基于光电码盘的高精度电机转速测量

近终形连续铸轧技术是以转动的铸轧辊为结晶器，直接生产薄带的新技术；用80C552单片机和光电码盘配合改进的M／T法，检测铸轧辊的执行电机转速可获得大范围内测速精度。介绍了该测速法的基本原理、实现步骤和软硬件设计。     

Decellularization of Human Pancreatic Fragments with Pronounced Signs of Structural Changes

A significant lack of donor organs restricts the opportunity to obtain tissue-specific scaffolds for tissue-engineering technologies. One of the acceptable solutions is the development of decellularization protocols for a human donor pancreas unsuitable for transplantation. A protocol of obtaining a biocompatible tissue-specific scaffold from decellularized fragments with pronounced human pancreas lipomatosis signs with preserved basic fibrillary proteins of a pancreatic tissue extracellular matrix was developed. The scaffold supports the adhesion and proliferation of human adipose derived stem cell (hADSCs) and prolongs the viability and insulin-producing function of pancreatic islets. Experiments conducted allow for the reliance on the prospects of using the donor pancreas unsuitable for transplantation in the technologies of tissue engineering and regenerative medicine, including the development of a tissue equivalent of a pancreas.     

Mechanical Properties of TC11 Titanium Alloy and Graphene Nanoplatelets/TC11 Composites Prepared by Selective Laser Melting

Titanium matrix composites (TMCs) with excellent mechanical properties, reinforced by graphene, is deemed the lightweight and high strength structural materials. In this study, TC11 titanium alloy powder and graphene nanosheets (GNPs) were used as raw materials, and the composite powder with good uniformity and fluidity was obtained through non-interventional homogeneous mixing by a planetary mixer. The microstructure and mechanical properties of the GNPs-TC11 composites and TC11 alloy were compared. The results showed that the microstructure of TC11 and the composites was acicular martensite α’ phase under the process parameters of 280 W laser power, 1200 mm/s scanning speed, and 0.1 mm hatch spacing. The GNPs in addition, in the composites, reduced the acicular martensite particle size and expanded the proportion of low-angle grain boundaries. The tensile strength and percentage elongation after the fracture of the TC11 titanium alloy were 1265 MPa and 4.3%, respectively. Because of addition of the GNPs, the strength and percentage elongation after the fracture of the composite increased to 1384 MPa and 8.1%, respectively, at a GNPs mass content of 0.2%. The enhancement of mechanical properties can be attributed to grain refinement, dislocation strengthening, Orowan strengthening, and load transfer strengthening.     

Evaluation of the performance of metameric indices

Forty three metameric pairs were obtained by comparison, shade-adjustment, and redyeing of 660 self shades dyed with direct, azoic, vat, and reactive dyes. The pairs were regrouped shadewise and ranked visually in increasing order of metamerism. Spearman's rank correlation coefficients were calculated between 11 measures of metamerism and the visual metameric ranking under three illuminants A, D65, and TL84 in pairs. The illuminant-independent general indices included the indices based on reflectance differences (Bridgeman), weighted reflectance differences (Nimeroff and Yurow), Cohen-Kappauf's residual differences (proposed) obtained from the spectral decompositions of the reflectance spectra of the metameric pair. Illuminant-specific special indices included color-differences under test illuminant, addition, subtraction, division, and multiplication of color-differences under test and reference illuminants, indices based on ΔL*, Δa*, Δb* differences under two illuminants, based on chromatic adapted ΔL*, Δa*, Δb* differences with multiplicative corrections for tristimulus differences under reference illuminant (Berns-Billmeyer), differences of the color constancy indices. The present work showed that indices based on ΔL*, Δa*, Δb* differences under two illuminants, both unmodified and modified by Berns-Billmeyer performed best among the existing indices. The differences of color constancy indices showed good correlation with the degree of metamerism in some cases, and this may be utilized for developing newer indices of metamerism. © 1996 John Wiley & Sons, Inc.     

提升管反应器中颗粒浓度径向分布的力学特性

采用空气动力学中的Kutta-Joukowski升力定理分析了提升管内颗粒的受力,得到了Kutta-Joukowski力FK-J的计算公式FK-J=ρg(vg,Z-vp,Z)(?vp,Z/?r)r.根据在大型冷模实验装置上由PV-6D型颗粒密度两用仪测量的局部固含率和颗粒速度径向分布的实验数据,计算了Kutta-Joukowski力在提升管内的分布特征,分析了颗粒循环量、表观气速、轴向位置对其径向分布的影响.结果表明,当无因次半径r/R=0时,FK-J=0,在r/R=0.85时,FK-J最大;FK-J随颗粒循环量增大而增大,表观气速对FK-J的径向分布没有显著影响;在提升管内的充分发展段FK-J的数值明显大于提升管加速区和出口约束区.由实验数据回归出了提升管内FK-J径向分布的经验关联式,计算值与理论值吻合较好.     

Immunohistochemical Evaluation of Periodontal Regeneration Using a Porous Collagen Scaffold

(1) Aim: To immunohistochemically evaluate the effect of a volume-stable collagen scaffold (VCMX) on periodontal regeneration. (2) Methods: In eight beagle dogs, acute two-wall intrabony defects were treated with open flap debridement either with VCMX (test) or without (control). After 12 weeks, eight defects out of four animals were processed for paraffin histology and immunohistochemistry. (3) Results: All defects (four test + four control) revealed periodontal regeneration with cementum and bone formation. VCMX remnants were integrated in bone, periodontal ligament (PDL), and cementum. No differences in immunohistochemical labeling patterns were observed between test and control sites. New bone and cementum were labeled for bone sialoprotein, while the regenerated PDL was labeled for periostin and collagen type 1. Cytokeratin-positive epithelial cell rests of Malassez were detected in 50% of the defects. The regenerated PDL demonstrated a larger blood vessel area at the test (14.48% ± 3.52%) than at control sites (8.04% ± 1.85%, p = 0.0007). The number of blood vessels was higher in the regenerated PDL (test + control) compared to the pristine one (p = 0.012). The cell proliferative index was not statistically significantly different in pristine and regenerated PDL. (4) Conclusions: The data suggest a positive effect of VCMX on angiogenesis and an equally high cell turnover in the regenerated and pristine PDL. This VCMX supported periodontal regeneration in intrabony defects.     

改进型四波束Butler矩阵的幅度加权

在4×4Butler矩阵基础上,在保持波束数目和指向不变的情况下,通过增加4个功分器和4个180^。移相器,对矩阵进行改进。将天线阵列扩展为8单元线阵,并对改进后的矩阵进行近似切比雪夫分布幅度加权,仿真结果表明加权后副瓣电平明显改善,最后对半功率覆盖范围和波束交叉电平的影响进行分析。     

高性能铝基复合材料的设计与加工技术

从铝基复合材料微观结构特征与性能关系角度,回顾了承载结构用典型铝基复合材料在体系设计、制备与成型加工研究方面的成果与进展,同时简要介绍了近期铝基复合材料为实现性能突破所开展的研究探索,最后根据铝基复合材料的发展历程与现有研究的特点对铝基复合材料今后的研究应用进行了展望。     

新型基质分散挤压萃取-高效液相色谱法测定辣椒粉中6种苏丹红色素

目的 建立新型基质分散挤压萃取-高效液相色谱法(matrix dispersion squeezing extraction-high performance liquid chromatography, MDSE-HPLC)测定辣椒粉中苏丹红色素的方法。方法 样品与分散剂混匀后、加入提取剂充分研磨,通过挤压收集提取溶剂,经Al2O3固相萃取柱净化,采用高效液相色谱法进行检测,外标法定量。结果 6种苏丹红色素在1.20~9.60 μg/g浓度范围内具有良好的线性关系,相关系数均大于0.9989,方法检出限为0.10~0.15 μg/g,定量限为在0.30~0.45 μg/g范围内。样品在3个水平加标浓度(1.0、5.0、10.0 μg/g)下的平均回收率为72.0%~102.4%,相对标准偏差为1.9%~6.8%。结论 本方法简单新颖、成本低、污染少,能快速有效提取目标物,准确度和精密度符合要求,可用于辣椒粉中的6种苏丹红色素的检测。     

硼酸对FAAS法测定硅质材料中微量铁的基体改进效应的研究

火焰原子吸收法(简称FAAS)测定硅质材料中的微量铁,采用硼酸为基体改进剂,消除了测定铁时大量硅的干扰,扩大了测微量铁的应用范围。方法具有准确度好、检出限低、分析速度快、操作方便等优点。加标回收率96·0%~101%,线性范围0%~10·5μg/mL,灵敏度0·19μg/mL,检出限77ng/mL,相对标准偏差小于2·2%