HIPPI效率分析及程序实现

本文对ＨＩＰＰＩ的静态数据传输效率进行了分析，并阐述了在ＩＲＩＳ上的ＨＩＰＰＩ驱动程序实现的有关问题。     

高灵敏度单波长激发能量色散X射线荧光光谱法测定铜精矿中16种组分

铜精矿技术条件中要求的组分覆盖范围从主量、常量、微量到痕量,要使用一种检测技术同时测定这些组分是铜精矿测定的难题。单波长激发能量色散X射线荧光光谱仪,采用双曲弯晶全聚焦技术,将X射线连续谱单色化,降低了连续谱背景,改善检出限,提高灵敏度,对组分的检测范围可覆盖主量到痕量。实验基于高灵敏度单波长激发能量色散X射线荧光光谱法(HS-EDXRF)结合快速基本参数法建立了铜精矿中主量组分Cu、S、Fe、SiO₂,常量组分CaO、MgO、Al₂O₃,微量和痕量组分Zn、Ni、Cr、Pb、Sb、Cl、Ag、As、Bi等16种组分的分析方法。采用实验方法测定铜精矿样品,结果与标准方法或经典分析方法结果对比,无显著性差异(t_0.05,82值均小于1.98)。此外,主量组分Cu、S、Fe、SiO₂测定结果的相对标准偏差(RSD,n=7)不大于0.70%,常量组分CaO、MgO、Al₂O₃的RSD小于1.6%,微量组分Zn、Ni、Cr、Pb、Sb、Cl的RSD不大于3.3%,痕量组分Ag、As、Bi等的RSD均小于10%。方法可满足铜冶炼工艺对铜精矿中16种组分的检测需求。     

基于SETP7和WinCC结构下的SOE 1ms功能的实现

本文介绍了基于STEP7和WinCC结构下的SOE 1ms功能的实现。     

超高效液相色谱-串联质谱法测定土壤、蔬菜及水果中苯醚甲环唑和丙环唑残留

建立了超高效液相色谱-串联四极杆液质谱联用(UPLC-MS/MS)检测土壤、番茄、茄子、梨和香蕉中苯醚甲环唑和丙环唑的残留分析方法.样品采用乙酸乙酯提取,弗罗里硅土固相萃取柱净化,超高效液相色谱分离多反应监测模式下测定,外标法定量.结果显示:苯醚甲环唑和丙环唑的线性关系良好.苯醚甲环唑和丙环唑在不同基质中平均回收率分别为79.7%～107.1%和72.8%～104.6%,相对标准偏差分别为0.7%～13.1%和2.7%～18.9%.最低检出质量分数均为0.001 mg/kg.     

光纤MEMS法布里-珀罗压力传感器的准分布式测量

提出了一种基于傅立叶解调法的空分复用系统,实现了光纤微机电系统（M icroE lectroM echan ical System,MEMS）法-珀（FP）压力传感器的准分布式测量.传感器基于FP腔干涉的原理,采用MEMS技术加工制作,用傅立叶方法解调干涉信号,用光开关实现传感器复用.理论分析与实验验证了传感器解调和复用的基本原理.结果表明,该系统具有好的线性、灵敏度、精度和重复性,响应速度快,复用的传感器间无明显串扰,系统复用能力取决于光开关的通道数.     

Real-time pixel based early apple bruise detection using short wave infrared hyperspectral imaging in combination with calibration and glare correction techniques

High speed data processing for online food quality inspection using hyperspectral imaging (HSI) is challenging as over hundred spectral images have to be analyzed simultaneously. In this study, a real-time pixel based early apple bruise detection system based on HSI in the shortwave infrared (SWIR) range has been developed. This systems consists of a novel, homogeneous SWIR illumination unit and a line scan camera. The system performance was tested on Jonagold apples bruised less than two hours before scanning. Partial least squares-discriminant analysis was used to discriminate bruised pixel spectra from sound pixel spectra. As the glossiness of many fruit and vegetables limits the accuracy in the detection of defects, several reflectance calibrations and pre-processing techniques were compared for glare correction and maximizing the signal to noise ratio. With the best combination of first derivative and mean centering, followed by image post-processing, this system was able to detect fresh bruises in thirty apples with 98% accuracy at the pixel level with a processing time per apple below 200 ms.     

基于模式增长的不确定数据的频繁模式挖掘算法

为提高不确定数据频繁模式(FP)挖掘算法的时空效率,提出了基于最大概率的不确定频繁模式挖掘(UFPM-MP)算法。首先,利用事务项集中的最大概率值预估期望支持数;然后,使用该期望支持数与最小期望支持数阈值进行比较,以确定某一项集是否为候选频繁项集,并对候选项集建立子树以递归挖掘频繁模式。实验中,UFPM-MP算法与AT-Mine算法进行了对比,并在6个典型的数据集上进行实验验证。实验结果表明,UFPM-MP算法的时空效率得到了提高,稀疏数据集上提高约30%,稠密数据集上的效率提高更为明显(约3~4倍)。预估期望支持数的策略有效地减少了子树和头表项的数量,从而提高了算法的时空效率;且最小期望支持数越小,或需要挖掘的频繁模式越多的时候,算法的时间效率提高越多。     

一种新的微波/毫米波产生方法

提出一种新的微波/毫米波光产生方法,将激光脉冲入射到单模光纤FP腔中,激发腔中的两个本征模,利用两本征模相位失谐与光外差方法得到微波/毫米波信号,得出单模光纤FP腔结构参数与微波/毫米波信号频率间的关系表达式。数值计算表明：调制频率为25 MHz的脉冲激光入射到单模光纤FP腔时,可得到频率为2.083 GHz的微波信号。通过调节FP腔内的双折射强度,可得到从微波到毫米波的信号。该方案只需一个激光光源,成本低、可靠性高、稳定性好。     

基于特征挖掘的电网故障诊断方法

专家系统在应用方面的主要瓶颈是:规则库的维护;推理的速度和准确度的协调。分析了故障信息序列中必有或特有的信息,提出了基于特征挖掘的关联规则挖掘方法。结合电网故障信息的特征,改进了频繁模式(frequent pattern,FP)–算法:考虑了故障信息的特征,如时序和因果关联关系、故障性质、严重故障、稀有故障等因素;增加了规则的或逻辑;改进了FP-树的修剪技术。算例表明该算法能够大量减少无效挖掘,推理速度和准确度显著提高,适用于在线诊断。     

Evaluation of the anti-fouling properties of nm thick atmospheric plasma deposited coatings

Both organic and inorganic fouling are significant problems for stainless steel surfaces used in industrial applications as diverse as shipping and paper making. The objective of this study is to evaluate the anti-fouling properties of a range of fluoropolymer, fluorinated and non-fluorinated siloxane coatings on stainless steel substrates. These nm thick coatings were deposited using the atmospheric plasma jet system called PlasmaStream™. The surface properties of the plasma polymerised coatings were examined using optical profilometry, SEM-EDX, ellipsometry, contact angle measurement and FTIR. Accelerated wear testing of the coated heat exchangers indicated that coating durability was a significant issue for the nanometre thick coatings investigated. A crystallization fouling study was carried out using a laboratory scale heat exchanger test apparatus. In this the heated steel surface was in contact with flowing fluid containing CaCO₃ particles. The coated steel exhibited both a delay before fouling was initiated and in addition a decrease in the fouling rate. A lubricant oil fouling study was also carried out involving a comparison between both coated and uncoated stainless steel separator discs over a 30 day period, in the engine of a passenger ferry. A significant reduction in the level of oil fouling was observed for the fluorosiloxane and fluoropolymer coated separator discs compared with the uncoated discs.