Second Generation Nanostructured Metal Oxide Matrices to Increase the Thermal Stability of CO and NO2 Sensing Layers Based on Iron(II) Phthalocyanine

An iron(II) phthalocyanine (FePc) complex solubilized by decylamine (DA) and benzylamine (BA) is incorporated into a nanoparticulate metal oxide matrix to develop optical sensor films sensitive to NO₂ and CO. Eleven amine solvents have been tested as N‐donor ligands that permit ligand exchange with the gas molecules. We have systematically investigated the suitability of different N‐donor ligands, studied the thermal stability of the NO₂‐ and CO‐sensing films at 4, 25, 60, and 80 °C by photometry, and corroborated our findings by using NMR experiments. A satisfactory thermal stability of the films has not been obtained for chemically unmodified nanoparticulate metal oxide matrices. We have therefore developed a second generation of nanostructured metal oxide supports that show increased thermal stability and adequate sensitivity to NO₂ and CO. These novel nanostructured matrices have been chemically modified using amines, alumina oligomers, and/or anti‐gas‐fading agents. These components have been integrated into the metal oxide matrices to avoid degradation of the optical films and to preserve their sensitivity.     

微点焊技术在薄膜基板焊接中的应用

概述微点焊接的工作原理和技术特点,以及用于薄膜铂电阻温度传感器中的薄膜基板上细小金属引线的微点焊技术。     

判断金属/薄层半导体欧姆接触质量的一个新方法

提出了一个判断金属／薄层半导体欧姆接触质量的新方法－－环内圆形传输线模型外的支,样品制备简单,无需台面绝缘,测试局域在很小的圆环内无需考虑圆环外的任何边界影响,由于结构的对称性,消除了侧向电流聚集效应,通过测试值的直线拟合消除了部分偶然误差,提高了精度。     

聚焦离子束曝光技术

聚焦离子束技术是一种集形貌观测、定位制样、成份分析、薄膜淀积和无掩模刻蚀各过程 于一身的新型微纳加工技术。它大大提高了微电子工业上材料、工艺、器件分析及修补的精度和速 度,目前已经成为微电子技术领域必不可少的关键技术之一。对聚焦离子束曝光技术作了介绍。     

深入探讨沉锡表面变色的问题

近年来,电子产业无铅化在迅速推进,PCB表面处理工艺也在向无铅化迅速发展。作为无铅表面工艺的一种,沉锡因其优良的可靠性在众多工艺中占有一席之地。但是,锡面回流变色问题却是一个顽疾。关于锡面回流变色,业内普遍认为是水洗质量不佳、药水残留导致,而系统深入地研究很少。本文由生产实际出发并结合相关试验测试,从金属氧化的角度,对锡面变色的机理进行了深入分析与独特探讨,找到关键影响因素,为改善这一问题提供切实有效的理论依据。     

一种新型校车智能监控终端的设计

近年来不断发生的校车事故引发了全社会对校车安全的普遍关注,本文设计了一种校车智能监控终端的设计方案,该系统要包括GPS定位模块设计、RFID无线射频识别模块设计,音视频模块接口模块设计、CAN总线接口模块、3G无线传输接口模块设计、存储模块设计、提醒及报警模块设、电源模块设计以及基于ARM9的控制平台等。本设计采用实时性高的ARM9处理器芯片作为控制器的核心,提高车载智能终端的同时,维护预期目标的设计理念,能够保证各个终端信息同时满足客户需求。     

Development, implementation, and testing of fault detection strategies on the National Wind Technology Center’s controls advanced research turbines

The National Renewable Energy Laboratory’s National Wind Technology Center dedicates two 600 kW turbines for advanced control systems research. A fault detection system for both turbines has been developed, analyzed, and improved across years of experiments to protect the turbines as each new controller is tested. Analysis of field data and ongoing fault detection strategy improvements have resulted in a system of sensors, fault definitions, and detection strategies that have thus far been effective at protecting the turbines. In this paper, we document this fault detection system and provide field data illustrating its operation while detecting a range of failures. In some cases, we discuss the refinement process over time as fault detection strategies were improved. The purpose of this article is to share field experience obtained during the development and field testing of the existing fault detection system, and to offer a possible baseline for comparison with more advanced turbine fault detection controllers.     

CONTINUOUS FERMENTATION OF GLUCOSE SOLUTIONS

Use of a continuous-flow plug fermentor to ferment glucose solutions was found to be possible only with unrefined commercial glucose and not with pure glucose. Even when the former was used problems were encountered due to a gradual increase in back pressure across the yeast bed. With the commencement of glucose metabolism in the yeast bed, ‘shock’ excretion of potassium and magnesium ions as well as of low molecular weight nitrogenous material was observed. The product from the fermentor contained an abnormally high level of α-diketones viz., 1–3 mg/litre.     

铁型覆砂铸造球墨铸铁曲轴

介绍了铁型覆砂铸造球墨铸铁曲轴的工艺,并就推广应用中发现的铸造缺陷提出了防止措施.