Yttrium sol–gel coating effects on the cyclic oxidation behaviour of 304 stainless steel

The present results reveal the interest of sol–gel coating technique to improve 304 steel high temperature oxidation resistance. An yttrium sol–gel coating appears to enhance the oxidation resistance during isothermal oxidation test, to decrease widely the oxide weight gain and to reduce the initial transient oxidation stage generally observed in the case of blank steels. Moreover, the experimental results confirm that yttrium sol–gel coating also plays a significant role on the cyclic oxidation behaviour of the 304 steel. In fact, the yttrium addition promotes remarkably the prolongation of the period during which the oxide scale still remains adherent to the substrate.     

贯彻食用盐新标准 做好食用盐质量检测

介绍了食用盐新国标制定的指导思想，新标准的特点及所修订的内容，指出为做好食用盐的质量检测要掌握和控制的技术要点，以保证和提高盐质分析结果的准确度，确保食用盐产品质量符合标准要求。     

In Situ Formation of a Novel Nanocomposite Structure Based on MCM-41 and Polyethylene

M41S materials are prepared by in situ assembly of inorganic precursors and organic template and can be viewed as nanocomposites of the siliceous phase and organic surfactant. Calcination of these precursors gives the M41S materials that have been used to prepare novel nanocomposite structures, in which the organic phase inside the nano-sized pores is isolated by the nano-sized inorganic pore walls. The nanocomposite structures can be formed by in situ polymerization of monomers inside the channels. Polymerization of ethylene takes place inside the nano-sized pores, producing the desired nanocomposite structure. The resulting polyethylene was found to be a mixture of crystalline and amorphous phases.     

长脉冲激光沉积原位生成YBaCuO超导膜

用长脉冲激光(脉冲宽度150μs,波长1.06μm)辐照高温烧结的YBa_2Cu_3O_(7-x)靶,在6Pa的氧气压强下,巳在(100)YSZ单晶衬底上原位生成YBa_2Cu_(?)O_(7-x)超导膜。衬底置于750℃的加热器上,衬底与靶之间的距离5cm,用该法制得的薄膜光亮坚实,正常态呈金属性,零电阻温度为84.7K。用XRD和SEM对薄膜进行了分析研究。     

Atmospheric and low pressure shadow masked MOVPE growth of InGaAs(P)/InP and (In)GaAs/(Al)GaAs heterostructures and quantum wells

The shadow masked growth technique is presented as a tool to achieve thickness and bandgap variations laterally over the substrate during metalorganic vapor phase epitaxy. Lateral thickness and bandgap variations are very important for the fabrication of photonic integrated circuits, where several passive and active optical components need to be integrated on the same substrate. Several aspects of the shadow masked growth are characterized for InP based materials as well as for GaAs based materials. Thickness reductions are studied as a function of the mask dimensions, the reactor pressure, the orientation of the masked channels and the undercutting of the mask. The thickness reduction is strongly influenced by the mask dimensions and the reactor pressure, while the influence of the orientation of the channels and the amount of undercutting is only significant for narrow mask windows. During shadow masked growth, there are not only thickness variations but also compositional variations. Therefore, we studied the changes in In/Ga and As/P ratios for InGaAs and InGaAsP layers. It appears that mainly the In/Ga-ratio is responsible for compositional changes and that the As/P-ratio remains unchanged during shadow masked growth.     

Current and emerging molecular diagnostic technologies applicable to bacterial food safety

There is an increasing need for rapid test methods to certify the quality and safety of food products. Current tests applied for the microbiological assessment of food products are based on standard approved culture-based isolation methods and can take several days to yield results. Nucleic acid diagnostic (NAD) tests for the identification of bacterial foodborne pathogens employing in vitro amplification technologies are capable of sensitive and specific detection of single or multiple pathogens in foods in a shorter timeframe than traditional methods. New developments in molecular biosensors have the potential to provide at-line bioanalysis, whereas microarray-based technologies may in the future be the NAD platforms of choice for multiple pathogen detection and identification. This article reviews current and emerging NAD platforms for foodborne bacterial pathogens that have the potential to impact food safety.     

氧气放电辅助激光淀积原位制备高T_c超导薄膜

采用低压氧气放电辅助的激光淀积方法,原位外延生长出零电阻温度91K,临界电流密度10~5A/cm~2的Y-Ba-Cu-O高温超导薄膜。扫描电镜和X光衍射分析结果表明,薄膜中超导相晶粒的生长具有c轴垂直于表面的择优取向。     

Evidence of thermally induced borehole elongation: a case study at Soultz, France

When they occur, borehole breakouts are considered strong markers of principal stress directions at depth. An innovative processing method for automatically identifying breakouts from ultrasonic borehole wall images has been developed. It has been applied to data sets from two deep, sub-vertical wells (GPK1 and GPK2) at the Soultz geothermal site in eastern France. In well GPK1, below 3 km depth, compression breakouts, with a 95°±7° azimuth, increasingly occur with depth. They result from time dependent compression failure at sub-critical stress levels and are indicators of the minimum horizontal principal stress orientation. However, in the uppermost logged section of well GPK2 (1.6–2.9 km depth), continuous borehole elongations share roughly the same azimuth with so called drilling-induced fractures (164°±18° and 175°±17° azimuth, respectively). Both features concomitantly vanish with depth, together with the amplitude of the thermal perturbation induced by drilling. It is proposed that these latter borehole elongations result from a pervasive, cooling-induced, tensile micro-cracking process prior to macroscopic failure localization. They are termed thermal elongations and are indicators of the maximum horizontal principal stress orientation. Had a simple logging caliper tool been used for this work, these thermal elongations might have been confused with classical compression breakouts. A simple criterion for differentiating compression breakouts from thermal elongation is proposed.     

Geotechnical Investigation Strategies for Lunar Base

Geotechnical characterization of potential lunar sites will be a critical part of the planning and design process. The strategies used to conduct a geotechnical investigation will be dictated by the specific needs of the lunar base, the unique environment of the lunar surface, and general character of the lunar soils and rocks. This paper outlines some of the types of geotechnical information that will be important and identifies some of the more promising strategies which might be used to obtain such information in the lunar environment. Some of the most important geotechnical information for planning and site development will be related to construction in the lunar soil. In addition to construction concerns, geotechnical data for foundation design (or verification of predesigned foundations) will be needed. The geotechnical site‐characterization work should include geophysical techniques, supplemented by conventional mechanical boring and testing only to the degree necessary to correlate geophysical measurements with conventional soil properties and to investigate anomalies. Equipment used for geotechnical site characterization will also serve for mineralogical exploration. Several techniques for geotechnical investigation that may provide very useful information in an expedient manner are described. Geophysical methods include seismic and electromagnetic methods, including seismic surveys that utilize surface waves. Electromagnetic methods such as ground‐penetrating radar are fast, efficient methods for mapping the subsurface, although these techniques do not measure soil characteristics that can readily be correlated with engineering properties. Seismic methods provide information that may correlate with soil strength, compressibility, and excavatability. In‐situ physical testing will likely include penetration testing for direct physical measurement of lunar soil behavior.     

Subsurface Characterization at Ground Failure Sites in Adapazari, Turkey

Ground failure in Adapazari, Turkey during the 1999 Kocaeli earthquake was severe. Hundreds of structures settled, slid, tilted, and collapsed due in part to liquefaction and ground softening. Ground failure was more severe adjacent to and under buildings. The soils that led to severe building damage were generally low plasticity silts. In this paper, the results of a comprehensive investigation of the soils of Adapazari, which included cone penetration test (CPT) profiles followed by borings with standard penetration tests (SPTs) and soil index tests, are presented. The effects of subsurface conditions on the occurrence of ground failure and its resulting effect on building performance are explored through representative case histories. CPT- and SPT-based liquefaction triggering procedures adequately identified soils that liquefied if the clay-size criterion of the Chinese criteria was disregarded. The CPT was able to identify thin seams of loose liquefiable silt, and the SPT (with retrieved samples) allowed for reliable evaluation of the liquefaction susceptibility of fine-grained soils. A well-documented database of in situ and index testing is now available for incorporating in future CPT- and SPT-based liquefaction triggering correlations.