An International Collaborative Study on Trypsin Inhibitor Assay for Legumes,Cereals, and Related Products

For determining trypsin inhibitor activity (TIA) in soy products, the American Oil Chemists' Society (AOCS) Method Ba 12-75 has been used. It measures differences in absorbance at 410 nm of bovine trypsin activity toward a synthetic substrate (Nα-benzoyl-DL-arginine-p-nitroanilide) in the absence and presence of an inhibitor. Recently, a significantly improved method was developed (JAOCS, 2019, 96:635–645), featuring 5 mL of total assay volume, enzyme-last sequence, and single inhibitor level in duplicate. It is proposed as the AOCS Method Ba 12a-2020. As a part of the AOCS method approval process, a collaborative study involving 12 international laboratories was conducted to evaluate the performance of the proposed method. The study involved measuring TIA in 10 selected test samples plus a blind duplicate. They included soybeans, pulses, cereals, and their processed products (flours, concentrates, and isolates). After rigorous statistical treatment of the data, only three outliers were removed from the data of two samples. Repeatability relative standard deviations (RSDr) for the 11 samples ranged from 0.99% to 5.52%. Reproducibility RSD (RSD_R) ranged from 7.07% to 22.92%, with seven samples having RSD_R around 10% or less. The remaining four samples had very low TIA, and their RSD_R values ranged from 13.34% to 22.92%. The study has demonstrated reliable performance of the proposed AOCS method. Several collaborators carried out additional experiments addressing some aspects of the method, leading to further refinements. The proposed method is undergoing evaluation by the AOCS Uniform Methods Committee for adoption as an Official Method for measuring TIA in various legume and grain products.     

电化学法处理废硬质合金直接回收金属钴和碳化钨

首次采用电化学法处理废硬质合金直接回收金属钴和碳化钨，工艺简单可靠，具有较好的环境和经济效益。     

车用空调器压缩机前端板铸件壳型铸造工艺实践

对前端板铸件壳型铸造中存在的铸造缺陷,采用优化浇注系统,对铁水进行二次孕育处理,调整碳当量控制在3.90%~4.15%,硅含量降低0.15%~0.20%,使产品抗拉强度≥270MPa,硬度(HB)为187~241,满足用户要求。     

倾斜板角度对亚共晶高铬铸铁半固态组织的影响

采用倾斜板冷却体法对亚共晶高铬铸铁进行半固态成形,研究了倾斜板角度对亚共晶高铬铸铁半固态组织的影响规律。结果表明:倾斜板角度过大或过小都将使得组织中的初生奥氏体较粗大、圆整度较小。当倾斜板角度较小时,金属液的流速相对较慢,枝晶与枝晶和枝晶与金属液间的冲刷、碰撞、剪切作用较小,晶粒易于长大,导致枝晶状初生奥氏体比较多。当倾斜板角度较大时,金属液流速相对较快,金属液在倾斜板上流动的时间相对较短,枝晶间以及枝晶与金属液间的冲刷、碰撞、剪切作用时间相对较短,导致枝晶状初生奥氏体也比较多。当倾斜板角度为45°时,制备的亚共晶高铬铸铁初生奥氏体的尺寸最小,圆整度最高。     

热处理工艺对高速钢轧辊组织和性能的影响

研究了淬火温度、冷却方式、回火温度和回火次数对高速钢轧辊组织和性能的影响。结果表明,空冷的高速钢轧辊淬透性差,油冷的高速钢轧辊易出现裂纹,盐冷的高速钢轧辊具有优良的淬透性,不易出现裂纹,辊面硬度高,硬度均匀性好,耐磨性好。     

粉煤灰颗粒增强铝基复合材料的研究

采用粉末冶金法成功制备了煤粉灰颗粒增强铝基复合材料。煤粉灰颗粒大多为球形,密度为2.75g/cm3,颗粒直径主要集中在5～60μm范围内,主要成分为SiO2、Al2O3和Fe2O3,三者质量分数总和超过85%。经SEM分析表明,该复合材料中存在着颗粒团聚,并有少量气孔产生。随着煤粉灰质量分数的增加,复合材料的密度逐渐减少;当煤粉灰颗粒的质量分数在10%以下时,该复合材料的硬度是上升的,超过10%时硬度开始下降。     

Control of material flow in a combined backward can - forward rod extrusion

The paper deals with an analysis of an extrusion process with a divided material flow. As we are forced to seek for optimal technological solutions with short testing times and low risks and costs, a reliable process evaluation is of the greatest importance.

The paper discusses the influences of tool geometry, friction and lubrication as well as workpiece properties on balanced material flow in a combined extrusion process. The FEM analysis applying the DEFORM code has been used in order to predict the process parameters and to estimate its stability. The subsequent experimental verification has resulted in a conclusion that modern computer aided tools, tuned by proper experimental sets, can be used for fast and reliable cold metal forging process planning.     

仙居抽水蓄能电站下水库事故闸门井深井开挖技术

仙居抽水蓄能电站下水库泄放洞事故闸门井开挖施工作业面狭窄、安全隐患大,经方案比选,采用"先导井后扩挖"方式进行开挖。其中导井开挖采用VCR法,具有作业安全、施工进度快、爆破成型效果好等优点,取得了较好的经济效益。     

基于有限元法的E-K模型参数敏感性分析

模型参数的确定是数值分析过程中的重要环节,合理把握参数的选取原则,可大大提高结构分析的可靠度以及参数反分析的计算效率.本文借助有限单元法考察了E-K模型参数变化对一个均质堤坝的位移和应力值的影响程度.通过分析明确了E-K模型中各参数对计算结果的敏感程度,同时提出了模型参数的选取原则.