Preparation and characterization of electrospun,biodegradable membranes

Nonwoven, biodegradable membranes fabricated by electrospinning have recently attracted a great deal of attention for biomedical applications. In this study, microporous, nonwoven membranes of poly(L ‐lactide) and its copolymers and blends were fabricated through electrospinning. The structures and morphologies of the electrospun membranes were investigated with scanning electron microscopy, differential scanning calorimetry, and X‐ray diffraction. Different polymer membranes, incorporated with carmofur, were fabricated, and their drug release profiles were investigated. Scanning electron microscopy images showed that the fiber diameters were down to the nanometer range. The diameters and morphologies of thenanofibers depended on processing parameters such as the solution properties (concentration and polymer molecular weight), applied electric voltage, solution feeding rate, and needle diameter. Differential scanning calorimetry showed that the crystallinity of the electrospun membranes was lower than that of the cast film. For all the membranes incorporated with the drug, there was a burst release in the first 10 h of incubation in phosphate‐buffered saline at 37°C. Poly(glycolide‐co‐lactide) membranes showed faster and more complete drug release than poly(L ‐lactide), and this could be attributed to its faster degradation. The incorporation of polylactide–poly(ethylene glycol) could shorten the drug release time. A combination of suitable degradable biomaterials with an appropriate electrospinning process could be useful in the fabrication of a new kind of membrane suitable for different biomedical applications such as tissue engineering and drug delivery. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

离子液体/盐双水相萃取技术的研究进展

离子液体/盐双水相萃取技术是一种新型的双水相萃取技术。它具有传统双水相萃取技术所不具备的诸多优点。本文介绍了离子液体/盐双水相体系的类型和特点,综述了离子液体/盐双水相萃取技术在生物分离、天然有机物的提取、有毒物质处理中的应用,指出了该技术目前存在的问题并提出今后发展的展望。     

基于位并行DA结构的高速FIR滤波器

针对目前利用FPGA实现基于分布式算法(DA)FIR滤波器的不足,以及为了实现高速FIR滤波器,提出了一种位并行分布式算法结构的解决方案。采用位并行分布式算法和流水线式并行加法器树,在Xilinx Virtex5系列FPGA上实现了高速FIR滤波器。该滤波器工程经ISE 12.3综合、布局布线后,利用Modelsim SE 6.5和Matlab联合仿真。仿真结果表明,该设计可以提高滤波器处理速度,32阶的滤波器最高时钟频率可达到399.624 MHz。对滤波器进行进一步优化,节约了硬件资源占用。     

电弧喷涂技术在中国的发展和应用

电弧喷涂虽然不是一项新技术,随着电弧喷涂设备的改造和完善、新型喷涂材料的不断出现以及对电弧喷涂过程和涂层机理研究的深入,特别是电弧喷涂用管状丝材的开发和应用,使电弧喷涂技术得到越来越广泛的应用,成为最具有活力的热喷涂方法之一。在中国,电弧喷涂技术已成为最有效的钢结构长效防腐手段之一,另外,电弧喷涂技术在零部件修复和表面强化、电弧喷涂制模、锅炉水冷壁的抗热腐蚀、制造防滑涂层以及减磨涂层等方面得到了广泛应用。     

过程装备多媒体CAI应用软件的开发

以创作软件３ Ｄ Ｓｔｕｄｉｏ ４．０ 及 Ｍｉｃｒｏｓｏｆｔ Ｐｏｗ ｅｒｐｏｉｎｔ ９５ 与著作软件 Ａｕｔｈｏｒｗ ａｒｅ Ｐｒｏｆｅｓｓｉｏｎａｌ３．５ 为开发工具,开发了过程装备多媒体 Ｃ Ａ Ｉ应用软件,它涵盖了《化工设备设计》课程,并增加了生物流化床反应器等方面的内容,动画效果逼真、生动、形象地反映了单元操作设备零部件之间的结构关系。完善的交互设计,界面设计和导航设计极大地方便了用户的使用,尤其适合于课堂教学。     

Low-cycle fatigue strength of 10GN2MFA steel with a single-layer corrosion-resisting coating produced by electroslag strip cladding

The method of testing the uniform single-layer corrosion resisting coating, produced by electroslag strip cladding on 10GN2MFA steel, on the resistance to low-cycle fatigue strength using special specimens is described. Tests were carried out at a temperature of 20 °C with the symmetric axial tension–compression loading cycle (R_e = –1) with the given amplitude of the parent and cladding metal. The tests were carried out in the strain amplitude range ε_a = 0.28–0.8%, the number of cycles to the initiation of a crack was N_i = 340–16,000 cycles, loading frequency f = (0.25–2.0). The area of formation of the cracks was recorded in the experiments. In most cases, the cracks formed in the heat-affected zone in the vicinity of the fusion line and propagated in both the parent and deposited metal. The results show that in the range of low-cycle fatigue for the investigated 10GN2MFA steel with a deposited layer, the calculation coefficient of the decrease of the cyclic strength of the metal with a deposited layer in relation to the fatigue curve for the carbon and alloyed steel with 0.8 ≤ σ_0.2/σ_B ≤ 0.9, the value φ_S = 0.68 should be used in the calculations.     

贵溪冶炼厂硫酸二系列的仪表控制系统

介绍了贵溪冶炼厂硫酸二系列的技术特点、工艺流程及其集散系统的主要检测、控制点,并对冶炼烟气的分配,动力波洗涤器液位的测量,主鼓风机的联锁运行及全厂的联锁运行进行了说明。     

批量旋转混料机的研制及应用

介绍了批量旋转混料机的结构、性能与工作原理,以及正立方体混合室的翻转、推拉作用,使室内多组分聚合物在非熔融状态下的扩散,更换位置,以达到各组分混合物趋于均匀,即分布混合的目的。     

Optical fiber distributed acoustic sensing based on the self-interference of Rayleigh backscattering

In order to detect the weak underwater acoustic signal, a Distributed Acoustic Sensing (DAS) scheme based on the self-interference of Rayleigh backscattering is presented. Rayleigh backscattered light which contains a phase change induced by acoustic signal along the sensing fiber which is a standard telecom single-mode fiber is split and fed into an imbalance Michelson interferometer. With the self-interference of two Rayleigh backscattered beams, the phase change is amplified theoretically compared with phase-sensitive OTDR. We designed an experiment to prove the scheme, and successfully restored the acoustic information, meanwhile, the DAS system has preliminary realized around the acoustic phase sensitivity of −151 dB (re rad/μPa) at 600 Hz, and the minimum detectable acoustic pressure of 6 Pa in the experiment.     

少齿差行星齿轮齿根弯曲应力计算方法研究

少齿差齿轮副在啮合时由于轮齿受载产生变形可能引发多对齿同时接触承载的情况[1],啮合齿对实际承担的载荷将下降。少齿差齿轮副啮合时存在多对齿同时接触承载的现象,且由于内外齿轮齿廓的凹凸曲率非常接近,啮合时齿面接触面积较大,接触力为分布力,在计算齿根弯曲应力时不宜按集中力处理,这些情况使得准确计算少齿差齿轮副的齿根弯曲应力变得复杂。现以大量有限元计算分析为基础,综合考虑多对齿同时接触承载这一情况,建立了适用于少齿差齿轮副齿根弯曲应力的计算方法,并进行了实验验证。