持体积不变的前提下得出了纵、横向残余应力密切相关的推论，即横向残余应力也会影响纵向残余应力的值。在此基础上提出了减轻焊件自重引起的与焊接平台间的摩擦拘束以调控焊件中的横向残余应力的构想，并以Q235钢板为对象研究了采用该措施后平板对接接头纵、横向焊接残余应力的变化情况。试验结果表明，采取了减轻焊件自重引起的横向拘束的工艺措施后，板厚为8mm的试件上即获得焊接构件上的横向残余应力显著降低的结果。该措施对纵向残余应力亦有较大的影响，即减小横向残余应力的同时，接头上的纵向残余应力亦随之有所下降。     

Effects of oxygen and carbon on the magnetic properties and microstructure of Sm2Co17 permanent magnets

The research on the sintered Sm2Co17 permanent magnets prepared by metal injection molding is still at the exploratory stage. Carbon and oxygen are two key factors that influence the magnetic properties. In this article, the effects of oxygen and carbon on the properties and microstructure of the magnets have been studied. The results indicate that oxygen consumes the effective Sm content of the magnets and forms Sm2O3-the non-magnetism phase, which result in the deterioration of the magnetic properties. Besides, the magnetic properties decrease in evidence with increasing carbon content. The main factor that affects the magnetic properties is the deterioration of the microstructure of the magnets. The Sm（Co, Cu）5 phase decreases, whereas the cell size increases with the increase of the carbon content. When the carbon content is above 0.43 wt.%, the Sm（Co, Cu）5 phase is not enough to form a uniform cellular microstructure. Thus the magnetic properties disappear. ZrC is detected in the magnets by XRD when the carbon content is above 0.21 wt.%. ZrC also reduces the properties of the magnets.     

EFFECT OF MICROSTRUCTURE ON CORROSION FATIGUE BEHAVIOUR OF A LOW CARBON BAINITE STEEL

The behaviour towards corrosion fatigue of low carbon bainite steel with variousmicrostructures after tempered at different temperatures has been examined. The susceptibilityof the steel to corrosion fatigue may be improved by tempering at 300℃.