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61.
The interaction of different metal oxides such as Co3O4, NiO, Al2O3, Cr2O3, Fe2O3 and SiO2 with Na2SO4 at a temperature of 1100 and 1200 K in flowing oxygen has been studied. The thermogravimetric studies for each system were
carried out as a function of Na2SO4 in the mixture. The presence of different constituents in the reaction products were identified by X-ray diffraction analysis
and the morphologies of the reaction products were characterized using metallography and scanning electron microscopy (SEM).
The formation of products was also investigated by thermodynamic computation of free energies of the reactions and the study
of relevant equilibrium phase diagrams. The soluble species in the aqueous solutions of the reaction products were determined
quantitatively using atomic absorption spectrophotometry.
The high temperature interaction products usually contain a 3-phase structure namely, Na2O·M2O
x
, M2O
x
and metal sulphide and/or metal sulphate. The formation of Na2O·M2O
x
depends upon the solid state solubility of metal oxide in the molten salt at high temperatures. Under limited solubility
conditions Na2O·M2O
x
is invariably formed, but as soon as this condition is relaxed the oxide. M2O
x
, precipitates and forms a separate phase. 相似文献
62.
63.
中央空调系统水泵变频应用中存在的几个问题 总被引:3,自引:0,他引:3
本文分析了中央空调系统中水泵变频及其运行管理方面所存在的影响节能效果与运行管理质量的几个主要问题 ,提出了相应的解决办法 ,并对中央空调系统水泵变频决策与运行管理提出了几点建议。 相似文献
64.
65.
66.
Lithium-ion batteries are becoming more and more important not only for portable electronic devices, but also in prevision of high power electric vehicles. In such an optic, deep studies regarding all the components of a secondary battery are in development. In this study, high voltage cathode materials have been selected. Crystals with spinel structure have a 3D vacancy pathway suitable for Li-ions transport. The material under study was LiNi0.5Mn1.5O4 doped with magnesium replacing the nickel. Various samples were synthesized via three different routes: a solid-state method, a modified sol–gel method and a xerogel method. The structure and morphology of the powders were analyzed with HRTEM and XRD. Electrochemical tests were also performed. A wide range of particle sizes (from micro to nanosize) was the result of the different synthesis routes. Unfortunately pure materials were not always obtained. The electrochemical tests showed improvement of the material's cyclability, by reducing the particle size. The electrochemical tests further confirmed the existence of a Li1+dMn2−dO4 impurity. The results are quite promising, however, further improvement of the purity of the electrode composition are needed. 相似文献
67.
Koji Yamada Noboru Miura Chihiro Hamaguchi Norihiko Kamata 《Solid-state electronics》1989,32(12):1113-1117
Hot carrier magnetophonon resonances of n-type Si, short channel InP and p-type InSb were investigated in pulsed high magnetic fields up to 40 T. Using a recently developed high resolution technique in pulsed high fields, many new features of the hot carrier-phonon interactions in high magnetic fields were found. 相似文献
68.
房间空调器高效节能技术分析 总被引:2,自引:0,他引:2
周彬 《制冷与空调(北京)》2003,3(4):44-46
本文主要介绍了高效节能型空调器的优化设计,包括选用高效压缩机、增大换热面积,增大风量、管路的合理设计,旨在提高制冷量,降低功耗,提高能效比。 相似文献
69.
70.